Hach PHC729 Скачать руководство пользователя страница 16

Figure 6  Add KCl crystals to the probe

8.4 Replace the filling solution

Replace the filling solution and KCl crystals when one of the conditions that follow occurs:

• The filling solution becomes contaminated.
• The KCl crystals in a probe do not move freely through the liquid when the probe is inverted.

1.

Tilt the probe and open the filling hole.

2.

Use a syringe or small transfer pipet to remove as much of the filling solution and KCl crystals
from the probe as possible. Discard the solution and KCl crystals.

3.

Remove the remaining KCl crystals as follows:

a.

Fill the probe half full with deionized water. Close the filling hole.

b.

Shake the probe until the crystals become loose.

Note: If the crystals do not loosen, fill the probe with deionized water and put the probe in a warm water
bath (maximum 60 °C (140 °F)) for approximately 10 minutes.

c.

Use a syringe or small transfer pipet to remove the remaining solution and KCl crystals.

4.

Rinse the inner probe three times with deionized water.

5.

Rinse the inner probe three times with new filling solution.

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Содержание PHC729

Страница 1: ...DOC022 53 80433 PHC729 05 2021 Edition 2 User Manual...

Страница 2: ......

Страница 3: ...rocedure 8 Section 6 Sample measurement 9 6 1 Sample requirements 9 6 2 Sample measurement notes 9 6 3 Sample measurement procedure 9 Section 7 Verify the calibration 10 7 1 Verification procedure 10...

Страница 4: ...Table of Contents 2...

Страница 5: ...r the best accuracy do not use the probe to measure the pH of very alkaline samples Figure 1 Probe overview 1 Probe soaker bottle with storage solution 5 Probe soaker bottle holder 2 Filling hole plug...

Страница 6: ...but not improper use or wear Certifications CE FCC ISED Section 3 Safety information 3 1 Intended use The Intellical PHC729 probe is intended for use by individuals in the laboratory who measure the p...

Страница 7: ...probe with a blocked filling hole will not operate correctly New probes are filled with electrolyte filling solution and have a soaker bottle that contains storage solution to keep the glass bulb and...

Страница 8: ...e meter starts for the first time or after battery replacement 8 Connect the probe to the meter 9 Remove the filling hole plug before use Keep the level of the electrolyte filling solution above the l...

Страница 9: ...2 or more pH units apart For a one point calibration use a pH buffer near the expected sample pH Use the default calibration options or change the options in the probe settings menu Use the single di...

Страница 10: ...ffer solution Make sure that the sensor and reference junction are fully in the solution Do not put the probe on the bottom or sides of the beaker 6 Shake the probe from side to side to refresh the re...

Страница 11: ...e specified operating temperature of the probe Refer to Specifications on page 3 6 2 Sample measurement notes Read the notes that follow before sample measurements Rinse the probe with deionized water...

Страница 12: ...ay shows the pH buffer solution to use for verification Note Menu name for HQd meters Run check standard 2 Prepare or pour the pH buffer solution into a beaker 3 Open the filling hole 4 Rinse the prob...

Страница 13: ...ater Dry the probe body with a lint free cloth 4 Soak the probe in pH 4 buffer for 20 minutes 5 Rinse the probe with deionized water Dry the probe body with a lint free cloth Table 1 Cleaning solution...

Страница 14: ...crystals to the probe The filling solution in the probe contains crystals of potassium chloride KCl that keeps the filling solution saturated with KCl When the sample temperature is more than 60 C 140...

Страница 15: ...ttle 2 Measuring scoop 5 Saturated KCl solution 3 KCl crystals Table 2 KCl quantity at high temperatures Temperature KCl quantity 60 C 140 F 0 5 g 0 5 cm 0 2 in 70 C 158 F 0 625 g 80 C 176 F 0 750 g 9...

Страница 16: ...d KCl crystals from the probe as possible Discard the solution and KCl crystals 3 Remove the remaining KCl crystals as follows a Fill the probe half full with deionized water Close the filling hole b...

Страница 17: ...N O T I C E Probes can become permanently damaged if kept in a storage solution that is not specified by the manufacturer Use only the specified storage solution saturated KCl Do not store the probe i...

Страница 18: ...perature difference between samples Increase the sample temperature or adjust the temperature of different samples to be the same within 2 C 3 6 F Procedure problem causes slow stabilization and preve...

Страница 19: ...lution kit Singlet one use packets 20 mL each 2 x 10 pkg 2769920 pH 7 00 and 10 01 buffer solution kit Singlet one use packets 20 mL each 2 x 10 pkg 2769820 pH color coded buffer solution kit NIST 500...

Страница 20: ...5013 Beaker 30 mL plastic green 80 pkg SM5014 Beaker dispenser and holder 30 mL 1 923 656 Beaker holder 30 mL 1 923 556 Beaker 100 mL polypropylene 1 108042 Filling hole plug clip on 1 M035J35 LIS low...

Страница 21: ......

Страница 22: ...669 2932 orders hach com www hach com HACH LANGE GMBH Willst tterstra e 11 D 40549 D sseldorf Germany Tel 49 0 2 11 52 88 320 Fax 49 0 2 11 52 88 210 info de hach com www de hach com HACH LANGE S rl 6...

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