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2.3  Calibration Menu 

 

Calibration menu allows the user to calibrate the analyzer. Zero and Span Calibration menus allow the user to 

run the zero and span calibration cycles for a single range or for all system ranges available. 

 

Calibration Menu Diagram 

 

2.3.1  Zero Calibration 

 

Z E R O    C A L I B R A T I O N                0 9 : 1 7 : 2 8    1 2 - 0 9 - 0 2 

                                                                               
  1 <    Z E R O    A D J U S T              1        0 . 0        [ 0 . 0 ]         
  2                                        2        0 . 0        [ 0 . 0 ]         
  3                                        3        0 . 0        [ 0 . 0 ]         
  4      R U N    R E A G E N T S    P U R G E                                     
  5      R U N    Z E R O    C A L I B R A T I O N                                 
  6      R U N    Z E R O    C H E C K                                             
  7                                              R 1        R 2        R 3         
  8      Z E R O    P R O G R A M                    6    ,      4    ,      4         
  9      Z E R O    A V E R A G E                    4    ,      2    ,      2         

1 0                                                                             
1 1      - - >    Z E R O    P R O G R A M                                         

 

 

                                                                           

 

Zero Calibration menu allows the user to enter the suggested Zero Adjust values, to start the Reagent Purge 

cycle, to start the Zero Calibration and Zero Check cycles and to program the number of zero reactions run at 

each range.  

 

1.-3. Zero Adjust. 

The Zero Adjust is used to compensate any organic contamination in the acid and base 

reagents and any absorbed CO

2

 in the base reagent. The Zero Adjust values are generated automatically 

by the system for each range when the zero calibration cycle is completed without any system warnings. 

Zero Calibration cycle is activated by selecting the RUN ZERO CALIBRATION function in this menu. 

 

When a Zero Check cycle is run using the RUN ZERO CHECK function, the system only checks the zero 

response at each range and displays the suggested Zero Adjust values in brackets “[ ]” for all ranges next 

to the current Zero Adjust settings. When a Zero Check cycle is completed, if necessary the suggested 

Zero Adjust values can be programmed manually by entering the corresponding suggested Zero Offset 

values for each range (1, 2 and 3) in this menu. When the Zero Adjust settings are entered manually, 

system logs this information in the reaction archive with the prefix “ZM” (Zero Manual).  

 

4.   Run  Reagents Purge. 

The RUN REAGENTS PURGE function is used to prime all reagents in the 

BioTector. If necessary, the pump operation time for Reagent Purge cycle can be increased in the 

Reagents Purge menu.  

 

5.   Run Zero Calibration. 

Each time BioTector reagents are replaced or topped up and each time a service 

is carried out, it is strongly recommended to use the RUN ZERO CALIBRATION function so that the 

system can set the zero offset values automatically. The zero calibration reactions operate in the same 

manner as a normal reaction. Depending on system settings, BioTector  either takes DI Water as a 

sample or does not take any sample during the Zero Calibration cycle. See ZERO WATER in section 

8.3.4.2 

Zero Program

 for details. To start the zero calibration, press the ENTER key at this menu 

item. An “*” will indicate that the function is running. At the end of the Zero Calibration cycle, the following 

settings are checked and updated: 

ENTER PASSWORD

CALIBRATION

 ZERO CALIBRATION

 SPAN CALIBRATION

Содержание BioTector B3500

Страница 1: ...DOC023 53 90740 BioTector B3500 Online TOC Analyzer BASIC USER MANUAL 6 2018 Edition 1...

Страница 2: ......

Страница 3: ...cautions 12 1 5 3 Pr cautions chimiques 12 1 5 4 Sample Stream Precautions 13 1 5 4 Pr cautions relatives aux chantillons 14 SECTION 2 OPERATOR S MANUAL 15 2 1 SOFTWARE SCREENS AND SOFTWARE MENU DIAGR...

Страница 4: ...be impaired 1 1 Information and Safety Signs used in the Manual When any supplementary information is required and if any hazards exist the necessary information and safety signs Information Caution...

Страница 5: ...sary to work with this component it should be handled with care This symbol when noted on a product illustrates the risk of chemical harm due to its corrosive acidic caustic or solvent nature Only qua...

Страница 6: ...rop ene indicates that The instrument complies with the European product directives health safety and environmental protection legislations Conforms to ANSI UL Std 61010 1 Certified to CAN CSA Std 610...

Страница 7: ...ned herein or for incidental or consequential damages in connection with the furnishing performance or use of this material The information contained in this manual is subject to change without notice...

Страница 8: ...ary oedema may develop with delayed onset usually one or more hours after exposure Following severe acute ozone toxification recovery is slow In the few severe human cases reported 10 14 days of hospi...

Страница 9: ...s g n rales de s curit Pri re d tre toujours attentif toutes les notices de prudence d avertissement ou de danger Le non respect des instructions de s curit peut engendrer la blessure grave d individu...

Страница 10: ...en Isoler les fils lectriques de l appareil avant de commencer tout travail dans le bo tier lectronique Seul le personnel lectricien qualifi est habilit effectuer tous travaux d lectricit Se conformer...

Страница 11: ...t Pour son fonctionnement BioTector emploie de l oxyg ne O2 comme gaz porteur L oxyg ne ne doit comporter aucun gaz carbonique CO2 ni d azote N2 Le taux moyen de consommation d oxyg ne du BioTector es...

Страница 12: ...sing appropriate safety equipment 1 5 3 Pr cautions chimiques La liste de la Section 6 R actifs et Standards de Calibration Section 6 Reagents and Calibration Standards num re un certain nombre de pro...

Страница 13: ...FA Per fluoro alkoxy Vinyl Reinforced Silicon Reinforced PVC Poly vinyl chloride Fittings PFA Per fluoro alkoxy Stainless Steel SS 316 PVDF Poly vinylidene flouride Brass Pump Tubing EMPP Elastomer mo...

Страница 14: ...xy Vinyle Silicone renforc PVC renforc poly chlorure de vinyle Raccords PFA perfluoroalkoxy Acier inoxydable SS 316 PVDF polyfluorure de polyvinylid ne Laiton Tuyauterie de la pompe PPMOD polypropyl n...

Страница 15: ...ramming the BioTector The ENTER key which advances user to the next screen is also used to enter programmed settings in the BioTector The symbols used on BioTector LCD screen and their meanings are as...

Страница 16: ...Page 16 Software Menu Diagram...

Страница 17: ...yed on the top left hand side of the Analysis Data and Reagent Status screens On most other screens only the screen name is displayed in this location System status messages are displayed in the follo...

Страница 18: ...mple if the reaction is currently in the TIC Base Oxidation TOC phase The operation Range e g Range 1 2 or 3 the BioTector is using to carry out its analysis The Reaction Time which is the elapsed tim...

Страница 19: ...he analyzer in C e g 26 C The CO2 instantaneous value e g 56ppm CO2i and the CO2 zero value e g 12ppm CO2z of the reaction The elapsed time e g 265s since the start of the analysis 2 1 5 Reagent Statu...

Страница 20: ...r diagnostics to download data to program the software functions and to program the system specific settings in the BioTector The sub menus in this level can be password protected using the Password m...

Страница 21: ...Standby in the system reaction archive The 4 20mA signal or other output devices are not updated When remote standby signal is deactivated the BioTector starts analyzing When remote standby signal is...

Страница 22: ...eyboard the BioTector stops as soon as its present reaction is completed An is displayed to let the operator know the function has been activated 4 Emergency Stop When this function is activated the B...

Страница 23: ...ils The comprehensive Zero Check Calibration and Span Check Calibration parameters are programmed in Zero Program and Span Program menus respectively see Section 8 3 4 2 Zero Program and 8 3 4 3 Span...

Страница 24: ...n Check menu 3 If Span Calibration or Span Check is activated in New Reagents Program menu a Span Calibration or Span Check is carried out Once the procedure is completed the BioTector either stops or...

Страница 25: ...cate that this function has been selected If the BioTector is stopped then the Manual mode will start immediately To deactivate this function before the manual operation mode has started press the ENT...

Страница 26: ...on Archive screens To access the screens press the ENTER key and to return to the previous screen press the ESCAPE key 2 2 6 Fault Archive Menu In the Fault Archive menu the user can view the last 99...

Страница 27: ...startup time for a scheduled task for example the startup time for a manual sample sequence in Manual Program menu 2 2 8 Contact Information Contact Information menu displays the manufacturer distribu...

Страница 28: ...em only checks the zero response at each range and displays the suggested Zero Adjust values in brackets for all ranges next to the current Zero Adjust settings When a Zero Check cycle is completed if...

Страница 29: ...8 Zero Program Zero Program function allows the user to program the number of zero reactions run at one or more ranges R1 R2 and or R3 When the number of zero calibration reactions for one or two of t...

Страница 30: ...below are displayed in this menu 1 3 TOC Span Adjust This menu item allows the user to set the TOC span adjust factors manually by entering the STANDARD solution used and the calibrated average react...

Страница 31: ...alibration and Span Check reactions are carried out If the selected range is in conflict with the programmed CALIBRATION STANDARD concentration in this menu system automatically displays a Caution Rea...

Страница 32: ...for TOC Calibration Standard above Section 8 3 4 3 Span Program and Section 6 2 Calibration Standards for further details 21 TC Check Std In VOC systems the sum of the TIC and TOC Check Standard solut...

Страница 33: ...DOC012 97 80506 User Guidance for EMC Class A Equipment EMC A A A...

Страница 34: ...years The product manufacturing date can be found on the product label on the main board enclosure behind the display BioTector 25 EFUP CHINA ROHS DECLARATION TABLE ROHS Part name Toxic or Hazardous...

Страница 35: ......

Страница 36: ...orders hach com www hach com HACH LANGE GMBH Willst tterstra e 11 D 40549 D sseldorf Germany Tel 49 0 2 11 52 88 320 Fax 49 0 2 11 52 88 210 info de hach com www de hach com HACH LANGE S rl 6 route de...

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