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Section 12

Material Safety Data Sheets (MSDS)

12.1 Silicon antifoam (part number 33156)

PRODUCT AND COMPANY IDENTIFICATION

PRODUCT NAME

Silicon antifoam, emulsion, 30% in water

COMPANY

Hach Lange SA
6 Route de Compois
Case Postale 212
CH-1222 Vésenaz, Switzerland

PHONE NO.

0041 22 594 64 00

COMPOSITION / INFORMATION ABOUT THE COMPONENTS

INGREDIENT

CAS NO

PERCENT

HAZARDOUS

Silicone antifoam emulsion
Water

N/A
7732-18-5

70%
30%

No
No

IDENTIFICATION OF HAZARDS

OVERVIEW

SPECIAL INDICATION OF HAZARDS TO HUMANS AND THE ENVIRONMENT
Not hazardous according to Directive 67/548/EEC.

FIRST AID

INHALATION

If inhaled, remove to fresh air. If breathing becomes difficult,
call a physician.

INGESTION

If swallowed, wash out mouth with water provided person is
conscious. Call a physician.

SKIN CONTACT

In case of contact, immediately wash skin with soap and
copious amounts of water.

EYE CONTACT

In case of contact with eyes, flush with copious amounts of
water for at least 15 minutes. Assure adequate flushing by
separating the eyelids with fingers. Call a physician.

FIRE FIGHTING MEASURES

FIRE EXTINGUISHING MEDIA

Suitable: Water spray. Carbon dioxide, dry chemical powder,
or appropriate foam.

SPECIAL INFORMATION

Wear self-contained breathing apparatus and protective
clothing to prevent contact with skin and eyes.

MEASURES IN CASE OF SPILLAGE

Wash spill site with soap solution. Flush spill area with copious amounts of water. Absorb on sand or vermiculite and place in
closed containers for disposal.

HANDLING AND STORAGE

Directions for Safe Handling: Avoid inhalation. Avoid contact with eyes, skin, and clothing. Avoid prolonged or repeated
exposure. Conditions of Storage: Keep tightly closed.

EXPOSURE CONTROLS / INDIVIDUAL PROTECTION

ENGINEERING CONTROLS

Safety shower and eye bath. Mechanical exhaust required.

GENERAL HYGIENE MEASURES

Wash thoroughly after handling.

PERSONAL PROTECTIVE EQUIPMENT

Eye Protection: Chemical safety goggles.

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Содержание ORBISPHERE 6110

Страница 1: ...DOC024 52 93009 ORBISPHERE Model 6110 Package Analyzer User Manual 08 2013 Edition 5 ...

Страница 2: ......

Страница 3: ...ion 3 Installation 19 3 1 Unpacking 19 3 2 Main components 19 3 3 Positioning 20 3 4 Installation 20 3 4 1 Pre installation 20 3 4 2 Physical installation 21 3 4 3 Post installation procedures 21 3 5 Additional installation information 22 3 5 1 Microsoft ActiveSync configuration 22 3 5 2 Power supply 23 3 5 3 Emergency STOP button 23 3 5 4 Antifoam cartridge preparation 23 Section 4 User Interface...

Страница 4: ...le 45 6 4 Barometric pressure sensor 46 6 5 Pressure sensor 46 6 6 Temperature sensor 47 6 7 Carbon dioxide sensor 47 6 8 Flow sensor 48 6 9 Oxygen sensor 48 Section 7 Measurement 49 7 1 Main screen 50 7 1 1 User 50 7 1 2 Package ID 50 7 1 3 Start analysis 50 7 2 Diagnostic measurement and results views 53 7 2 1 Measurement view 53 7 2 2 Results view 53 Section 8 Analysis 55 8 1 Analysis menu over...

Страница 5: ...ning messages 63 10 1 1 Error messages 63 10 1 2 Warning messages 64 10 1 3 Red LED s on startup screen 65 10 1 4 Measurement problems 66 Section 11 Spare Parts and Accessories 67 Section 12 Material Safety Data Sheets MSDS 69 12 1 Silicon antifoam part number 33156 69 ...

Страница 6: ...4 Table of Contents ...

Страница 7: ...acking setting up or operating this instrument Pay particular attention to all warning and caution statements Failure to do so could result in serious injury to the operator or damage to the equipment To ensure the protection provided by this equipment is not impaired do not use or install this equipment in any manner other than that which is specified in this manual 1 3 1 Use of hazard informatio...

Страница 8: ...l not result in eye injury Class 1 LASERS may therefore be considered safe However Class 1 LASER products may contain LASER systems of a higher Class but there are adequate engineering control measures to ensure that access to the beam is not reasonably likely This Class 1 Laser product complies with 21 CFR Chapter 1 sub chapter J It is evaluated and tested in accordance with EN 61010 1 Safety Req...

Страница 9: ... only individuals qualified to work with hazardous voltages should open the enclosure or remove the barrier This symbol when noted on the product indicates that the marked item can be hot and should not be touched without care This symbol when noted on the product indicates the presence of devices sensitive to electrostatic discharge and indicates that care must be taken to prevent damage to them ...

Страница 10: ...réglementation européenne directive UE 2002 96 EC les utilisateurs de matériel électrique en Europe doivent désormais retourner le matériel usé ou périmé au fabricant pour élimination sans frais pour l utilisateur Remarque Veuillez vous adresser au fabricant ou au fournisseur du matériel pour les instructions de retour du matériel usé ou périmé aux fins d élimination conforme ITALIANO Le apparecch...

Страница 11: ...tlijn 2002 96 EC dienen gebruikers van elektrische apparaten voortaan hun oude of afgedankte apparatuur kosteloos voor recycling of vernietiging naar de producent terug te brengen Nota Als u apparatuur voor recycling terugbrengt moet u contact opnemen met de producent of leverancier voor instructies voor het terugbrengen van de afgedankte apparatuur voor een juiste verwerking POLSKI Sprzęt elektry...

Страница 12: ...bove symbol may not be disposed of in European public disposal systems after 12 August 2005 Hach Lange will offer to take back free of charge to the customer any old unserviceable or redundant instruments and systems which carry the above symbol and which were originally supplied by Hach Lange Hach Lange will then be responsible for the disposal of this equipment In addition Hach Lange will offer ...

Страница 13: ...ng of electrical and electronic equipment Currently monitoring and control instruments do not fall within the scope of the RoHS Directive however Hach Lange has taken the decision to adopt the recommendations in the Directive as the target for all future product design and component purchasing Note The following only applies to exports of this product into the People s Republic of China Backlit di...

Страница 14: ...12 General Information ...

Страница 15: ... height 340 mm 13 39 ins Minimum package height 90 mm 3 54 ins Minimum volume 150 ml Material Glass PET or aluminum Enclosure Dimensions L x W x H 537 x 540 x 942 mm 21 1 x 21 3 x 37 1 ins Weight 55 kg 121 lbs Enclosure protection IP20 Power requirements 100 240 VAC 10 50 60 Hz Power consumption Max 250 VA Purge gas CO2 with purity 99 9 at 6 to 7 bar absolute 87 to 102 psia Purge gas consumption 0...

Страница 16: ...14 Specifications 2 2 Instrument dimensions Figure 1 Instrument dimensions ...

Страница 17: ... Main instrument components 2 3 1 Front view 1 Display panel 4 Knob to tilt package 2 Package piercing device 5 Measurement start button with LED 3 Package holder 6 Package backstop Figure 2 Instrument components front view ...

Страница 18: ...ations 2 3 2 Left side view 1 Power socket 4 Ethernet connection 2 Power ON OFF rocker switch 5 USB B client 4 pin connector 3 USB A connector for mass storage device Figure 3 Instrument components left side view ...

Страница 19: ...on No 1 IN Forcing gas Air or N2 4 Gas connection No 4 OUT Pressure sensor calibration 2 Gas connection No 2 IN Purge gas CO2 99 9 purity 5 Emergency STOP button 3 Gas connection No 3 IN Reference gas CO2 only Figure 4 Instrument components right side view ...

Страница 20: ... coefficients can be included and the total O2 contained in the bottle is calculated by integrating this function Note For faster measurements the liquid analysis step can be skipped and the O2 value calculated from the headspace by setting specific parameters for the package see Package parameters on page 35 for additional details 4 Headspace volume At the end of the run the gas flow is stopped a...

Страница 21: ...Any work inside the analyzer should be performed exclusively by personnel specialized and authorized to work on electrical installations In addition and in accordance with safety standards it must be possible to disconnect the power supply of the analyzer in its immediate vicinity WARNING Electrical danger and fire hazard Only use the supplied power cable Only qualified experts may perform the tas...

Страница 22: ...ocedure for 6110 TPA document supplied with the instrument The new cartridge is included in the sensor recharge kit also supplied with the instrument Solenoid valve 2 2 NC with O ring 33122 Filter with Goretex membrane 52 items 33124 Piercing tip x1 for PET DG33308 Piercing tip x2 for metal 33127 Piercing tip mounting tool 33159 Pneumatic tubing kit 33154 Antifoam recharge bottle 1L 33156 Antifoam...

Страница 23: ...efer to Microsoft ActiveSync configuration on page 22 for installation details b Connect your PC to the instrument via the USB client connector No 5 in Figure 3 on page 16 ActiveSync will start automatically By default ActiveSync proposes to set up a partnership with the instrument This is not required so select NO before continuing c Insert the supplied USB memory stick into your PC d Inside the ...

Страница 24: ...y installed ActiveSync will start automatically each time the instrument is connected to the PC Note By default ActiveSync proposes to set up a partnership with the instrument This is not required so make sure this is set to NO as illustrated left before continuing The ActiveSync screen is then displayed and an icon will appear in the taskbar at the bottom of your screen When active the icon in th...

Страница 25: ...liquid to the cartridge 100mL volume syringe tubing and connectors Note One antifoam recharge bottle should be enough to fill the cartridge at least 3 times and a cartridge completely filled with antifoam is sufficient for approximately 3 000 measurements Important Note To optimize the performance and reliability of the instrument it is strongly recommended to only use the silicon antifoam supplie...

Страница 26: ...e syringe is full 4 Remove the syringe and tubing from the recharge bottle 5 Attach the end of the tubing from the syringe to the other piece of tubing using the quick fit connector 6 Remove any trapped air in the system by applying a small amount of pressure to the end of the connector with a small screwdriver or similar to open the valve Push slightly on the end of the syringe until antifoam can...

Страница 27: ... Screw the cap back onto the antifoam container and store the tools and container in a cool dry place Important Note After installation of the antifoam cartridge in the analyzer it is critical that any air bubbles be cleared from the antifoam circuit before taking any measurements To do this select the Antifoam system option from the Actuator verification option in the Maintenance menu and follow ...

Страница 28: ...26 Installation ...

Страница 29: ... time or if maintenance procedures need to be carried out inside the instrument 4 1 2 Touch screen The instrument front panel is comprised of a TFT VGA 640x480 color display touch screen acting as display touch pad and keyboard 4 1 3 Data entry When a text box alphanumeric field is selected for data entry a virtual keyboard appears on screen as illustrated below This is used in a similar way to a ...

Страница 30: ...e the instrument in operational mode if there is a long time delay between measurements The screen will go blank but can be reactivated by tapping it Once reactivated you will need to enter a valid user ID and password combination if this has been set up see User identification and access level on page 31 Configuration Refer to Configuration on page 33 Calibration Refer to Calibration on page 45 M...

Страница 31: ...em A green indicator means that no problems have been found A yellow indicator means that a problem has been found but is not serious enough to stop measurements being taken A red indicator means that there is a serious problem with the system which must be corrected before any measurements can be performed If multiple problems have been detected the color of the LED will reflect the most severe e...

Страница 32: ...e Skip button when the component has the yellow indicator against it to indicate the component check is in progress The right side of the screen lists each of the instrument components that are being checked and a colored indicator to the left of each component shows the current status A green indicator means that the component is installed and working correctly A red indicator means that there is...

Страница 33: ...ication and password in the boxes provided and press Ok to continue Your details will be displayed at the top left corner of the screen Then press the Ok button at the bottom left of the screen to gain access to the main menu There are three user access levels For security purposes when the session inactivity delay period has expired adjustable using the option Security and user management on page...

Страница 34: ...32 User Interface and Startup 4 3 Menu structure overview ...

Страница 35: ...33 Section 5 Configuration 5 1 Configuration menu overview ...

Страница 36: ...fine the display resolution for all values displayed by the instrument These are the same as listed for units with the addition of Formula For each parameter select the required display resolution from a drop down list A maximum of 4 digits and a decimal point can be displayed i e 1234 123 4 12 34 or 1 234 This does not affect the actual resolution of data measured and stored only the data display...

Страница 37: ...on page 36 for details Package tab Comment Enter a free format alphanumeric text This text will appear against the package description in the main package management screen Brimful volume Enter the volume of the package when full to overflowing Height Enter the overall height of the package This information is used if you activate the Package size check option in Instrument parameters on page 37 T...

Страница 38: ...the formula is invalid and green when valid When the indicator is red the Ok button will be unavailable Use the Select button to select an existing formula to include in the new formula The list of existing formulae is displayed as a rolling list When a valid formula has been entered press the Ok button to continue You are then requested to assign a name to the new formula after which an informati...

Страница 39: ...rd measurement progress screens being displayed during the measurement process the measurement values are displayed instead see example in Measurement view on page 53 Display diagnostic results Use this option to troubleshoot measurement problems If this box is checked then instead of the standard measurement results screen being displayed at the end of the measurement process more detailed measur...

Страница 40: ...buffer recording the last 1000 actions Logout timer Enter a maximum time of inactivity in minutes for all users Users are logged out automatically when the period of inactivity exceeds this value and the Auto logoff feature is enabled Clear audit trail file This option deletes the audit file Clear result file This option deletes the package measurement data User management When selected the list o...

Страница 41: ...orage device such as a USB memory stick into the USB A port at the rear left of the instrument No 3 in Figure 3 on page 16 The instrument should automatically recognize the presence of the device It may be that some USB memory sticks are not compatible with the instrument and will not be recognized In this case the only solution is to try another brand of memory stick or to access the instrument u...

Страница 42: ...nnection to download data from the instrument to a PC This can be to a web page see Web browser below using an HTTP connection or to an OPC client see OPC client on page 42 using a DCOM connection These options allow you to perform several operations directly from your PC To be able to use these options the instrument must be connected to the network At the bottom of the ethernet connection screen...

Страница 43: ... the option selected you will have the possibility to browse through all pages of the reports by clicking on the First Previous Next and Last buttons at the bottom Click on Exit to select another report or click directly on the list of reports on the left To download the data for your selected option right click on Import top right of the screen and select Save Target As Then selected a location o...

Страница 44: ...d the CLSID into the OPC client software on the PC to establish the two way network link to the instrument The OPC protocol identifies the data passed between server and client with a three level hierarchy called an item The item may contain data error messages or warning messages To ensure total synchronization between PC and instrument all modifications that are made to data elements on the inst...

Страница 45: ...anual calibration Select a sensor and check the activation flag as required Calibration frequency When set the system will set a yellow status indicator message to inform you when a sensor calibration is required see also Instrument status indicator on page 29 Frequency selection Press the button to set the desired frequency Choose between Daily Weekly Monthly or Yearly by pressing the appropriate...

Страница 46: ...44 Configuration ...

Страница 47: ...least once a year The instrument will provide accurate results provided accurate reference standards are used The following table shows the maximum ranges for the standards These ranges should not be exceeded 6 3 Calibration schedule This following table shows the recommended sensor calibration intervals using the instrument s automatic calibration feature based on an average of 500 package analys...

Страница 48: ...rometric pressure value displayed If the values are the same press Cancel otherwise enter the new barometric value in the New barometric value box and press Validation to store the new setting 3 On completion a calibration report is created Calibration reports View the last 10 barometric pressure sensor calibration reports Pressure sensor New calibration 1 A calibration screen is displayed showing...

Страница 49: ...tion screen is displayed and the instrument measures two temperature values and checks the stability of the measurements Provided the measurements are stable you can choose to accept or reject the new values Press Validation to store the new setting 2 On completion a calibration report is created Calibration reports View the last 10 temperature sensor calibration reports Carbon dioxide sensor New ...

Страница 50: ...iding a continuous flow of fresh air in front of the sensor head Flow sensor New calibration 1 A calibration screen is displayed and the instrument will then compute the measured flow in four steps at 0 200 ml s 0 400 ml s 0 800 ml s and at 0 000 ml s The results are displayed on screen 2 After a few minutes when the process is complete the Validation button is highlighted Press this button to acc...

Страница 51: ...49 Section 7 Measurement The following flow chart shows an overview of the measurement process The actions listed on the left are performed by the user and those on the right by the instrument ...

Страница 52: ...s the same For optimal operation the base of the package holder should always have a layer of water for improved transfer of the ultrasound energy to the liquid in the package For the correct amount of water tilt the package holder forward by turning the tilt knob No 4 in Figure 2 on page 15 to position 3 small can icon Next fill the holder with water until the water level reaches the top without ...

Страница 53: ...the locking wheel clockwise finger tight Once the package is secure against the backstop and the piercing position aligned with the two red laser beams close the front door Start the measurement process by pressing the START button on the right side of the instrument base No 5 in Figure 2 on page 15 A progress bar is displayed at the bottom of the screen showing the elapsed time to date and the es...

Страница 54: ...lts by entering them in the text boxes displayed down the left The numerical values will be required if they have been defined as part of a formula see Formula management on page 36 Press the Continue button to return to the main measurement screen or press the Info button to display more detailed results again color coded in a tabular format For additional information on viewing the full set of m...

Страница 55: ...urement details are displayed down the left side of the screen The first line of the display shows the current stage in the process The right side of the screen gives additional textual information 7 2 2 Results view The following screen is displayed on completion of the measurement process Note If the Stored measured sensor values box at the bottom of the screen is checked the values are recorded...

Страница 56: ...54 Measurement ...

Страница 57: ...data and the Info button will be made available Press the Info button to see more details of the measurement in a new screen Use the Exit button to return to the main analysis menu Table settings This options allows you to define up to 10 data elements that the instrument will display for each measurement More data is recorded but only 10 values can be displayed on screen Define for each of the 10...

Страница 58: ...56 Analysis ...

Страница 59: ...Clean laser optics used to position the package Weekly Refill the antifoam cartridge see Antifoam cartridge preparation on page 23 Approximately every 6 weeks O2 sensor cartridge replacement and calibration see Wizards on page 58 Every 2 3 months Piercing gasket replacement see Wizards on page 58 Every 3 months Piercing tip replacement see Wizards on page 58 Every 6 months Clean antifoam cartridge...

Страница 60: ...tions Antifoam cartridge replacement A replacement cartridge can be used or the existing cartridge refilled with antifoam If refilling the existing cartridge follow the instructions given in Antifoam cartridge preparation on page 23 To ensure the performance and reliability of the instrument it is strongly recommended to only use the silicon antifoam supplied by Hach Lange part number 33156 EC sen...

Страница 61: ... position activated The black dot indicates that the piercing device is positioned in the reference home location End of travel upper bound activated The upper bound limit is located higher than the reference position If this button is activated it means that the system is in an abnormal state of operation and you should call your local Hach Lange representative End of travel lower bound activated...

Страница 62: ...thout moving the piercing assembly Press on the icon with the up arrow to raise the needle back into the home position Ultrasound ON OFF Switch between having the ultrasound system on or off Important Note Before turning ON remove any pierced packages from the package holder to avoid any liquid spillage With some water in the base of the package holder test the system is working by moving your fin...

Страница 63: ...s available from the spares kit delivered with the instrument Place this on the ultrasonic base of the instrument using the lasers to center it and lower the plastic front door 2 Activate the motor to lower the instrument head allowing the needle to penetrate approximately to the center of the beaker illustrated below Refer to Manual displacement above for details on lowering the instrument head 3...

Страница 64: ...3 6 System initialization Selecting this option initiates the standard system startup process without having to power the instrument off and on See Instrument startup on page 30 for more information on system startup 9 3 7 End application Select this option to perform an orderly shut down of the instrument On completion the instrument can be powered OFF 9 3 8 Service validation This option lists t...

Страница 65: ...canceled Problem of flow regulation during the measurement Check the purge gas pressure Change the Goretex filter The gas path is partially or totally blocked Control the antifoam injection HEX040 E40 Check gas supply current pressure xxxxx Before filling the reference volume the pressure is lower than 1 5 bar Check the purge gas pressure HEX080 E80 Rim detector is dirty Please clean it and restar...

Страница 66: ...ercing unit 4 Check the purge gas pressure Check the forcing gas pressure Check the Goretex filter Gas path not airtight Check the airtightness of the gas path between the piercing unit and the measurement chamber HEX010 N A A spontaneous and or too fast degassing has occurred Restart the measurement with another package 10 The package especially in the case of cans is losing pressure due to a lea...

Страница 67: ...witch instrument off wait 10 seconds and switch back on If the problem persists call Hach Lange service support Flow sensor No communication between sensor and board Sensor damaged Switch instrument off wait 10 seconds and switch back on If the problem persists call Hach Lange service support Pressure sensor No communication between sensor and board Sensor damaged Switch instrument off wait 10 sec...

Страница 68: ...place and not unscrewed Release emergency STOP button by turning it clockwise and restart the instrument Open the front door to stop the process Remove the bottle and check that the piercing spike is in place and is not unscrewed Close the front door and press the Abort button on the screen No antifoam being injected Go to the antifoam section of the maintenance wizard see the Antifoam system sect...

Страница 69: ...tom plate 33144 Protection shield 33156 Antifoam recharge bottle 33157 Antifoam cartridge empty 33160 Cover detector with cable 33162 Syringe for antifoam cartridge 6110 AD2 Total O2 CO2 package analyzer version 2 A1100 S00T Oxygen sensor for the 6110 DG33308 PET piercing tip DG33365 One year of consumables for the 6110 DG6110 MAN D 6110 Manual in German DG6110 MAN E 6110 Manual in English DG6110 ...

Страница 70: ...68 Spare Parts and Accessories ...

Страница 71: ...of water EYE CONTACT In case of contact with eyes flush with copious amounts of water for at least 15 minutes Assure adequate flushing by separating the eyelids with fingers Call a physician FIRE FIGHTING MEASURES FIRE EXTINGUISHING MEDIA Suitable Water spray Carbon dioxide dry chemical powder or appropriate foam SPECIAL INFORMATION Wear self contained breathing apparatus and protective clothing t...

Страница 72: ... N A N A N A N A N A N A N A N A 760 mmHg STABILITY AND REACTIVITY STABILITY Stable HAZARDOUS EXOTHERMIC REACTIONS Will not occur HAZARDOUS POLYMERIZATION Will not occur MATERIALS TO AVOID Strong oxidizing agents TOXICOLOGICAL INFORMATION ACUTE TOXICITY LD50 Oral Rat 5 000 mg kg LD50 Skin Rat 2 000 mg kg SENSITIZATION Sensitization Will not occur SIGNS AND SYMPTOMS OF EXPOSURE To the best of our k...

Страница 73: ...FORMATION Not hazardous according to Directive 67 548 EEC Caution Substance not yet fully tested EU COUNTRY SPECIFIC INFORMATION Germany WGK 1 Self Classification OTHER INFORMATION WARRANTY The above information is believed to be correct but does not purport to be all inclusive and shall be used only as a guide The information in this document is based on the present state of our knowledge and is ...

Страница 74: ...72 Material Safety Data Sheets MSDS ...

Страница 75: ...73 ...

Страница 76: ...2 orders hach com www hach com HACH LANGE GMBH Willstätterstraße 11 D 40549 Düsseldorf Germany Tel 49 0 2 11 52 88 320 Fax 49 0 2 11 52 88 210 info hach lange de www hach lange de HACH LANGE Sàrl 6 route de Compois 1222 Vésenaz SWITZERLAND Tel 41 22 594 6400 Fax 41 22 594 6499 Hach Lange 2013 All rights reserved Printed in Europe ...

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