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Содержание Aquamax KF

Страница 1: ...amax KF Portable Aquamax KF Portable v 13 08 UK Distribution by IMA Ltd Parkwell House Otley Road Guiseley West Yorkshire LS20 8BH England Tel 44 0 1943 878877 Email info ima co uk Website www ima co...

Страница 2: ...Panel Description Page 11 Setting Time Date Page 12 Connection Start Up Procedure Page 13 Programming A Method Page 14 20 Water Standard Test Page 21 Example Methods Applications Page 22 24 How To Run...

Страница 3: ...ula A anode reagent is suitable for most routine applications and is especially useful for water content determination of oil samples e g transformer oils crude oils etc This anode reagent is supplied...

Страница 4: ...lectrolysis current necessary to produce the required iodine This is an absolute technique which does not require calibration of the reagents For further information visit www grscientific com and dow...

Страница 5: ...user selectable Calculation modes Weight weight W w user programmable Weight dilution ratio W K Volume density V SG Volume volume V v Display format g mg kg ppm Print format g mg kg ppm Statistics max...

Страница 6: ...r prolonged period We advise connecting the Aquamax KF Portable to mains power supply for 12 hours before first switching the power on After unpacking your Aquamax KF Portable check that the glassware...

Страница 7: ...ator electrode lead connects to socket marked GENERATOR detector electrode lead connects to socket marked DETECTOR Place stirrer bar inside titration vessel Fit injection septa into plastic screw cap...

Страница 8: ...Aquamax KF Portable v 13 08 8 AQUAMAX KF TITRATION CELL...

Страница 9: ...microlitre syringe of water standard test pellet sampler and water standard pellets 1 0ml 5 0ml gas tight syringes and luer needles power pack in car adapter and Results Manager USB flash drive for s...

Страница 10: ...d reagent spillage onto the instrument casing Any spillage onto the instrument casing should be wiped off immediately to avoid damage or staining Remove the drying tube and injection septa Using the f...

Страница 11: ...blacked out while the drive is being written to and then as when idle The drive should only be removed when in the idle mode To read data saved on drive insert it into PC USB port Start Results Manage...

Страница 12: ...ing Aquamax KF Portable Press START 2 Hold down the key until the Aquamax KF Portable displays Set Date Time DD MM YYYY HH MM SS 3 Use the decimal point key to move the cursor across the screen 4 Use...

Страница 13: ...o precondition equilibrate microgram count Aquamax KF xxxx g 4 Precondition detector signal titration speed At the end of the precondition period the display will show Dft xxxx g Drift Test After the...

Страница 14: ...the previously stored value you can now select the correct value and press ENTER decimal point key allows scroll through of individual parameters in each menu When the required parameter is displayed...

Страница 15: ...Aquamax KF Portable v 13 08 15 PROGRAMMING FLOW CHART...

Страница 16: ...ition Press PROGRAM if you want to continue entering other parameters RESULT FORMAT Press PROGRAM Display will show Result Format g Results can be selected in g ppm mg kg or water If you want to selec...

Страница 17: ...e entered at any time during the titration by pressing PROGRAM or at the end of titration For ease of operation it is possible to enter the Total weight W as 0 0000gm then place the full sampler on th...

Страница 18: ...press ENTER Options available Off no result print out Every result will print result after every titration first result also prints all calculation input data Full Report will print results after ever...

Страница 19: ...applications such as certain gas samples or when using the Aquamax KF Portable combined with an oil evaporator or solids evaporator system it can prove useful to delay the end point of the titration B...

Страница 20: ...n be done by pressing a numerical key 0 9 and ENTER All titration parameters printer mode beeper mode etc are stored automatically Display then shows Save Method Done Then press CLEAR and the instrume...

Страница 21: ...show Water Standard Test Press Enter to activate and display will return to Ready mode Either using the 10 microlitre syringe with distilled water or using the water standard pellets and pellet sample...

Страница 22: ...Insulating liquids D 3401 Halogenated organic solvents D 4928 Crude oils D 5460 Rubber compounding materials D 6304 Petroleum products lubricating oils and additives D 6869 Plastics E 1064 Organic liq...

Страница 23: ...ml 0 1 0 5 0 5 or 1 ml 0 5 1 0 0 5 or 1 ml 1 0 5 0 0 2 ml above 5 0 0 1 ml or less Please note that these volumes are only a guide You may wish to experiment with sample size to determine the optimum...

Страница 24: ...1 then a sample size of 0 2 to 0 5 ml is suggested Some lubricating oils contain additives which can coat the detector electrode or block the glass frit of the generator electrode For these applicati...

Страница 25: ...rm that Aquamax KF Portable is in Ready mode 2 Flush 1 0ml syringe several times minimum 6 times with sample 3 Fit luer needle and flush through with sample 4 Draw sample into syringe beyond the 1 0ml...

Страница 26: ...either during the titration by pressing PROGRAM or waiting until the end of titration when display will prompt TARE Weight Enter the weight then press CLEAR ANALYSIS METHOD 2 1 Confirm that Aquamax KF...

Страница 27: ...e slot at the rear of the print head As soon as the printer sees the paper it will automatically load it To avoid damage to the printer mechanism it is advisable to only use the correct part number 50...

Страница 28: ...calibrated Date sample run Run number time of analysis F generator electrode with frit Nett microgram count after drift correction Drift value at start of titration Result format selected Calculation...

Страница 29: ...RATION If the detector electrode senses too much Iodine in the titration cell usually caused by instrument being left unoperated for a long period the display will read OVERTITRATION SEE INSTRUCTION M...

Страница 30: ...the titration cell and generator electrode 3 RINSE all parts with methanol Do not use brush on electrodes 4 DRY all parts 5 REASSEMBLE glassware 6 RECHARGE with fresh reagents If the cell is heavily...

Страница 31: ...new test WARNING LETTERS ON PRINT OUT Warning letters will be printed after time of each analysis to signify the following U Uncalibrated E Calibration expired B Battery level low A ACE system active...

Страница 32: ...Cell twin port glassware results manager software and accessories are supplied as standard As well as being a stand alone instrument the Aquamax KF Plus can be combined with our Oil Evaporator or a So...

Страница 33: ...titration vessel and micro combination electrode that regenerates to optimum efficiency in minutes and offers excellent stability for non aqueous titrations microTAN OPS Workstation Everything you ne...

Страница 34: ...urements we offer certified standards traceable to NIST and are tested using ISO 17025 accredited method Our conductivity standards have an accuracy of 1 0 and their shelf life is valid regardless of...

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