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24

463X Chlorine Systems Manual

Chlorine sensors need to be calibrated for accuracy. 

Calibration must be done with every new sensor and 

any time a membrane cap is replaced.  After the 4 hour 

conditioning period, Temperature Calibration and 

In-Process Calibration needs to be performed. Any 4 to 20 

mA or relay output devices should be of

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 ine.

Chlorine Sensor Temperature Calibration

The temperature element inside the chlorine sensor needs 

to be calibrated. Use a reference thermometer to verify 

the actual temperature of the sample. This value is then 

entered  in Step 4 to calibrate the system.  After completing 

Temperature Calibration, proceed to In-Process Calibration, 

page 25.

Tip:

 Remove the pH electrode from the 

fl

 ow cell and insert 

the reference thermometer. If no pH sensor is being used, 

remove the cell plug to insert the thermometer. Replace the 

plug after calibration.

Example: Set the calibrated temperature to 25.3 ºC.

1.  Go to the Calibrate Menu.

2.  Scroll down 

 3 menus to the 

Cl Temperature 

menu.

3.  Press 

 to enter Edit Mode.

4.  Enter the temperature reading. 

Example: 25.3

.

5.  Press the Enter button to save the setting.

6.  Exit to the View Menu.

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E X A M P L E

Step 2

4

 Cl Temperature

  Calibration:  

>

Cl Temp:  Cal

  +025.3 °C

Calibrate Menu

New temp. value

ENTER

ENTER

Lowest value noted for
Zero Cal.

Zero Cal:  ppm&nA

    0.20 / 001.0

  Cl Zero:

Calibration     

>

Calibrate Menu

Step 6

8

The signal level during a Zero Point 

Calibration must be at least 1 nA lower 

than the In-Process Calibration point.

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ENTER

ENTER

  Chlorine Sensor Calibration

Zero Point Calibration

Zero Point Calibration is only used at the factory to program 

the sensors zero calibration point. This value does not shift 

throughout the life of the electrode and does not need to 

be performed in the 

fi

 eld. After completing Temperature 

Calibration, proceed to In-Process Calibration, page 25.

For Reference Only:

The chlorine sensor needs to be calibrated against two 

chlorine references: zero chlorine and the process chlorine. 

Typically the zero point calibration is very stable. Calibration 

must be done with every new sensor and any time a 

membrane cap is replaced.

1.  Keep of

fl

 ine any 4 to 20 mA devices or relay actuated 

output devices that connect to the transmitter.

2.  Turn off the water 

fl

 ow and remove the powered chlorine 

sensor with the electronics still attached.

3.  Place the sensor tip in distilled water.

4.  Wait until the reading stabilizes, then save the 

calibration. Stirring the sensor in water is not necessary, 

but allows the signal to stabilize faster.

Example: Set the Zero Point Calibration at 1.0 nA.

5.  Go to the Calibrate Menu.

6.  Scroll down 

 one menu to the 

Cl Zero 

menu.

7.  Press 

 to enter Edit Mode. The live sensor readings in 

ppm and nA will be 

fl

 ashing. These readings cannot be 

modi

fi

 ed, but can only be saved as displayed.

8.  Press the Enter button at the lowest reading to save the 

setting or press           to escape without changes.

9.  Exit to the View Menu.

10. After Zero Point Calibration is complete, replace the 

sensor back into the 

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 ow cell and turn the water 

fl

 ow 

back on.

11. Wait until the chlorine readings stabilize once again, then 

perform a chlorine In-Process Calibration.

E X A M P L E

Содержание Signet 4630

Страница 1: ...The 4630 Free Chlorine and 4632 Chlorine Dioxide systems can be used for reporting chlorine residuals in accordance with EPA Method 334 0 Complete chlorine analyzer system allows quick setup and easy...

Страница 2: ...onal Protective Equipment PPE Always utilize the most appropriate PPE during installation and service of Signet products Pressurized System Warning Sensor may be under pressure take caution to vent sy...

Страница 3: ...Rating 1 to 8 bar 15 to 120 psi Pressure Regulator 0 69 bar 10 psi variation over all ranges of flow and pressure Flow tolerance 15 or rated specification above Flow rate limits 8 to 12 gph US 30 24 t...

Страница 4: ...Manual pH compensation If optional pH sensor is installed see page 22 to complete pH Sensor Calibration Step 7 Repeat step 5 and 6 if the optional pH sensor is being used Step 8 Install the influent...

Страница 5: ...low rate indicator Flow range limits Flow regulator with strainer Inlet port Drain port 3 8 inch hose Sampling port pH sensor electronics 3 2750 7 159 001 671 pH electrode 3 2724 00 159 001 545 Quick...

Страница 6: ...Flat washer Disc spring curved washer Knurled thumb nut 1700 2512 Flow cell bolt 2490 0554 Included in kit 3 4630 390 Item Quantity Flow cell nut 6 Flat washer 15 Disc spring 9 Knurled thumb nut 3 Flo...

Страница 7: ...the panel according to local electrical building and or plumbing codes and seismic requirements Use four 6 mm in diameter screws or bolts of sufficient length to mount the panel to a sturdy vertical...

Страница 8: ...Wiring Open the electrical box by loosening the four corner screws of the front cover Insert input power wiring into the pre drilled access hole on the left side of the electrical box using appropriat...

Страница 9: ...transmitter Recommended torque for the terminals is 7 lb in Do not run 4 to 20 mA loop cables in the same conduit as the power or other high voltage wiring Remove one installed jumper wire from both o...

Страница 10: ...net Chlorine Sensor Electronics 3 2650 7 159 001 670 10 9 8 7 6 5 4 3 2 1 GND 10 9 8 7 6 5 4 3 2 1 GND NO COM RELAY 2 NC NO COM RELAY 1 NC LOOP 2 LOOP 2 LOOP 1 LOOP 1 EARTH GROUND Black White Yellow R...

Страница 11: ...quire different electrolyte solutions 2630 Free Chlorine Electrode 2632 Chlorine Dioxide Electrode NOTE Inspect and change the membrane cap if damaged See page 36 Maintenance for cleaning procedure A...

Страница 12: ...e flow cell DryLoc Connection to Sensor Electronics Locking Ring Locking Ring Lock Lock 3 2724 00 159 001 545 pH electrode 3 2630 X FCL electrode 3 2750 7 159 001 671 pH electronics 3 2650 7 159 001 6...

Страница 13: ...sitioned lower than the influent water source to allow proper flow through the flow cell The flow cell must drain by gravity not system pressure When testing allow the sample to flow for a few seconds...

Страница 14: ...the previous operating display When editing the CALIBRATE or OPTIONS menus the transmitter will return to the default display after 10 minutes and then the VIEW menu in another 10 minutes if no activi...

Страница 15: ...ering the Key Code the display will show the first item in the selected menu Step 3 Scroll the menu in a loop with the or arrow keys Step 4 Press the key to select the menu item to be edited The first...

Страница 16: ...active during editing Only the flashing element can be edited Press ENTER to save the new value When you have set your desired value pressing the ENTER key stores the value on the screen making it imm...

Страница 17: ...maximum values for the current loop output Units are derived from Loop 1 Source If the Source 1 is changed be sure to re edit this page Loop 2 Source pH Choose pH or chlorine for this 4 to 20 mA curre...

Страница 18: ...Range Relay1 Rng ppm 0 00 5 00 Enter the range where Relay 1 will activate above and below this setpoint Relay1 PlsRate 120 pulses min Set the maximum pulse rate Range 1 to 400 pulses min Relay 1 Mod...

Страница 19: ...o Last Cal 10 18 09 Edit the calibration date End of Calibrate Menu Relay 2 Rng ppm 0 00 5 00 Enter the range where Relay 2 will activate above and below this setpoint Relay 2 Hys 0 20 ppm This relay...

Страница 20: ...OWN keys to manually output any current value from 3 6 mA to 21 00 mA to test Loop 1 output Test Loop 2 Press UP or DOWN keys to manually output any current value from 3 6 mA to 21 00 mA to test Loop...

Страница 21: ...of operation Low High C xxxx x xxxx x Lowest and highest temperatures the Cl sensor has been subjected to during operation Test Relay 1 Press UP or DOWN keys to manually toggle Relay 1 Off and On The...

Страница 22: ...5 prior to initially installing the sensor and during its normal lifetime If a pH sensor is not available but pH determination is necessary measure process pH with a separate test and enter the value...

Страница 23: ...nse it in distilled water 2 Place the pH sensor in a different buffer solution example pH 4 01 The pH standard and slope must be at least 2 pH units apart 3 Note the pH and mV readings on the View Men...

Страница 24: ...int E X A M P L E ENTER ENTER Chlorine Sensor Calibration Zero Point Calibration Zero Point Calibration is only used at the factory to program the sensors zero calibration point This value does not sh...

Страница 25: ...nd relay functions if applicable NOTE The current and relay outputs can be tested in the Options Menu Current Loop Settings Current outputs are passive outputs that can be spanned in the forward and r...

Страница 26: ...l The output will be 100 pulses minute when the input value is 1 or less The starting point endpoint and maximum pulse rate are selectable in the CALIBRATE menu Mechanical Relay Functions The 8630 rel...

Страница 27: ...11 Scroll down to the Relay 1 Hys menu 12 Press to enter Edit Mode 13 Set the hysteresis dead zone for this relay This affects the turn off only 0 3 ppm 14 Press Enter 15 Scroll down to the Relay 1 D...

Страница 28: ...lorine Gnd I O V 18 17 16 Signal Ground Digital S3 L data 5 VDC White Red Black Shield pH Signet 3 2750 7 159 001 671 N C 8630 Chlorine Gnd I O V 15 14 13 Signal Ground Digital S3 L data 5 VDC White R...

Страница 29: ...moval a Disconnect flow through system b Drain below sensor level 3 Confirm chemical compatibility before use 4 Do not alter product construction These electrodes require the Signet 2650 Amperometric...

Страница 30: ...e is 7 0 and the pH variation is 0 2 then automatic pH compensation is not required pH variation 6 5 7 0 7 5 8 0 8 5 9 0 0 0 3 0 1 0 2 Sample pH Automatic pH compensation recommended in ranges within...

Страница 31: ...ng with chemicals or solvents 4 Place a Lockout tag on the pipe when the sensor is removed for maintenance to prevent accidental opening and exposure to potentially hazardous chemicals Lubricate O rin...

Страница 32: ...buffer solutions from the electrode Dispose of all buffer solutions at the end of the day If the pH sensor will not calibrate within acceptable limits clean the electrode and recalibrate If the calibr...

Страница 33: ...for the application be used during the reassembling of the ow cell Maintenance 463X Chlorine Analyzer Flow Cell CAUTION Over time a sensor can get tight in the flow cell fitting When removing the sens...

Страница 34: ...for special O ring fitting instructions Butt all O ring joints together so there is no gap Remove the O rings during flow cell disassembly Both the O rings and all sealing grooves should be examined f...

Страница 35: ...shers and nuts 7 Install the assembled pressure regulator and the two round O rings into the flow cell 1 Install the four O ring segments 2 Insert the center bolt into the block 3 4 Align and place th...

Страница 36: ...olution Slowly fill until solution begins to flow out of holes Do not allow the solution to run down the electrode and wet the electrical contacts in the DryLoc connector 6 Slowly screw on the membran...

Страница 37: ...e nA reading should start to rise Response time and nA reading will depend upon the temperature of the appropriate solution 15 Once the sensor s nA reading reaches approximately 300 360 nA allow the s...

Страница 38: ...the glass wet when out of the process Never store the electrode at temperatures below 0 C 32 F or allow it to dehydrate Never scrape or sand the glass electrode surface Treat glass electrode surfaces...

Страница 39: ...tmosphere Algae growth in flow cell Low chlorine concentration in water Locate flow cell away from light Exposure to light Excessive small bubbles in flow cell accumulating on sensors Water source con...

Страница 40: ...water Electrode not properly conditioned Noise interfering with the measurement Calibration incorrect Condition new sensor for 4 hours Cap replacement or electrolyte refill 2 hours Properly ground sys...

Страница 41: ...e calibration point is too close to standard point Wrong data is entered pH buffer solution used has value too close to standard point Re enter correct data Use proper buffer solution at least 2 pH un...

Страница 42: ...ged pH sensor Check pH sensor connections or change pH input to Manual in Options Menu FCl CHK pH PREAMP pH preamp is not detected pH preamp is not connected Wrong wiring Damaged preamp Check pH pream...

Страница 43: ...priate DPD test Electrode not making good contact with electronics Inspect and reconnect Unstable output from sensor Electrode needs to be repolished Polish gold electrode Not enough electrolyte Check...

Страница 44: ...on of Conformity according to FCC Part 15 This device complies with Part 15 of the FCC rules Operation is subject to the following two conditions 1 This device may not cause harmful interference and 2...

Страница 45: ...y not cause harmful interference and 2 This device must accept any interference received including interference that may cause undesired operation General Compatibility Electrode Signet 2724 00 Flat p...

Страница 46: ...02 to 2 ppm mg L 3 2630 2 0 05 to 5 ppm mg L 3 2630 3 0 1 to 20 ppm mg L Free Chlorine pH 5 0 to 8 5 pH Chlorine Dioxide 3 2632 1 0 to 2 ppm mg L Chlorine Dioxide pH 4 0 to 11 0 pH Temperature 0 C to...

Страница 47: ...149 F 0 to 6 9 bar 0 to 100 psi 65 C to 85 C 149 F to 185 F Linearity derated 6 9 to 4 0 bar 100 to 58 psi Temperature Storage 0 C to 50 C 32 F to 120 F CAUTION The electrode glass will be shattered i...

Страница 48: ...ectrode pH flat PT1000 in NPT 3 2750 7 159 001 671 pH Inline Electronics Digital S3 L 4 6 m 15 ft cable 3 2650 7 159 001 670 Chlorine Inline Amperometric Electronics Digital S3 L 4 6 m 15 ft cable Acc...

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