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ECP2010

ECP2010H

ECOM spol. s r.o., Trebonicka 239, 252 19 Chrastany u Prahy, Czech Republic

tel: +420 221 511 310, fax: +420 242 498 212, [email protected], http://www.ecomsro.com/

IČO: 411

192, DIČ: CZ411

92 192

User’s Guide

ECP2010/ECP2010H

NALYTICAL

HPLC

UMP

Содержание ECP2010

Страница 1: ...pol s r o Trebonicka 239 252 19 Chrastany u Prahy Czech Republic tel 420 221 511 310 fax 420 242 498 212 info ecomsro cz http www ecomsro com I O 411 92 192 DI CZ411 92 192 User s Guide ECP2010 ECP201...

Страница 2: ...refining information 03 27 06 2019 Kate ina Kn ourkov Jaroslav Form nek Up date of chapters 1 2 1 3 4 3 4 4 12 03 05 11 2019 Dominika Pavlov Jaroslav Form nek Address changein the footage of the firs...

Страница 3: ...h 14 4 5 1 Simple Manual Use 15 4 5 2 Automatic Backwash 15 4 6 Assemblage of Waste System 16 4 7 Connections on Unit Rear Panel 19 4 8 Start of Unit 20 4 9 Basic Control by Keyboard 20 4 10 Pump Init...

Страница 4: ...tialization by Pressing PUMP 33 Status after Unit Turning Off and On 33 6 3 3 Init Stop Reinit Program 33 6 3 4 Program Setup 34 6 3 4 1 Load Program 34 6 3 4 2 View Program 34 View Time Table 34 View...

Страница 5: ...face 47 6 6 6 Leakage State 47 6 6 7 Pump 48 6 6 8 Solvents 48 6 6 9 Pulsation 48 6 6 10 Gradient State 48 6 7 Service 49 6 7 1 Parts Replacement 49 6 7 1 1 Seals 50 6 7 1 2 Check Valves 52 6 7 1 3 Pi...

Страница 6: ...Correct Pressure 61 Released Bubble 62 Damaged Check Valves 62 Damaged Seals 63 11 MAINTENANCE 63 11 1 Periods 63 11 2 Cleaning and Decontamination 64 11 3 Cleaning Check Valves 64 11 4 Storage and Tr...

Страница 7: ...ode e g Menu Parameters Concentration 1 2 Produced Versions ECP2010 Analytical HPLC pump 40Mpa Cat ACA0000X ECP2010H Analytical HPLC pump 60MPa Cat ACF0000X Compatible boxes With gradient valves ECB20...

Страница 8: ...NF ABA16000 1 Tubing 1 8 900 mm with filter 2 um and lid ID 1 16 volume 1781 L only tubing thread 28 UNF lid for mobile phase reservoir LCT 02 with plug for tubing metal filter guide for connection at...

Страница 9: ...ere is a danger of its damage Caution Never dismount unit cover There is nothing needing customer service or maintenance Caution The pump is filled with isopropanol after construction or service Cauti...

Страница 10: ...g and washing head 5 Leakage sensor 6 Drain channel with cone for connecting waste system 7 Door hinges 8 Slots for tubing and capillaries 9 Display 10 Status LED PUMP green for indication of pump mot...

Страница 11: ...tem confirms newly set parameter value evokes QUICK DIAGNOSTICS screen ESC Returns one step back without saving changes B D A C Direction keys Using arrows up down increases decreases value of set par...

Страница 12: ...vice Isocratic connection of pump inlet Connect inlet tubing with filter Snap the tubing to the socket for tubing and capillaries Set of inlet tubing with a lid and filter picture on the right Gradien...

Страница 13: ...stem accessories and shall be ordered separately The injection valve holder is constructed for mounting two different types of valves and with hole for outlet capillary from pump to injection valve Rh...

Страница 14: ...Put the cable through the window and connect to connector START or IO Interface connector on unit rear panel Make configuration see 6 4 3 4 5 Piston Backwash Caution If you are using puffers or other...

Страница 15: ...pistons from rear side Now once in a while during work with the pump push some liquid through the pump washing system approx 1x per hour 5 ml 4 5 2 Automatic Backwash Connect both Washing heads in se...

Страница 16: ...nd in chapter 6 6 6 is shown the leakage sensor status WASTE SET ECP2010 1 Silicone tubing 2 m with connector Y and I 2 Connector Y with two pieces of silicone tubing 3 Connectors L into the drain cha...

Страница 17: ...el with desktop and is connected with one of two tubing connected to connector Y of part 1 This tubing should be cut from 1 m silicon tubing part 1 according to your needs Second connector L is pushed...

Страница 18: ...r as described above Difference is in using shorter tubing of part 2 placed behind injection valve holder and the longer tubing remains in front of the holder Connector Y of part 2 should be connected...

Страница 19: ...r press the safety pin see arrow on right picture and pull out Insert terminal block into connector INTERFACE it is among the pump accessories If there is no signal connected to the terminal block it...

Страница 20: ...mple using a multiple socket outlet with a switch 4 9 Basic Control by Keyboard After unit start Mode START initial screen displays unit type ECP2010 ECP2010H Then the unit turns to mode IDD pump moto...

Страница 21: ...arrows up and down to change value Press ENTER key to confirm the value press PUMP to start the pump Press PUMP again to stop the pump For fast setting of one of the valves to 100 it is possible to u...

Страница 22: ...ve switching low percentage of component and higher flowrate it may not manage to display valve switching Mark X all valves are closed Indication of leakage at the same time may be displayed an error...

Страница 23: ...this unit can be found in installation directory of Clarity C Clarity C Clarity Bin in file CswEcomECP2000 chm Doubleclick on the file opens it for reading 6 WORKING WITH MENU Menu enables setting al...

Страница 24: ...1 MPa 150 psi lower than value of high pressure limit Default value for ECP2010 ECP2010H is 0 0 MPa 0 psi If the value is set on 0 0 MPa 0 psi the control of low pressure limit is deactivated Example...

Страница 25: ...longer beep for confirmation of value changes ERRORS At error occurrence will be generated sound signal of the error Three consecutive longer beeps in case of an error and in case of a fatal error wi...

Страница 26: ...valves automatically opened according to setting of used valves see 6 2 3 2 and their concentration setting see 6 1 3 Unit enables to change this setting also manually see 6 3 5 but after repeated pu...

Страница 27: ...mit Pump learning must be started in Menu Control Start compens learning 6 2 4 2 Pressure Pulsation Limit Pressure pulsation limit can be set in range 0 1 5 0 MPa 10 730 psi Default valuve is 1 MPa 15...

Страница 28: ...o carry out the learning process under working conditions including used tubing column etc Learning process is trying to find optimal curve of pump rotation speed so that pulsation meets condition set...

Страница 29: ...PULSATION LIMIT WITHIN THE TIME DATA WERE ANNULLED Operating error Pumping stops Check the unit according to instructions in chapter 10 E45 LEARNING WAS INTERRUPTED BECAUSE OF WORSENING DATA WERE ANN...

Страница 30: ...e phase is stabilizing as well as flowrate and pressure In this phase is a sample injected into loop e Program start by turning injecting valve from position LOAD to position INJECT sample gets to col...

Страница 31: ...een where are displayed parameters and symbols stated in chapter 4 11 At the same time are displayed new items regarding the gradient program process depending on program phase or performed action Val...

Страница 32: ...nd flashes step time stops pump stops Mobile phase concentration change stops After pressing key PUMP or D again program restarts b Pressing D On display is shown change from to I total time stops and...

Страница 33: ...n by pressing key PUMP for 3 s For RUN at first press PUMP shortly in order to stop pumping changes to and then after pressing key pump for 3 s program initiates changes to I For STOP press PUMP again...

Страница 34: ...programs Default status is EMPTY 6 3 4 1 Load Program By uploading a program into unit memory is the unit prepared for initialization by INIT PROGRAM System allows to upload only one program Use arrow...

Страница 35: ...ient Program Creating Choose desired sequence number of program X and press ENTER Note We recommend to set at first menu item VALVE USED and other functions before setting TIME TABLE Note We recommend...

Страница 36: ...rate remains set from program and END STEP REPEAT sets initialization phase flowrate DISABLED program does NOT change flowrate In column FLOW in TIME TABLE is displayed Running program works with actu...

Страница 37: ...step start time of step flowrate concentration in see table above 2 Exit TIME TABLE ESC 3 Controlling alterations made enter TIME TABLE New step is enlisted on its position in time axis of step beginn...

Страница 38: ...ient Programs Choose number of modified program X S xx press ENTER to enter and work as during first setting When leaving modified program X S xx you will always be asked whether to save changes or no...

Страница 39: ...changes are not applied to running program Program concludes according to original setting By reloading the program in menu item LOAD PROGRAM the changes are applied Note We do not recommend to combi...

Страница 40: ...r first modification during step 0 is the course represented by curve ES0 After second modification during step 2 is the course represented by curve ES2 Flowrate is displayed by curve F Start times of...

Страница 41: ...t In each submenu can be set possibilities of Ethernet connection Note Before connecting the unit into corporate network always contact local network administrator and consult connecting parameters Th...

Страница 42: ...inistrator if you are in corporate network in order to ensure stability of connecting parameters in time 6 4 1 2 IP Address IP address used in mode STATIC IP Default value is 192 168 91 30 6 4 1 3 Sub...

Страница 43: ...A 8 ACOA For external input output interface IO INTERFACE are used connector blocks with screwing contact included in accessories For connecting cable to connector block loosen the nut using small fla...

Страница 44: ...put PUMP When switching input from level H to level L pumping is started motor is excited even when flow rate is set on 0 ml min When switching input from level L to level H pumping is stopped Bottom...

Страница 45: ...total operating time 6 5 2 Boards Displays information about electronic boards in the unit BN board name HW board version FW firmware version UN board identification numer 6 5 2 1 Main Board Unit mai...

Страница 46: ...reporting fatal error pumping stops and its start is blocked Reset can be done by turning the unit off and on after elimination of the fatal error If an error occurs display shows symbol E with a numb...

Страница 47: ...start signal input from injection valve START STATUS OF IO INTERFACE Item Description AIN Voltage on analog input DIN1 a DIN 2 Status of digital inputs DOUT Status of digital output switch STRT Status...

Страница 48: ...Pulsation On main screen is displayed PULS In this menu item is displayed status of pump pulsation Units for pressure are stated in upper row PUMP PULSATION STATUS Item Description PU01 Pulsation dur...

Страница 49: ...FLOW DIAGRAM Caution Items marked with are not inaccessible for users Only authorized person can enter this part of menu Caution The following operations may be done only by a qualified person Before...

Страница 50: ...f fragile material Improper manipulation may cause irreversible harm or piston fracture Disconnect the unit from power source Disconnect inlet tubing Dismount connecting capillary between working left...

Страница 51: ...the same number of turns New seals should be run in before first use Disconnect all equipment connected to the pump output Connect reduction valve or another reliable hydrodynamic resistor directly t...

Страница 52: ...impurity stuck on the ball surface or the seat results in pressure fluctuation or it is not possible to start the pump If this issue is not solved by repeated purge it is necessary to replace or clea...

Страница 53: ...everse order Tight al screws strongly and after starting the pump check all connections for any leakage In unit menu item Menu Service Parts replacement Check valves tick the valve that has been repla...

Страница 54: ...g block 6 7 2 Calibrations In these parts of menu is calibrated pressure sensor flowrate and gradient For user is available only automatical calibration of pressure sensor zero OFFSET AUTO and automat...

Страница 55: ...the volume of accurately measured volumetric flask class A according to ISO 1042 where is dropping mobile phase flowing through the unit After filling exact volume of the volumetric flask is the measu...

Страница 56: ...6 Time and volume start countdown After filling volumetric flask press ENTER 5 6 Pumping stops time and volume countdown stops Display shows VCNT volume measured by the unit during measuring ml VREF...

Страница 57: ...tem enables to partially or completely reset the system Majority of the menu items is blocked for user and is available only to a qualified person FACTORY SETTINGS FLOW CHART 6 7 3 1 Partial Reset Use...

Страница 58: ...umping It enables to reconfigure operating parameters Unit is waiting for command to start pumping Pumping PUMPING PMP Mode during pumping Other Unit has several other modes used only for special reas...

Страница 59: ...ecreases Column injection valve or other equipment connected after the pump Test if the problem persists without any equipment after the pump Then try to connect any reliable source of hydrodynamic re...

Страница 60: ...d automatical calibration FLOW AUTO see 6 7 2 2 Electronic failure Contact service center Motor works hardly loudly there isn t indicated any pressure and flow rate is low or none Clogged frit of outl...

Страница 61: ...Parameters Solvents volume E6 GRADIENT VALVE MALFUNCTION CHECK CONNECTION TO BOX Simple error Check and tighten holding screws on connector ECB 2000 or on the box E7 BOX NOT RECOGNIZED CHECK CONNECTI...

Страница 62: ...e below After the bubble passes through the system signal returns to original line Stuck bubble in the system is manifested by pressure suppression to zero even though pumping stil runs and liquid doe...

Страница 63: ...kage to piston backwash system However pressure record is ok during low flowrate 1 ml min and seals can still be used In case of confusion damage of seals Check the tightness of the pump The pump outl...

Страница 64: ...gents used in chromatography process Use dry or moistened cotton cloth for cleaning or unit surface 11 3 Cleaning Check Valves Remove the valves see 6 7 1 2 and clean them using ultrasound in distille...

Страница 65: ...ithout frit and spring pru inky ACA23200 Piston with holder piston diameter 1 8 ACA23201 Piston with holder and mounting piston diameter 1 8 ART05477 O ring ID 4 47 mm cross section 1 78 mm Kalrez PG2...

Страница 66: ...of products in the warranty period carried out by other person than that authorized by the service organization is a reason for warranty nullification The scope of the warranty and its duration is giv...

Страница 67: ...ents concentrations 0 0 100 0 Gradient accuracy AB 5 95 1 ml min 10 MPa ethanol 1 Wetted materials Stainless steel 316 sapphire ceramics KEL F PEEK seals Communication RS232 Ethernet LAN USB Display k...

Страница 68: ...ndards were applied when evaluating conformity EN 61010 1 ed 2 2011 A1 2019 idt IEC 61010 1 2010 A1 2016 COR1 2019 EN 61000 6 3 ed 2 2007 A1 2011 Cor 1 2013 idt EN 61000 6 3 2007 A1 2011 AC 2012 EN 61...

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