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pH sensor - Diagnostics

12.1.3

2-point calibration procedure of the pH sensor

Caution

Risk of injury due to the nature of the operating agents

▶

Respect the prevailing regulations on accident prevention and safety relating to the use of dangerous

fluids.

▶

Observe the information on the safety data sheet. The safety data sheets can be found at:

Cleaning solution acid:

http://sds-id.com/200111-2

Cleaning solution alkaline:

http://sds-id.com/200112-1

Flushing solution (reagent):

http://sds-id.com/200116-7

Buffer solution pH 5:

http://sds-id.com/200113-0

Buffer solution pH 7:

http://sds-id.com/200114-19

Buffer solution pH 9:

http://sds-id.com/200115-8

▶

Wear personal protective equipment when working with cleaning solutions.

▶

Dispose of waste containing chemicals produced by the system in an environmentally friendly manner.

Prerequisites:

•

Buy a Type MZ15 handheld calibration-and-cleaning tool with article number 00568805.

•

Buy a büS extension-cable. Refer to Table 7

. If needed, buy a Y junction.

Table 7: Accessories: cables and connectors

Accessories

Article number

büS extension-cable with 5-pin M12 connectors, 0.5 m

772403

büS extension-cable with 5-pin M12 connectors, 1 m

772404

büS extension-cable with 5-pin M12 connectors, 3 m

772405

büS extension-cable with 5-pin M12 connectors, 5 m

772406

Y junction

772420

•

Buy a buffer solution with pH 5, article number 806698 and a buffer solution with pH 9, article number

806700.

→

Read the Type MZ15 Operating Instructions.

→

Observe the information on the safety data sheets for the used solutions. The relevant data sheet can be

found at the address given on the bottom of the bottle.

→

For a correct use of the Type MZ15 handheld calibration-and-cleaning tool, refer to the Operating

Instructions of the Type MZ15.

→

Unlock and remove the product from the on the backplane of the system.

→

Plug the product on the Type MZ15 handheld calibration-and-cleaning tool. Refer to the Operating

Instructions of the Type MZ15

English

Type MS01

Содержание Type MS01

Страница 1: ...Operating Instructions Type MS01 pH sensor cube...

Страница 2: ...ve the right to make technical changes without notice Technische nderungen vorbehalten Sous r serve de modifications techniques B rkert SAS 2014 2020 Operating Instructions 2011 01_EU ML 00566496 Orig...

Страница 3: ...4 2 Warranty conditions 12 4 3 Information on the internet 12 5 Description 13 5 1 Product 13 5 2 Type label 14 5 3 Memory card 14 5 4 Product status indicator 15 6 Technical data 16 6 1 Conditions o...

Страница 4: ...nitor the pH value of the water sample 25 10 5 Monitor the temperature value of the water sample 26 10 6 Monitor the leakage current value of the measuring cell 27 10 7 Freeze the values that are tran...

Страница 5: ...r a unique name for the product 52 13 5 Change the transmission speed of the product 52 13 6 Address of a product connected to b S 53 13 7 Change the address of the product connected to a CANopen fiel...

Страница 6: ...3 Structure of the PDO4 pH State 63 17 Maintenance 65 17 1 Safety instructions 65 17 2 When performing a maintenance operation 65 17 3 Remove the product from the backplane of the system 65 17 4 Clean...

Страница 7: ...ce 77 19 3 6 Message Error too high reference impedance 77 19 3 7 Message Error too low leakage current 77 19 3 8 Message Error too high leakage current 78 19 3 9 Message Warning too low pH 78 19 3 10...

Страница 8: ...ssories 82 21 Packaging Transport 83 22 Storage 84 22 1 To store the product for a maximum of 10 days 84 22 2 To store the product for more than 10 days 84 22 3 After storage 84 23 Disposal of the pro...

Страница 9: ...or even death Caution Warns against a possible risk Failure to observe this warning can result in substantial or minor injuries Notice Warns against material damage Advice or important recommendation...

Страница 10: ...duct that does not comply with the instructions could present risks to people nearby installations and the environment The product is intended solely for the measurement of the pH in water within a Ty...

Страница 11: ...o observe the general technical rules during the planning and use of the product not to use this product in explosive atmospheres not to use this product in an environment incompatible with the materi...

Страница 12: ...ert sales office The addresses of our international sales offices are available on the Internet at country burkert com 4 2 Warranty conditions The condition governing the legal warranty is the conform...

Страница 13: ...905 system Bayonet lever to lock unlock the product carry out maintenance operations Unlocked position Locked position Maintenance position Push button with measured process variable Fluid connections...

Страница 14: ...the product At product start up there are two possibilities If product specific data is stored on the inserted memory card the product adopts the data At product delivery the memory card contains pro...

Страница 15: ...Product status changes are not shown Messages are neither listed nor transmitted via any connected fieldbus White 0 Diagnostics are inactive Active or enabled diagnostics Product status is shown by t...

Страница 16: ...dards and directives The product conforms to the CE directives of the Type 8905 system only when the product is plugged in the Type 8905 system 6 3 Materials the product is made of Part Material Housi...

Страница 17: ...pH 0 05 10 s ISFET 3 mol KCl Temperature measurement Measuring range Measurement sensor 0 50 C Pt1000 Class B no contact with the water sample Maintenance interval of the reference electrode 12 months...

Страница 18: ...ctromagnetic interference ultraviolet rays and when installed outdoors the effects of the climatic conditions 7 2 Mounting the product on the backplane The product is plugged in the backplane of the T...

Страница 19: ...rst commissioning of the system 1 Let the fluid flow through the system Make sure that the system is tight 2 Energize the system 3 Let the fluid flow through the system for at least 12 hours Observing...

Страница 20: ...ation must only be operated by suitably trained staff 9 2 Adjustment tools and adjustment software The adjustments can be made with the following tools a PC with the software Type 8920 B rkert Communi...

Страница 21: ...ls Symbol 1 User level Description Basic user No password is required This level is active by default and by default password protection is switched off The menu items with the symbol enable read only...

Страница 22: ...store factory values Menus of a product function Select a function to access its menus List of devices that are connected to b S Product functions Product Device view pH sensor General settings pH sen...

Страница 23: ...d 10 10 Hold refer to chpt 10 7 and 10 9 Restore factory values refer to chpt 10 10 10 1 Deactivate or activate the measurement of the impedance value of the reference electrode The parameter Referenc...

Страница 24: ...0 s then the variations of the measured values are damped 10 3 Monitor the impedance value of the reference electrode The water pH is correctly measured if the reference electrode is in contact with...

Страница 25: ...event are given in chpt 19 3 6 to 19 3 14 10 4 Monitor the pH value of the water sample Do the following procedure 1 Make sure that the login user level is Installer Refer to chpt 9 4 2 Configure and...

Страница 26: ...ake sure that the login user level is Installer Refer to chpt 9 4 2 Configure and activate the warning limits of the temperature value Go to device pH sensor MS01 function pH sensor tab Parameter Sele...

Страница 27: ...ng cell and thus to each product Upon delivery the product has a specific leakage current value Deterioration of the measuring cell causes the value of the leakage current to increase If the value of...

Страница 28: ...uct makes it possible to temporarily freeze the values that are sent by the product on the fieldbus You can choose one of the following options If you want to manually freeze the values refer to chpt...

Страница 29: ...sor tab Parameter Select Hold 1 Choose the values to be sent on the fieldbus If you want to send the last measured values do the following procedure Select Action Last values If you want to send user...

Страница 30: ...ected to b S then the connection is broken and the message b S event producer not found is displayed whether the parameter Hold is activated or not To restore the connection refer to chpt 19 1 3 3 Act...

Страница 31: ...the changes into account The next step restarts the product Select Finish to restart the product 10 8 Stop the manual freeze or the automatic freeze Make sure that the login user level is Installer Re...

Страница 32: ...sensor MS01 function pH sensor tab Parameter Select Restore factory values Select Parameter Confirm with Finish The parameters in Table 3 are set to their default values 10 10 Deactivate the monitori...

Страница 33: ...e of the electronics in C Reference impedance Measured impedance of the reference electrode in W VDS Value of the operating voltage of the measuring cell about 500 mV Offset Offset value of the operat...

Страница 34: ...the pH sensor Calibration of the pH sensor is required to measure pH values with as less deviation as possible Calibrate the product every 3 months with one of the following means Adjust by hand the...

Страница 35: ...0115 8 Wear personal protective equipment when working with cleaning solutions Dispose of waste containing chemicals produced by the system in an environmentally friendly manner Prerequisites Buy a Ty...

Страница 36: ...the Type MZ15 If necessary unscrew the termination resistance from the Type 8905 system and screw the termination resistance on the Y junction Refer to the Operating Instructions of the Type MZ15 Star...

Страница 37: ...alue of buffer solution Enter the pH value of the buffer solution Validate with Select Next Step 3 5 When the pH measurement is stable select Next Step 4 5 There are 3 possible results The calibration...

Страница 38: ...the following procedure Is the buffer solution used the correct one No Cancel the calibration procedure Do a new calibration procedure with a correct buffer solution Yes Do you accept the new offset...

Страница 39: ...Press the actuator button in order to allow air to dry the fluid system of the product 5 Remove the product from the Type MZ15 6 Insert and lock the product back on the backplane of the system 7 Remo...

Страница 40: ...ol with article number 00568805 Buy a b S extension cable Refer to Table 7 If needed buy a Y junction Table 7 Accessories cables and connectors Accessories Article number b S extension cable with 5 pi...

Страница 41: ...e sure that the login user level is at least Advanced user Refer to chpt 9 4 Go to device pH sensor MS01 function pH sensor tab Maintenance Select pH calibration 2 point The product status indicator f...

Страница 42: ...ating Instructions of the Type MZ15 Step 5 9 Screw the bottle with the second buffer solution as shown in Fig 11 To let the second buffer solution flow through the product press the actuator button of...

Страница 43: ...ranges To find which value is out of its error range refer to tab Diagnostics Slope limits and tab Diag nostics Offset limits If the slope value is out of its error range then do the following proced...

Страница 44: ...cs tab pH offset is updated pH sensor function Diag nostics tab pH slope is updated The date of the last calibration is updated See chpt 12 3 Step 9 9 select Finish The calibration is completed Plan t...

Страница 45: ...12 1 4 Connect the Type MZ15 calibration and cleaning tool to the Type 8905 system that has no Type ME21 touchscreeen Buy the USB b S interface set with article number 00772426 from B rkert See Fig 13...

Страница 46: ...he B rkert Communicator software to establish the communication between the B rkert Communicator software and the product A window opens Select b S Stick Choose the port B rkert b S Stick click on Fin...

Страница 47: ...level is Installer Refer to chpt 9 4 Select Interval in days Enter the number of days between two calibration procedures B rkert recommends to calibrate the product every 3 months Validate with The da...

Страница 48: ...sends the entered pH value and the displayed temperature value on the fieldbus Make sure that the product and the system behave depending on the pH value and the temperature value that are both displa...

Страница 49: ...he offset value of the temperature is set to its factory value 12 7 Restore the offset value and the slope value of the pH sensor calibration curve to their factory values Make sure that the login use...

Страница 50: ...g chapters b S refer to chpt 13 1 13 2 13 3 13 4 13 5 13 6 13 7 13 8 13 9 and 13 10 Diagnostics refer to chpt 13 11 PDO configuration refer to chpt 13 12 and 13 13 13 1 Enter a name for the product Th...

Страница 51: ...procedure Make sure that the login user level is Installer Refer to chpt 9 4 Go to device pH sensor MS01 function General settings tab Parameter Select b S Location and enter a location Validate with...

Страница 52: ...chpt 9 4 Go to device pH sensor MS01 function General settings tab Parameter Select b S Advanced Unique device name and enter the name max 19 characters Save the name with The unique name is set Resta...

Страница 53: ...unt 13 8 Set the digital communication for b S or for a CANopen fieldbus By default the operating mode of the digital communication is set to b S and the measured process data PDOs process data object...

Страница 54: ...roduct to take the operating mode of digital communication into account The PDOs are no more sent to the connected fieldbus 13 10 Change the time to check the presence of a participant on the fieldbus...

Страница 55: ...At least one of the monitored parameters is outside its monitored limits Blue 2 Maintenance required The product is in controlled oper ation however the function is briefly restricted Do the required...

Страница 56: ...rom other participants to the fieldbus For more information about the structure of the PDO refer to chpt 16 3 The transmission time between 2 values of a PDO is described by the 2 following parameters...

Страница 57: ...t the transmission time between 2 values of the PDO do the following procedure Make sure that the login user level is Installer Refer to chpt 9 4 Go to device pH sensor MS01 function General settings...

Страница 58: ...d 14 9 Logbook refer to chpt 14 10 14 1 Read the number of product starts Go to device pH sensor MS01 function General settings tab Diagnostics Select Device status The parameter Device boot counter i...

Страница 59: ...MS01 function General settings tab Diagnostics Select b S status Read the value of the parameter Receive errors max 14 6 Read the number of current transmit errors Make sure that the login user level...

Страница 60: ...n b S or on the CANopen fieldbus and the message b S is not operational is generated in the message list Refer to chpt 19 1 4 14 10 Read the generated events 2 types of events can be generated events...

Страница 61: ...ive Event happens during the start of the product Time at which the event was checked Time at which the event occurred Symbol related to the event status Refer to Table 15 Fig 20 Overview of events in...

Страница 62: ...version EDS version number Device driver Driver version Version number of the product driver Driver ident number Article number of the product driver Firmware group Product name and EDS version numbe...

Страница 63: ...electrode 0x2504 REAL32 W 0 1 MW 1000 Leakage current of the measuring cell sensor ISFET 0x2505 REAL32 A 1 0 E 8 PDO3 Temperature of the water sample 0x2502 REAL32 K 233 398 K 0 05 PDO4 pH State 0x25...

Страница 64: ...2 3 Reserved 4 High error limits of the monitored values 0 limits not exceeded 1 one of the limits is exceeded Refer to chpt 19 3 5 Low error limits of the monitored values 0 monitored values are abov...

Страница 65: ...nt of the reference electrode or after replacement of the pH measuring cell let the system operate for a time of 12 hours and calibrate the product if necessary Calibrate the product every 3 months 17...

Страница 66: ...ble Refer to Table 21 If needed buy a Y junction Table 21 Accessories cables and connectors Accessories Article number b S extension cable with 5 pin M12 connectors 0 5 m 772403 b S extension cable wi...

Страница 67: ...e correctly Press the actuator button of the Type MZ15 in order to allow the cleaning solution to flow through the fluid system of the product The pump will operate as long as the button is pressed Ad...

Страница 68: ...ing to the degree of contamination Refer to Table 26 Table 26 Recommended flushing durations according to degree of contamination Degree of contamination Flushing duration s Light contamination 10 Ave...

Страница 69: ...e 2 Remove the reference electrode from the product Lift the folding lever of the reference electrode and turn it by a quarter turn to the left Folding lever Fig 24 Extraction of the reference electro...

Страница 70: ...ions Type MS01 MS02 MS04 The Service Instructions is available at country burkert com 17 7 Replace a defect product by a new one You can only replace a product by a product with the same article numbe...

Страница 71: ...owing means Measure the water pH value with an external pH meter If the pH values measured by the product have been recorded with the internal or an external data acquisition system then analyze the r...

Страница 72: ...cell Parameter Description Range VDS Value of the ISFET operating voltage 480 mV value 520 mV I drain Value of the ISFET drain current 80 A value 120 A I source Value of the ISFET source current 80 A...

Страница 73: ...mperature value with an external instrument If the temperature values that are measured by the product are wrong restart the product If the color of the product status indicator changes to red go to c...

Страница 74: ...age displayed on your product is not explained in the Operating Instructions contact B rkert 19 1 1 Message Error 2 memory Product status symbol Bit status of the PDO pH state bit 0 1 Possible cause P...

Страница 75: ...sages function check If the message displayed on your product is not explained in the Operating Instructions contact B rkert 19 2 1 Message Simulation mode active Product status symbol Bit status of t...

Страница 76: ...t The message can only be displayed if the monitoring of the pH value has been configured and activated Refer to chpt 10 4 What to do Check the process 19 3 3 Message Error too low temperature Product...

Страница 77: ...eference electrode is above the set limit The message can only be displayed if the monitoring of the impedance value has been configured and activated Refer to chpt 10 3 What to do Replace the referen...

Страница 78: ...water sample is is under the set limit The message can only be displayed if the monitoring of the pH value has been configured and activated Refer to chpt 10 4 What to do Check the process 19 3 10 Mes...

Страница 79: ...value has been configured and activated Refer to chpt 10 3 What to do As the monitoring of the low limit is not important make sure that the parameter Warning triggers Activation flags Low ref impedan...

Страница 80: ...tion flags Low ISFET leak current is not selected 19 3 16 Message Warning too high leakage current Product status symbol Bit status of the PDO pH state bit 6 1 Possible cause The leakage current of th...

Страница 81: ...le at country burkert com 19 4 2 Message Calibration date has expired Product status symbol Bit status of the PDO pH state bit 1 1 Possible cause The calibration date is due What to do Calibrate the p...

Страница 82: ...t includes the following items 1 pH measuring cell 1 black seal 1 rubber elastomer 568038 Memory card On request Table 29 Accessories cables and connectors Accessories Article number b S extension cab...

Страница 83: ...l 806709 Flushing solution 250 ml 806710 Table 34 Accessories storage solution Accessories Article number Storage solution pH electrode 500 ml 418557 21 Packaging Transport Before any packaging or tra...

Страница 84: ...ater 2 Purge the product with air at a max pressure of 2 bar 3 Remove the reference electrode To protect the capillary tube put a few drops of a 3 mol KCl solution or another storage solution in the p...

Страница 85: ...pose of the product and its packaging in an environmentally friendly way Notice Damage to the environment caused by products contaminated by fluids Comply with the national and or local regulations wh...

Страница 86: ...86 English Type MS01...

Страница 87: ......

Страница 88: ...www burkert com...

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