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5  Putting into operation

57

NIRFlex N-500

 Operation Manual, Version G

Internal and External Reference measurements provided by the measuring cells/add-ons

Measuring cell / Add-on

Internal reference

External Reference

NIRFlex Solids with Spinner add-on

-

manually

NIRFlex Solids Transmittance

-

built-in

NIRFlex Fiber Optic Solids

x

manually

NIRFlex Fiber Optic Liquids

x

manually

NIRFlex Liquids

-

built-in

NIRFlex Fiber Optic SMA  
(+ individual accessories)

x

manually

without internal reference:

Spectrum 

=

sample

ext. reference

with internal reference:

Spectrum 

=

sample (recent) / int. reference (recent)

ext. reference (old) / int. reference (old)

For more information on the reference measurements, see also section 6.

Содержание N-500 NIRFlex

Страница 1: ...N 500 NIRFlex Operation Manual 093020G en...

Страница 2: ...e right to make changes to the manual as deemed necessary in the light of experience espe cially in respect to structure illustrations and technical detail This manual is copyright Information from it...

Страница 3: ...3 1 NIRFlex Solids 14 3 3 2 NIRFlex Solids Transmittance 14 3 3 3 NIRFlex Liquids 15 3 4 Fiber optic measuring cells and accessories 16 3 4 1 NIRFlex Fiber Optic Solids 16 3 4 2 NIRFlex Fiber Optic L...

Страница 4: ...4 2 Network integration 48 5 5 Installing the measuring cells 49 5 6 Installing the cover of the NIRFlex Solids Transmittance 50 5 7 Preparing the transflectance adapter 51 5 7 1 Adjusting the pathlen...

Страница 5: ...7 8 NIRFlex Solids 78 7 9 NIRFlex Liquids 78 7 10 Customer service 79 8 Storage transport and disposal 80 8 1 Storage and transport 80 8 2 Disposal 80 9 Spare parts and accessories 82 9 1 Scope of del...

Страница 6: ...distributed or used for competi tive purposes nor made available to third parties The manufacture of any component with the aid of this manual without prior written agreement is also prohibited The E...

Страница 7: ...it no trace analysis Thanks to its ruggedness the instrument is suitable for use on most production floors at line near line For suitable environmental conditions see tables of technical data The NIRF...

Страница 8: ...ion which if not avoided could result in death or serious injury CAUTION Indicates a hazardous situation which if not avoided may result in minor or moderate injury no NOTICE Indicates possible proper...

Страница 9: ...protective goggles Wear protective gloves Do not dispose as unsorted household waste Additional user information Paragraphs starting with NOTE transport helpful information for working with the devic...

Страница 10: ...ed counter measures in order to achieve and maintain the lowest possible level of hazard NOTE The instrument contains a laser for wavenumber calibration When closed the instrument is consi dered a Cla...

Страница 11: ...using and assemblies The following warning sticker s can be found on the housing or assemblies of the NIRFlex N 500 Symbol Meaning Location Hot item hot surface Inside housing next to lamp modules LAS...

Страница 12: ...f any safety related incidents which might occur during operation of the instrument or its accessories Legal regulations such as local state and federal laws applying to the instrument or its accessor...

Страница 13: ...7 at 35 C max 2500 m for indoor use only Ambient temperature 5 35 C 25 5 C recommended Pollution degree 2 Installation category II Spectral range 800 2500 nm default 1000 2500 nm 12 500 4 000 cm 1 def...

Страница 14: ...alibrations 3 3 Non fiber optic measuring cells 3 3 1 NIRFlex Solids Technical data NIRFlex Solids Detector extended range InGaAs temperature controlled Electric power supply 100 230 VAC 10 50 60 Hz 2...

Страница 15: ...64 scans Blackman apodization 3 3 3 NIRFlex Liquids Technical data NIRFlex Liquids Detector extended range InGaAs temperature controlled Electric power supply provided from NIRFlex N 500 100 230 VAC...

Страница 16: ...er Fiber Optic Solids Max operating temperature 120 C Material Transflectance sleeve material Steel no 1 4435 Spacer ring material Steel no 1 4305 Transflectance adapter window Quartz glass Infrasil 3...

Страница 17: ...power supply 100 230 VAC 10 50 60 Hz 20 W Ambient conditions 80 relative humidity for T 31 C linear decreasing to 67 at 35 C max 2500 m for indoor use only Ambient temperature 5 35 C 25 5 C recommend...

Страница 18: ...ce giving high wavenumber stability and good data transferability Single beam interferometer without typical double beam divergence for mechanically and tempera ture stable beam alignment More robust...

Страница 19: ...ing amplitude This alternating amplitude is detected via the the Laser sensor e giving precise information about velocity and relative position of the wedge The feedback signal is used to control the...

Страница 20: ...erent measuring cell modules for different kinds of sample materials can be easily attached to the basic intrument To choose the best measuring cell for a specific range of samples the optical proper...

Страница 21: ...that can influence the measurement Not enough sample material available Air bubbles in the measurement path and under the transflectance cover Sample not homogeneous or representative Temperature of...

Страница 22: ...tion The NIR light penetration is limited by the sample material It interacts with the sample is refracted and diffusely reflected into the sensor The reflected rays contain the spectral information o...

Страница 23: ...information This is the preferred method for testing liquids Detector Cuvette NIR light pathlength 4 2 4 Diffuse transmission mode The diffuse transmission mode is a mixture of diffuse reflection and...

Страница 24: ...h serial number e Ethernet connection f Interfaces for service intervals USB 1 USB 2 KBD MS VGA COM g Ventilation filter 4 3 1 Lamp unit The lamp unit comprises two lamp modules A primary lamp module...

Страница 25: ...rmal measurements Five different grey standards to check the linearity The software is designed for the automatic use of the standard wheel i e the operator does not have to start one of the above men...

Страница 26: ...ools x x Security Designer x x Library Designer x Regulatory Kit x Each package includes the following program elements by default Operator interface to run routine analysis Administrative tools Repor...

Страница 27: ...rol System Service controls the complete system It runs in the background as a service Normally there is no user interaction necessary 4 5 2 NIRWare software suite The PC is running the NIRWare Softwa...

Страница 28: ...he light is then detected in the measuring cell and the data is sent to the basic instrument The measuring cell has its own power supply and is galvanically isolated from the basic instrument It can b...

Страница 29: ...small plastic bags x Internal reference x x x External Reference x x x x x Sample dimensions Spinner 34 mm Petri dish 100 mm Glass vials 10 15 mm Tablets 5 10 mm 0 3 ml The NIRFlex Solids is the ideal...

Страница 30: ...the NIRFlex Solids 4 6 3 Petri dish add on for NIRFlex Solids NIRFlex Solids with petri dish add on The NIRFlex Solids with the petri dish add on is the ideal configuration to measure solid samples i...

Страница 31: ...of the reference and afterwards the mea surement of the sample positions 1 6 which have been pre defined in the NIRWare Operator The actually measured spectrum is set against the last measured referen...

Страница 32: ...rotate during the measurement To carry out the reference measurement the user has to place the External Reference see also section 5 10 onto the sample window 4 6 7 XL add on with iris aperture for NI...

Страница 33: ...r reference measurement remove the B L cup first Place the centering ring and the External Refe rence onto the XL add on and perform the measurement XL add on for B L sample cups 4 6 9 External Refere...

Страница 34: ...i e Hellma cuvette or glass vials with a diameter of 34 mm can be used as sample vessel in the motor driven Spinner For reference measurement the Spinner can hold the External Reference 4 6 11 Flow c...

Страница 35: ...el claim Traditionally these analyses are made using HPLC determining only the active content which is time consuming and very costly The speed efficiency and cost situation can be very much improved...

Страница 36: ...osage forms like tablets or capsules a b a Detector b Sample position Sensor position and beam path 4 6 13 Sample plates for the NIRFlex Solids Transmittance The autosampler accepts up to thirty sampl...

Страница 37: ...iquids NIRFlex Liquids The NIRFlex Liquids is the ideal configuration to measure liquids like solvents oils etc in transmission mode using glass cuvettes The NIRFlex Liquids enables quantitative and q...

Страница 38: ...1 4 6 5 15 14 13 7 8 9 10 11 12 a STOP button b START button c Status LED d Detector e Optic 2 f Ventilation g Heating h Motor i Optic 1 j Mirror k Aperture l Light barrier m Magnetic coding n Magnet...

Страница 39: ...ing the results using LEDs on the handle The LEDs at the handle of the fiber optic probe indicate the status of the system and the results of the prediction in routine operation Applications without c...

Страница 40: ...START button d Handle e Fiber bundle f Electrical connections probe g Light barrier h Holder for fiber optic i Internal reference j Optic 3 k Detector l Motor m Optic 1 n Optic 2 o Directly reflected...

Страница 41: ...is suitable for the analysis of viscous non agressive liquids Thanks to the reproducible adjustable pathlength it is suitable both for the meausurement of slightly and of strongly absorbing samples T...

Страница 42: ...uring red LED on green LED on message on monitor green LED on result conforms red LED on result does not conform Because the fiber optic probe is used at a certain distance from the spectrometer the l...

Страница 43: ...two SMA connectors Laboratory and immersion process probes in transmission or diffuse reflection mode as well as flow through cells can be attached NIRFlex Fiber Optic SMA NOTE Glas fibers have to be...

Страница 44: ...E Inspect the instrument package for damage immediately after delivery If necessary prepare a status report immediately and inform customer and your local Buchi representative Keep the original packag...

Страница 45: ...ING movement b Output window of the interferometer c UNLOCKING movement The installation position of the shield depends on the locking status of the transportation lock The label of the shield in this...

Страница 46: ...tize at relocation The electric plug on the measuring cell is only designed to plug in the measuring cells Do not connect any other item The spectrometer must be placed onto a clean level and stable s...

Страница 47: ...the supplied Ethernet cable Connect the mains cable to the socket Switch on the NIRFlex N 500 via the main switch on the rear of the instrument Start the PC and install the NIRWare software Set up the...

Страница 48: ...e NIRFlex N 500 can be installed and used In the following two examples are given All data on one PC via direct link The PC with the NIRWare database is directly connected to the NIRFlex N 500 All dat...

Страница 49: ...catches Make sure it is seated well by means of the centerning pins at the NIRFlex N 500 Subsequently fasten the measuring cell with the fixating screw at the bottom of the NIRFlex N 500 NOTE When usi...

Страница 50: ...er back into a straight position b c Keep the right hinge of the cover in a matching position with the bushing screw Fasten the screw c with a few turns the screwdriver is part of the scope of deliver...

Страница 51: ...er with a new instrument When you receive your transflectance adpater together with a new NIRFlex N 500 instrument the pathlength has already been adjusted to the probe head by the manufacturer When y...

Страница 52: ...dapter window a Slide the transflectance adapter over the probe head and orient it so that the pin at the probe head is pushed into the groove of the spacer ring Push the transflectance sleeve upwards...

Страница 53: ...o additional adjustment is necessary when you change from one spacer ring to another 5 7 2 Exchanging the spacer ring To exchange the spacer ring in order to work with another pathlength proceed as fo...

Страница 54: ...tor and secure the end of the connector with the threadened spacer nut NOTE The spring must be freely movable after installation Fasten the spacer nut handtight only Insert the optical fiber cable Pla...

Страница 55: ...e and quality control NOTE The time between two SST requests can be set with the NIRWare Application Designer The recom mended standard value between two tests is 24 hours a test run takes approximate...

Страница 56: ...ic dynamic range 5 10 Reference measurements Frequent reference measurements compensate for environmental effects which might influence the spectra Each measuring cell offers a possibility for the ref...

Страница 57: ...dd on manually NIRFlex Solids Transmittance built in NIRFlex Fiber Optic Solids x manually NIRFlex Fiber Optic Liquids x manually NIRFlex Liquids built in NIRFlex Fiber Optic SMA individual accessorie...

Страница 58: ...tative calibration 16 32 granules 64 The spectral range of the NIRFlex Solids Transmittance is limited to 6000 cm 1 The number of scans should be 64 by default General recommendations for measuring so...

Страница 59: ...t liquids Clean probe head Max temperature 150 C avoid air bubbles NIRFlex Solids with petri dish add on and transflectance cover Clear liquids turbid liquids Empty petri dish with transflectance cove...

Страница 60: ...hen an add on or a new measuring cell is selected or every time the software is restarted To measure the External Reference proceed as follows Remove any sample from the add on and ensure that the sam...

Страница 61: ...t reflection and light leakage All sample plates include an External Reference position By default reference measurements are performed automatically before every measurement sequence NOTICE Risk of d...

Страница 62: ...to use 1 5 and 10 mm cuvettes as well If doing so the spacers which fix the cuvettes in the measurement position must be changed A set of different spacers is included in the scope of delivery For qu...

Страница 63: ...IRFlex Fiber Optic Solids The handle is equipped with a remote control for initiating the measurements remotely and displaying the results using LEDs on the handle Because the fiber optic probe is use...

Страница 64: ...ersions with other pathlengths are available For sample measurements with the NIRFlex Fiber Optic Liquids make sure that the quartz window in the probe head is in full contact with the sample to be an...

Страница 65: ...e operator is advised to attend common laboratory biosafety measures in accordance the chosen application and environ ment The Laboratory Biosafety Manual of the World Health Organization can be used...

Страница 66: ...between the measurements clean the surfaces in direct contact with the sample after each measurement For this purpose use abrasion resistant precision cloths such as Kimwipes from Kimberly Clark Loose...

Страница 67: ...vaporates completely For this purpose you can place the External Reference in an oven for a few minutes at a maximum of 60 C The reference material adsorbs oils and fats 7 2 3 Cleaning of the Transfle...

Страница 68: ...he SST NIRWare 1 x includes the NIRWare Automatic Diagnose NADIA NADIA is a tool which enables Buchi service personnel to judge the condition of the NIRFlex N 500 or to do a performance check of the i...

Страница 69: ...ced quickly after failure This action can be performed by a trained operator After failure of the primary lamp module the following instructive message appears NOTE When the primary lamp is broken the...

Страница 70: ...he housing towards the rear side of the instrument There is a built in sensor to record the opening of the housing A safety tack ensures that the lamp remains in the correct position Slide the safety...

Страница 71: ...dule exchange the following message appears at power on Message concerning required instrument setup Click the OK icon to confirm the message Now click the Service icon Operator and double click Assem...

Страница 72: ...he standard working conditions of the NIRFlex N 500 a b c Start the Operator software Switch from secondary lamp a to primary lamp Resetting the hour b counter will bring up a prompt for confirmation...

Страница 73: ...at laser power supply NOTICE Risk of optical misalignment and damage at the LASER module Do not touch the optical surfaces of the module Handle the module with care i e do not expose the module to hea...

Страница 74: ...it with the two screws and connect the electric plug Close the housing of the laser unit This can easily be done by first positioning the slits over the screws When the instrument and the PC is switch...

Страница 75: ...t setup Click the OK icon to confirm the message Now click the Service icon Operator The following dialog opens Assembly setup dialog Click the icon next to the Laser Module row The following dialog a...

Страница 76: ...pad after 6 month of use at the latest An earlier exchange might be necessary when the instrument is operated in a dusty environment To replace the ventilation filter proceed as follows Remove the fi...

Страница 77: ...50 V Reconnect the power supply connector and switch on the instrument Replacing the primary fuses 7 7 1 Measuring cell fuse replacement Each measuring cell is provided with two fuses located at the b...

Страница 78: ...remove them with a soft tissue and clean the sample holder with a non aggressive liquid water or alcohol Special attention is needed to prevent the glass window from getting any scratches by using opt...

Страница 79: ...e technical training and knowledge of possible dangers which might arise from the instrument Addresses of official Buchi customer service offices are given on the Buchi website under www buchi com If...

Страница 80: ...TE Because of its weight it is recommended to carry the instrument with two persons Clean the instrument thoroughly before storage or transport When returning the instrument to BUCHI fill out a copy o...

Страница 81: ...ed in the laboratory and is new was not in contact with toxic corrosive biologically active explosive radioactive or other dangerous matters is free of contamination The solvents or residues of pumped...

Страница 82: ...arts Use only genuine consumables and genuine spare parts for maintenance and repair to assure good system performance and reliability Any modifications to the spare parts used is allowed only with th...

Страница 83: ...dd on accepting B L sample cups N510 006 Spinner add on N510 012 Flow cell adapter add on N510 013 NIRFlex Solids Transmittance Product Order number For measurements in diffuse transmission mode with...

Страница 84: ...om made lengths up to 7 m available N513 000 NIRFlex Fiber Optic SMA Product Order number For measurements in transmission or diffuse reflection mode External optical probes or and measuring cells can...

Страница 85: ...019 French 93021 Italian 93022 Spanish 93023 Quick Guide NIRWare 1 2 en 93124 NIRWare Quick Guide English 93124 German 93125 French 93126 Italian 93127 Quick Guide NIRWare 1 4 English 11593434 German...

Страница 86: ...acer for 5 mm cuvettes 1 spacer for 2 mm cuvettes 1 spacer for 1 mm cuvettes Set of spacers 6 pieces of each 45430 45431 45432 N560 013 Set of 100 glass vials to be used with NIRFlex Solids with the v...

Страница 87: ...d on for NIRFlex Solids accepting B L cups N510 006 High performance sample cup for NIRFlex Solids 46259 Exchange glass bottom 46246 a b b b c d e f Transflectance adapter for NIRFlex Fiber Optic Soli...

Страница 88: ...Product Order number Holder for fiber optic probe 46273 Barcode reader 42762 Special Vials set of 6 11056492 Unbreakable Sample Cup for NIRFlex Solids 11055058 Transflectance cover for Unbreakable Cup...

Страница 89: ...add on 11055051 Flow Through cuvettes 11055911 9 2 NIRFlex spectrometer Spare parts NIRFlex spectrometer Product Order number Primary lamp module N560 001 Laser unit N560 002 Fuse T 10 A slow blow L 2...

Страница 90: ...mm 41583 Set of 100 glass vials for vial add on N560 015 10 filter pads 42778 XL add on with iris aperture N510 005 XL add on accepting B L sample cup N510 006 High performance sample cup 046259 Exch...

Страница 91: ...se 2 0 AT 02998 Cuvette holder complete N560 010 Set of 2 quartz glass cuvettes 2 mm 46266 1 spacer for 5 mm cuvettes 45430 1 spacer for 2 mm cuvettes 45431 1 spacer for 1 mm cuvettes 45432 10 filter...

Страница 92: ...e parts Fiber Optic Solids Product Order number Fuse 2 0 AT 02998 10 filter pads 42778 Packing parts SMA 11056060 9 9 Transflectance adapter Spare parts transflectance adatper Product Order number Spa...

Страница 93: ...to cause harmful interference in which case the user will be required to correct the interference at his own expense Fran ais Cet appareil a t test et s est av r conforme aux limites pr vues pour les...

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Страница 96: ...w buchi com cn India BUCHI India Private Ltd IN Mumbai 400 055 T 91 22 667 75400 F 91 22 667 18986 india buchi com www buchi in Indonesia PT BUCHI Indonesia ID Tangerang 15321 T 62 21 537 62 16 F 62 2...

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