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Operation

SPECTROLAB — 23.07.2020

— 25

6

Operation

6.1

Overview of controls

Fig. 6

No. Control element

Function

1

Switch

Start/Stop measurement

2

Switch

Switches the plasma generator on/off, see chapter 6.2.

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Содержание 76004143

Страница 1: ...kann nicht angezeigt werden M glicherweise wurde die Datei verschoben umbenannt oder gel scht Stellen Sie sicher dass die Verkn pfung auf die korrekt SPECTROLAB Stationary metal analyzer Original ope...

Страница 2: ......

Страница 3: ...2 Preparing the Sample 14 2 3 3 Sample material 15 2 3 4 Sample weight 15 2 3 5 Gas cleaning cartridge 16 2 3 6 Spark stand 16 2 3 7 Sample clamp 16 2 3 8 Gas supply 17 2 4 Prohibited operating condi...

Страница 4: ...edule 33 7 3 Cleaning the UV optics light inlet window 34 7 4 Cleaning the spark stand 37 7 5 Cleaning the exhaust filter system and changing the filter insert 42 7 6 Inspecting the gas washing bottle...

Страница 5: ...vaporated by spark discharge inside the unit In this process the released atoms and ions are excited and emit light This light is directed into the optical systems and measured using sensors Calibrati...

Страница 6: ...side Fig 1 No Component No Component 1 Filter mat spark excitation plasma generator 5 Sample clamp 2 Unlocking mechanism for protective cover 6 Start Stop measurement 3 Filter mat for cooling system...

Страница 7: ...e Fig 2 No Component No Component 1 Sample clamp 5 Door opener 2 Start Stop measurement 6 Access to the setting gage electrode Allen key wash bottle and filter bottle inside the instrument 3 On Off sw...

Страница 8: ...inside Fig 3 No Component No Component 1 Gas washing bottle 5 ICAL sample s 2 Gas cleaning cartridge Notice Only qualified personnel shall be permitted to change the cartridge 6 Setting gage electrod...

Страница 9: ...Description of instrument SPECTROLAB 23 07 2020 9 1 3 4 Instrument back Fig 4 No Component No Component 1 Argon connection 3 Mains connection socket 2 PC data transmission connection...

Страница 10: ...ss to electrode clamp 7 Locking wheel for contact 2 Sparky stand plate 8 Electrode and spark stand insert 3 Clamp swinging 9 Outlet to filter system 4 Contact movable 10 Electrode holder 5 Start Stop...

Страница 11: ...used The following symbols are used in these abbreviated operating instructions and or on the instrument If required additional important information is available in connection with these symbols Gen...

Страница 12: ...ed Only service personnel authorized by the manufacturer are permitted to unpack install set up and connect the instrument The instrument must only be connected to the mains power supply with a protec...

Страница 13: ...ional regulation Compliance with the maintenance schedule specified by the manufacturer and the recording of all maintenance activities is mandatory This helps maintain the operational safety of the i...

Страница 14: ...the sample material When disposing of these dusts compliance with legal regulations and fire prevention instructions is mandatory The operating company of the spectrometer shall be responsible for com...

Страница 15: ...with legal regulations and fire prevention instructions is mandatory If the samples contain toxic substances an extraction system must be installed at the spark stand In this case the gas escaping fro...

Страница 16: ...kin For samples that do not completely cover the spark stand opening use the respective sample adapters in such a way that the opening is completely closed Take appropriate protective measures e g wea...

Страница 17: ...on is required for a nitrogen oxygen analysis The spectrometer requires an argon supply line A suitable pressure reducer is required for the argon supply bottles or liquid gas tank Adjustable output p...

Страница 18: ...e cooling system contains a coolant The associated material safety data sheet is available at http MSDS spectro com Warning High voltage When the instrument is switched on there is a risk of an electr...

Страница 19: ...ealthy person this electrical transmission is of no concern These are electromagnetic fields of low intensity Due to this transmission the electromagnetic characteristics of the instrument may be outs...

Страница 20: ...altitude of 2000 m above sea level vibration free not subject to impact or vibration load conditions Air humidity range 20 80 not condensing Sound pressure level 55 dB A Argon inlet pressure on the i...

Страница 21: ...ns and shocks measurement errors may occur during the measuring process The instrument must be installed at a vibration and shock free location Measurement errors can result from temperature differenc...

Страница 22: ...Transportation Setting up 22 SPECTROLAB 23 07 2020 4 1 Space requirements 4 2 Storage Storage conditions The instrument must be stored in a dry place Room temperature 15 C 45 C 5 F 113 F...

Страница 23: ...able output pressure 0 10 bar The argon inlet pressure at the instrument is 4 8 5 bar 69 6 72 5 psi The pressure reducer must be adjusted so that the maximum permissible inlet pressure of the instrume...

Страница 24: ...198 253 VAC 50 60 Hz 2 Check if the mains voltage selector switch of the PC is set to the proper input voltage 230V 115V 3 Check the filling level of the gas washing bottle Fill with water if require...

Страница 25: ...Operation SPECTROLAB 23 07 2020 25 6 Operation 6 1 Overview of controls Fig 6 No Control element Function 1 Switch Start Stop measurement 2 Switch Switches the plasma generator on off see chapter 6 2...

Страница 26: ...onnect the instrument to the power supply 2 In order to switch on the plasma generator press the following buttons 3 Switch on the computer The operating system is booted 4 After booting the operating...

Страница 27: ...It is recommended to leave the instrument connected to the power supply and to leave the argon supply line open all the time To switch off the instrument proceed as follows 1 Exit the spectrometer pro...

Страница 28: ...Warning Hot surface A sample can get hot if it is measured several times Touch the sample only after it has sufficiently cooled Warning Optical radiation The plasma in the spark stand generates UV ra...

Страница 29: ...standardized optional see page 30 and the correct and base relevant parts have been installed see page 30 2 Check the spark stand and the sample for any moisture It is important that no moisture is v...

Страница 30: ...ns on the screen and perform the necessary measurements with the profiling samples Use the Finish button or press the respective function key to finish the respective sample After calculation of the s...

Страница 31: ...ction key F10 2 Put the sample in position The sample must fully cover the opening in the spark stand plate The sample clamp must have contact with the sample the safety device is activated 3 Use the...

Страница 32: ...Maintenance Reminder The instrument is equipped with a diagnostic system that will prompt you to proceed with a variety of maintenance tasks The intervals between the individual maintenance tasks are...

Страница 33: ...rks clean the bottom of the insert around the electrode A brush of the same type as that used for electrode cleaning can be used To avoid contamination of the electrode tip this brush should not be us...

Страница 34: ...the spark stand Warning Toxic substances When removing the light entry window contact with the condensate of the samples is likely Depending on the sample material the condensate may be toxic Protecti...

Страница 35: ...holder 2 from the spark stand 7 Loosen the window holder 3 from the spark stand The quartz window is located between the holder and the O ring Direct contact with the optical surfaces must be avoided...

Страница 36: ...channel 5 with a grease free cloth or a bottle brush with plastic bristles Fig 12 9 If necessary use a grease free cloth to clean the O ring 6 Fig 13 10 Reassemble components in reverse order Cleanin...

Страница 37: ...creases the risk of burn injuries During normal operation the electrode will heat up to several hundred degrees Never touch the electrode with your bare hands even after shutting down the spectrometer...

Страница 38: ...onnection between the electrode and the metal structure of the spark stand wall To clean the spark stand proceed as follows 1 Turn off the Plasma generator 1 2 Unscrew the 4 fasteners 2 and remove the...

Страница 39: ...ng the Allen key AF 2 5 until the electrode can be removed When loosening the electrode hold firmly on to it After loosening the screw a spring presses the screw upward Loosen the screw only until the...

Страница 40: ...ce of the spark stand body 11 Use a dry grease free cloth or a bottle brush with plastic bristles to clean the light channel 2 Fig 19 12 Install the spark stand insert The spark stand insert is center...

Страница 41: ...e the setting gage 1 in order to align the electrode Press the setting gage with the 3 4 mm shoulder into the spark stand opening and at the same time use the Allen key 2 AF 2 5 to screw the electrode...

Страница 42: ...e been sparked off wearing a breathing mask to prevent the inhalation of condensate particles is mandatory When disposing of the condensate and the used filters compliance with legal regulations is ma...

Страница 43: ...ring 1 is clean and sits inside the groove If necessary use a clean cloth to clean the O ring The filter container should only be tightened by hand The filter bottle screws in easily If not the filter...

Страница 44: ...7 2020 Pull the nozzle 2 out of the water hose Use a cloth to clean the nozzle and replace it Screw the water bottle back into the holder The water bottle should only be tightened by hand Fig 30 The e...

Страница 45: ...pplies when replacing the filter insert When disposing of the condensate and the used filters compliance with legal regulations is mandatory In order to inspect the gas washing bottle proceed as follo...

Страница 46: ...AB 23 07 2020 5 Make sure that the O ring 1 sits in the groove and is clean If necessary use a clean cloth to clean the O ring 6 Screw the gas washing bottle back manually Fig 34 Checking changing the...

Страница 47: ...1 electronics room 2 and plasma generator spark stand 3 The filter mats for these openings are all of the same size whereby two filter mats are required for opening 1 Fig 35 1 Press down onto the upp...

Страница 48: ...ew samples must be matched to those of the old samples Please contact your Service Center Information Do not discard the old ICALization sample before the intensities have been matched Matching is not...

Страница 49: ...ument is ready for measurement if all specifications according to chapter 6 4 1 on page 29 have been met Temperature of the optical system Is shown in red as soon as the optimum temperature of the opt...

Страница 50: ...he argon outlet Insufficient argon supply Check argon supply and pressure Poor argon quality Connect new argon specifications chapter 3 Technical data on page 20 Incorrect electrode gap Clean the elec...

Страница 51: ...e dropped below the minimum limit of the matrix depending reference channel e g Fe 273 nm Insufficient intensity 1 Check argon 2 Clean spark stand adjust electrode 3 Clean light inlet window 4 Profile...

Страница 52: ...e safety circuit has not been activated within the last 5 minutes Acknowledge the message Move the clamp up for approx 1 second An error has occurred whilst attempting to access the spectrometer Plasm...

Страница 53: ...us of the instrument To open the diagnostic system click the green or red LED symbol in the lower right hand corner of the status bar Fig 38 When the instrument is ready for operation the green LED sy...

Страница 54: ...Parts Catalogue on our website at www spectro com 11 De commissioning Only organizations or persons authorized by the instrument manufacturer shall be permitted to de commission the instrument Please...

Страница 55: ...EC Declaration of Conformity SPECTROLAB 23 07 2020 55 13 EC Declaration of Conformity...

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