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Park XE-70 AFM User Manual 

Ed Fei and Ryan Brock 

Updated 10/30/13

 

 

NOTE: 

This document is intended as a quick reference for basic operation of the 

Park XE-70 and is by no means a comprehensive manual.  It is strongly suggested 
that users look through the Park documentation.  The better you understand the 
instrument, the more effectively you will be able to use it. 

 
Basic AFM Principles 
 

When the tip is suspended in air, the laser will hit the center of the quadrant photodetector. 
If the tip encounters a feature on the surface, the tip deflects and the laser will move on the 
quadrant photodetector.  This is relayed to a motor controlling the tip which adjusts the tip’s 
vertical position until the laser is aimed in the center of the quadrant photodetector once again.  
Effectively, this keeps the tip at a constant distance from the sample surface.  By recording the 
position of the motor height, we can now know the topography of the sample surface.  
 
The tips provided in this lab are intended for ‘non-contact’ AFM, which is similar in principle to 
what is described above. Rather than relying on physical contact with the surface, the 
cantilever/tip is oscillated at a given frequency above the sample surface, and interactive forces 
from the surface lead to changes in the amplitude/phase of this oscillation.  
 
Setting up the AFM is simple: adjust the mirrors until the light path follows the diagram below 

 

 

 

Summary of Contents for XE-70

Page 1: ...is is relayed to a motor controlling the tip which adjusts the tip s vertical position until the laser is aimed in the center of the quadrant photodetector once again Effectively this keeps the tip at...

Page 2: ...and place it in the good tips box Ensure new tip is rested in place and that bearings fit into tip slots 4 Replace head and push flaps away from you until slightly tight This secures the head positio...

Page 3: ...on t see the laser reflected off the cantilever and the laser is on use the Mirror 1 knobs to move the laser along the vertical axis until you see it reflected on the edge of the probe then move horiz...

Page 4: ...eeded until the sum is at the appropriate value If after several tries you still can t get the sum high enough remove the head and check mirror 2 s position visually it should be roughly parallel to t...

Page 5: ...o 1 00 Cantilever General 4 Click OK 5 Turn Head back on in software Frequency Sweep Window will open 6 The software will automatically detect the cantilever s resonance peak and select a driving freq...

Page 6: ...he tip into the sample which could damage it 10 When sample is in focus image of tip should be slightly blurry 11 Check laser position to ensure A B and C D are still less than 0 3 V 12 Shut acoustic...

Page 7: ...will change the distance the tip hovers above the sample surface when scanning and can improve resolution of features surface tracking This can be done manually by changing the number in the Set Poin...

Page 8: ...h XEI You can send images directly to the XEI data analysis software from the Buffer in XEP by right clicking on them Or you can open them from the spmdata or User Files folders Flattening your sample...

Page 9: ...f laser switch unplug head and remove head 6a If the tip you used was good leave it on the AFM Otherwise remove head and place tip in the Bad Probes box 7 Remove sample from stage and replace head plu...

Page 10: ...f photodetector A B 3V A B and C D 0 3V 6 Select appropriate mode scanner and frequency 7 Approach surface i Get optically close several mm ii Focus microscope 1mm from surface move Z stage til cantil...

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