Performing pump diagnostic tests
5-5
•
If there is a bad outlet check valve, pressure can possibly increase,
and then immediately decrease as the plunger recedes.
•
If the pressure does not rise to the high-pressure limit, try
repriming the pump or increasing the flow rate parameter setting.
9. Allow the pump to reach the high-pressure limit. The pump should stop
flow automatically.
10. After two minutes, record the pressure (P1). One minute later, record
the pressure again (P2).
Calculate head pressure decay with the formula (P1 – P2)/P1. Verify
that head pressure decay is 0.15 or less. If the pressure decay for the
pump head is greater than 0.15, you can possibly have one or more
faulty check valves. Remove and clean or replace the inlet and outlet
).
11. Relieve head pressure by slowly turning the reference valve knob 1/2
turn to the left (for the 1525µ, position the vent valve to the system).
12. Disconnect the right-hand pump head outlet tubing from the draw-off
valve.
13. Transfer the compression plug from the left-hand port of the draw-off
valve to the right-hand one.
14. Reconnect the left-hand pump head outlet tubing to the left-hand port of
the draw-off valve.
15. Repeat
to test the left-hand pump head.
16. Remove the compression plugs from the draw-off valve and the tee.
Reconnect the right pump head outlet tubing. Reconnect the tubing from
the pulse dampener.
17. For binary-type pumps, repeat
through
on Pump B, in
, disconnecting Pump A from the tee.
18. Remove the compression plug from the reference valve (or vent valve)
and reconnect the outlet tube to the system.
19. When you finish, purge the pump with eluent (see
). Direct the
eluent to system by turning the reference valve to the left (for the 1525µ,
position the vent valve to the system).
Summary of Contents for 1500-Series
Page 14: ...xiv Table of Contents ...
Page 32: ...1 18 Introduction ...
Page 50: ...2 18 Installing the HPLC Pump ...
Page 84: ...3 34 Installing Options and Accessories ...
Page 108: ...4 24 Preparing for Operation ...
Page 160: ...A 14 Safety Advisories ...
Page 184: ...C 16 Solvent Considerations ...