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Waltron User Manual 101-024-B.1 
3048 Dissolved Iron Analyzer 

Maintenance 

MAINTENANCE 

7.1 

SCHEDULED MAINTENANCE 

Basic maintenance of the Waltron 3048 Analyzer requires that the reagent containers are refilled 
or replaced and that the colorimetric cell is cleaned on a regular basis.  In addition, the user 
should perform a regular 'visual overall-check' of the wet part for immediate corrective measures, 
e.g. in case of leakages etc. Cleaning of the analyzer cabinet is best performed using a soft, non-
aggressive cleaner. 
 
The use of a logbook for cataloging reagent refilling, corrective measures and scheduled 
maintenance is strongly recommended. 
 
During the performance of the basic maintenance work, as described in this chapter, the analyzer 
can not be operational. Prior to the maintenance work, all necessary precautions regarding 
personal safety (protective clothing, safety glasses etc.) are to be taken into consideration.  
Always be sure to label and rinse all connected tubing with water prior to removal. 
 

 

 

Waltron Colorimeter is based on colorimetric analysis 
methods, using chemical solutions.  Make sure that proper 
safety precautions are taken (e.g. using safety gloves and 
glasses) during handling the chemical solutions. 

 

 
 

List of scheduled maintenance: 

 

Visual check 

Everytime that it is possible, visually check the following items: 

 

Liquid leakages 

 

Cell sample level (during cycle) 

 

Glass cell cleaness condition  

 

Reagent level % 

 

Monthly 

 

Visual overall check 

 

Colorimetric cell cleaning 

 

Reagent(s) replacement (reset reagent counters) 

 

Reagent pump(s) priming 

 

Calibration blank with DI water, slope with calibration solution 

 

Quarterly (Every 3 Months)

 

 

Pinch valve drain tubing replacement 

 

Peristaltic reagent pumps tubing replacement 

 

Peristaltic sample pump tubing replacement 

 

 

Summary of Contents for 3048

Page 1: ...101 024 B 1 EXPERTS IN WATER CHEMISTRY SINCE 1903 3048 Dissolved Iron Analyzer User Manual...

Page 2: ...534 5546 www waltron net Please be ready to provide the following information Date analyzer was purchased Analyzer model and serial number Recent maintenance history Calibration slope values and detai...

Page 3: ...ontainers packages and chemicals Only qualified personnel should be involved in the installation operation and servicing of the analyzer Follow safety precautions when operating analyzer in conditions...

Page 4: ...hnical Service Department Customer name address and department Name and telephone number of the individual responsible for returning items for repair Brief problem description Ship to Waltron service...

Page 5: ...oving and shipping needs Check all items received against those on the packing list Chemicals are usually shipped in a separate package and will be itemized accordingly Verify that the number of packa...

Page 6: ...10 1 2 1 General Information 10 1 2 2 List of Warnings and Potential Dangers 11 1 2 3 Reagents 12 1 2 4 Sample 12 1 2 5 Waste Disposal 12 1 2 6 Analyzer General Hazards 12 2 Introduction 15 2 1 Analy...

Page 7: ...5 6 2 Chart 35 5 6 3 Manual Step 35 5 7 Data Logger 36 5 7 1 Save to USB 36 5 8 Program Menu 37 5 8 1 Settings Menu 37 5 8 2 Calibration Menu 38 5 9 Service Menu 39 6 Operation 40 6 1 Reagents Prime 4...

Page 8: ...gure 3 2 Reccomended complete system installation 26 Figure 3 3 Electrical connections for user connections and power connections 28 Figure 3 4 Mounting schematics for the reagent holding bracket 29 F...

Page 9: ...ic determination 18 Table 3 1 Terminal block pin locations 28 Table 5 1 User password 31 Table 5 2 Menu access level with password 31 Table 5 3 Analyzer operating statuses 32 Table 5 4 Main menu butto...

Page 10: ...cy Alarms 2 or 4 configurable alarm relays Reproducibility 2 of reading whichever is greater Degree of Protection IP55 NEMA 4 Wet section IP65 NEMA 4x Electronics Required Maintenance Monthly replenis...

Page 11: ...ements written on this manual The user has the responsibility to read and understand the information contained in this manual and to abide by all applicable employee health and safety regulations Use...

Page 12: ...istaltic pump motor input terminal mixing pump heater Hazard of chemical burns This symbol is used to indicate the potential hazard of severe burns and serious injury due to hazardous chemicals All ha...

Page 13: ...the materials of construction listed below Table 1 2 List of materials used in Waltron 3048 Analyzer Pump tubing Silicon or Norprene Fittings PP Connection tubing Norprene Silicon Colorimetric cell G...

Page 14: ...have been designed built and located in a closed enclosure with a special key Inside the enclosure these parts have protective covers to avoid any contact and physical injuries to users HAZARD Hazard...

Page 15: ...electrocution have been designed built and located in an enclosure with a special key Inside the enclosure these parts have protective covers with warning labels to avoid contact and serious injuries...

Page 16: ...ng a colorimetric method The analyzer is assembled in an enclosure with a lockable door The LIQUIDS enclosure includes all the components involved in sample and reagent flows as well as mixing and rea...

Page 17: ...solution is measured at a specific wavelength The absorbance is related to sample concentration according to Beer s law The Lambert Beer law is an empirical relationship that relates the absorption of...

Page 18: ...ranges from 0 to 1 but it can go higher An absorbance of 0 at some wavelength means that no light of that particular wavelength has been absorbed The intensities of the sample and reference beam are...

Page 19: ...aiting time is programmed in order to eliminate bubbles and suspensions First measurement Reference function A reading is taken using the colorimeter to provide a reference value to compare the measur...

Page 20: ...on Analyzer 2 4 2 FLOW DIAGRAM Figure 2 4 Flow diagram 2 4 3 ANALYZER OPERATIONS The Waltron 3048 Dissolved Iron Analyzer performs several operations throughout a cycle A list of common operations is...

Page 21: ...r sample circulation to avoid accumulation of suspended solids The sample flow should be adjusted to allow continuous sample overflow to waste through the U shaped stainless steel tube Inside the rese...

Page 22: ...Introduction 21 Waltron User Manual 101 024 B 1 3048 Dissolved Iron Analyzer Figure 2 6 Mounting dimensions for the fast loop reservoir 10 36 259 mm 5 84 146 mm 5 24 131 mm 5 20 130 mm 0 26 6 5 mm...

Page 23: ...let pass through the housing enclosure on the right hand side of the unit and are connected to the 3 way valve Colorimetric Reaction Cell The colorimetric reaction cell is made of glass the diameter i...

Page 24: ...the colorimetric cell 2 7 ELECTRONICS The microprocessor and its PCB assembly are located in the electronic section It provides control for the entire analyzing system It handles the analyzer operatio...

Page 25: ...80 relative humidity If the temperature could fall below 5 C the analyzer should be installed in a heated cabinet Because of chemicals and waste gases it is necessary to have a well ventilated locati...

Page 26: ...about 8 20 cm on either side and about 40 100 cm in the front Sufficient space for the reagent containers should be provided on the side or beneath the analyzer The reagent containers should be positi...

Page 27: ...26 Waltron User Manual 101 024 B 1 3048 Dissolved Iron Analyzer Installation Figure 3 2 Reccomended complete system installation Note Single channel analyzers will only have one Fast Loop Reservoir...

Page 28: ...fficiency of the analyzer s grounding Users and qualified maintenance personnel must proceed as follows Be aware of electrical shock and or electrocution labels placed on the analyzer Always isolate p...

Page 29: ...tact labels starting with pin 1 on the left Figure 3 3 Electrical connections for user connections and power connections Table 3 1 Terminal block pin locations Pin Number Terminal Label Description 1...

Page 30: ...e reagent bracket below the analyzer NOTE Mount the bracket below the analyzer so that the base of the bracket is at least 14 inches 40 cm below the analyzer but no more than 30 inches 75 cm below the...

Page 31: ...mple tubing as follows a For single channel analyzers connect the sample to connection 1 on the inlet block and the standard to connection 2 b For dual channel instruments connect sample 1 to connecti...

Page 32: ...ly pressing the touchscreen buttons Figure 5 1 User interface main display screen 5 2 USER PASSWORD Table 5 1 User password First Level Password service 1111 Second Level Password admin Contact Waltro...

Page 33: ...in the PROGRAM menu Analysis Cycle and started when the START ON LINE button has been pressed As soon as the analyzer completes an analysis cycle it will restart with a new analysis This condition is...

Page 34: ...ent level falls below a value of 4 the analyzer goes into FAULT status and stops automatically The alarm message will be displayed in the main menu and the FAULT contact will be activated Every time t...

Page 35: ...y mode and wait for the user s next command CH 2 available on dual stream units only This command will perform a single analysis cycle on stream 2 At the end of the cycle the analyzer will go into sta...

Page 36: ...culated Blank shows the most recent blank value Led shows the led supplied Valid it shows the validation value in compared to the calibration value Current operation this window displays the current a...

Page 37: ...all results in memory Figure 5 6 Data logger screen of the user interface 5 7 1 SAVE TO USB To export the stored results in the data log to a csv file 1 Insert a USB memory stick into the bottom of t...

Page 38: ...user to set the ratio of the analysis cycles versus the extra cycles the alarm value low or high and to enable or disable the loss of sample alarm and the 4 20 mA output CALIBRATION MENU This function...

Page 39: ...between analysis cycles when the analyzer is in on line mode Result alarm Programs the low high value alarm The alarm is expressed in of full scale Output Signal Enables disables the 4 20 mA output Da...

Page 40: ...he range of the analyzer This setting only applies to dual stream analyzers Configuring Relay 1 2 3 and 4 There are 4 cells on the service screen to configure Relay 1 Relay 2 Relay 3 and Relay 4 Touch...

Page 41: ...PLE function for 20 seconds 4 Select ADD REAG 1 function for 60 seconds in order to prime the reagent line Visually confirm that reagent is being drawn into the lines and into the flowcell If no reage...

Page 42: ...period of extended shut down The recommended and default setting for automatic calibration is approximately once per week 1 Login with the 1st level service password 1111 2 Connect the CAL tube to the...

Page 43: ...analyzer into online operation until a calibration has been performed 1 Connect the sample tubing to the fast loop reservoir and turn on sample flow to the fast loop reservoir 2 Check that the sample...

Page 44: ...ng will be displayed on the main screen The result can also be found in the data logger 6 The analysis returns to standby mode and waits for another user command 7 When the user is finished with the g...

Page 45: ...aintenance work all necessary precautions regarding personal safety protective clothing safety glasses etc are to be taken into consideration Always be sure to label and rinse all connected tubing wit...

Page 46: ...d manintenance reference chart Scheduled Maintenance Frequency Daily Monthly Quarterly Annually Visual check of FAULT alarm indicator X Visual check of liquids enclosures for leakages detection X Visu...

Page 47: ...pills 7 Place the pump half containing the rotor in one hand and place the rollers in the 2 6 and 10 o clock positions Place tubing in the outer port and against the two rollers as shown keeping your...

Page 48: ...the drain tubing into the drain valve pinch mechanism 9 Feed the drain tubing through the bottom of the enclosure 10 Connect the drain tubing to the T fitting 11 Perform a manual command of sample 1...

Page 49: ...the first pump roller into the open space 9 From the manual commands menu perform an add reagent 1 command for 1 second This should rotate the first pump roller into place against the tubing and open...

Page 50: ...down period please proceed as follows 1 Replace the reagents in the container with distilled water and perform a priming of all the pumps with DI water a Login with the 1st level service password 1111...

Page 51: ...mple cell Loss of Sample 1 The sample to stream 1 is lost Check the flow of Sample 1 Loss of Sample 2 The sample to stream 2 is lost Check the flow of Sample 2 Dual stream analyzers only Emergency Sto...

Page 52: ...ing Description Part Number Pump Head 7016 Sampling Pump W9040 007 Pump motor 70 80 rpm 24 Vdc W3040 015 External Reservoir Fast loop with level switch W3040 003 Peristaltic pump for reagents W3040 05...

Page 53: ...52 Waltron User Manual 101 024 B 1 3048 Dissolved Iron Analyzer Appendix A Panel Mount Schematics APPENDIX A PANEL MOUNT SCHEMATICS...

Page 54: ...Appendix A Panel Mount Schematics 53 Waltron User Manual 101 024 B 1 3048 Dissolved Iron Analyzer...

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