Thermo Scientific Savant Speedvac ISS110, Instruction Manual

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The ISS
110
SpeedVac ® Concentrator is a complete system for solvent
evaporation, sample concentration, and drying using a patented technique that
combines centrifugal force, vacuum, and applied heat. It is intended for use with
aqueous and non-aggressive solvents such as ethanol and methanol. It may also
be used with small quantities of acetonitrile and ammonium hydroxide.
The ISS110 SpeedVac Concentrator combines a sample chamber, a rotor assem-
bly, an oil-free vacuum pump and a refrigerated vapor trap in a small
compact housing. The ISS110 applies vacuum to samples only when the rotor is
spinning, thus preventing bumping and foaming. Where required, the ISS110 can
apply thermal energy to the samples to counteract the cooling effect of
evaporation under vacuum.
Polypropylene fittings and Teflon
®
coated sample chamber and vacuum pump
heads resist corrosion and ensure reliable operation.
UNPACKING. Open the shipping carton. Compare the contents with the packing
list. Inspect the system and components for any damage from shipment. If
damage is evident, save the shipping carton and immediately notify the carrier or
your distributor.
SITE PREPARATION. The ISS
110
requires a stable, level surface for proper
operation. Units configured for 115 VAC, 60Hz, should be plugged into a circuit
rated for at least 10 amps. Units configured for 230 VAC, 50Hz, should be
plugged into a circuit rated for, at least, 5 amps.
I MPORTANT INFORMATION. Before operating the unit, read section 3.0
Operation and Section 4.0 Application Information to determine your specific
application requirements.
Start-of-day procedure . At the start of each day, ensure that the refrigerated
trap contains a clean, dry, Glass Condensation Flask (GCF400) and that the sup-
ply of CryoCool
® Heat Transfer Fluid is adequate.
The CryoCool fluid in the refrigerated trap must be cold before drying samples.
For the best results, maintain electrical power to the system at all times to keep
the refrigerated trap cold and ready for use. When you first turn on the ISS110,
wait 45 minutes for the system to reach operating temperature before processing
samples!
GLASS CONDENSATION FLASK INSTALLATION.
1. Prepare the refrigerated stainless steel trap chamber by adding approximately
800 ml of CryoCool fluid. A line scribed on the wall of the stainless steel trap
indicates the minimum appropriate fluid level (with flask removed from trap).
CryoCool conducts heat away from the Glass Condensation Flask, allowing
vapors to condense on the flask walls.
1.0 INTRODUCTION
2.0 INSTALLATION
3.0 OPERATION
1