Page 1: ...Orbitrap Tribrid Series Getting Connected Guide 80000 97025 Revision A June 2018...
Page 2: ...of the division of Saint Gobain Performance Plastics Corporation Chemyx is a trademark of Chemyx Inc MX Series II is a trademark of IDEX Health Science LLC All other trademarks are the property of The...
Page 3: ...ation instructions provided in the documentation that comes with your system Order replacement parts as specified in the instrument manual and additional components options and periph erals directly f...
Page 4: ...Directive 2014 30 EU and other EMC test standards This device was tested by T V Rheinland of North America and complies with the following EMC standards 47 CFR 15 Subpart B Class A 2012 EN 61326 1 201...
Page 5: ...you purchased the product Number of product pieces and the estimated total weight and volume Pick up address and contact person include contact information Appropriate pick up time Declaration of dec...
Page 6: ......
Page 7: ...g the Workbench Wheels 4 Chapter 2 Connecting the Nitrogen and Helium Gases 5 Gas Specifications 5 Connecting the Instrument Gas Lines 6 Chapter 3 Connecting the API Source and Waste Container 9 Insta...
Page 8: ...Contents viii Orbitrap Tribrid Series Getting Connected Guide Thermo Scientific MS Setup Kit 24 Power Cords 25 Index 27...
Page 9: ...pectrometry applications such as the Thermo Xcalibur data system For a list of hardware differences for this MS series see Model Differences Also because this guide uses drawings of various connection...
Page 10: ...r All Programs Windows 7 Thermo Instruments model x x and then open the applicable PDF file Viewing Online User Documentation Visit the Thermo Fisher Scientific website for product manuals and more To...
Page 11: ...hat can make a task easier Caution Read the cautionary information associated with this task Chemical hazard Observe safe laboratory practices and procedures when handling chemicals Only work with vol...
Page 12: ...s the required number of forepumps and the available options for the Orbitrap Tribrid Series MSs Instrument Number of forepumps Available options EASY IC ion source EASY ETD ion source Advanced peak d...
Page 13: ...To find global contact information or customize your request 1 Go to thermofisher com 2 Click Contact Us select the country and then select the type of support you need 3 At the prompt type the produc...
Page 14: ...Preface xiv Orbitrap Tribrid Series Getting Connected Guide Thermo Scientific...
Page 15: ...orepumps to the Lab Exhaust System Locking the Workbench Wheels Connecting the Forepumps to the Mass Spectrometer Before you begin lift up and remove the workbench s front panel To determine which ins...
Page 16: ...g clamp connect a 90 degree plumbing elbow to the MS s back vacuum port with the open end facing toward the side not the floor as shown Then using a center ring and swing clamp from the vacuum hose as...
Page 17: ...cts as a trap for exhaust fumes that would otherwise recondense in the forepump oil Maintain the exhaust pressure from atmospheric pressure minus 15 mbar to 1 15 bar absolute 0 15 bar relative Althoug...
Page 18: ...eels 1 Lift up the workbench s front panel to remove it and set it aside 2 Lock the front wheels by moving the locking levers forward to the upright position The locking levers have three positions To...
Page 19: ...sure and purity as listed in Table 2 Table 2 Summary of the required gases for the Orbitrap Tribrid Series MS Type Recommended purity Required pressure Typical daily consumptiona a Approximate value w...
Page 20: ...ther length of copper tubing except connect it between the Helium In inlet and your UHP helium gas supply 3 UHP nitrogen gas Cut a length of the copper tubing attach the 1 8 in ID Swagelok type nut an...
Page 21: ...eries Getting Connected Guide 7 IMPORTANT After you start using the MS do not shut off the gases Optimum performance requires a continuous gas flow Do not shut off the UHP nitrogen gas unless you have...
Page 22: ...2 Connecting the Nitrogen and Helium Gases Connecting the Instrument Gas Lines 8 Orbitrap Tribrid Series Getting Connected Guide Thermo Scientific...
Page 23: ...st Connections Connecting the Solvent Waste Container Installing the API Source All the wiring and gas plumbing for the API source are internal This means you can install or remove the API source or c...
Page 24: ...come contaminated if the drain waste tubing and the exhaust tubing from the forepump connect to the same fume exhaust system Ensure that the waste container vents to a dedicated fume exhaust system do...
Page 25: ...te container to a fume exhaust system To prevent solvent waste from backing up into the instrument make sure that all Tygon tubing is above the level of liquid in the waste container as follows From t...
Page 26: ...3 Connecting the API Source and Waste Container Connecting the Solvent Waste Container 12 Orbitrap Tribrid Series Getting Connected Guide Thermo Scientific...
Page 27: ...set up the syringe pump and plumb the modular valve refer to the Getting Started Guide Using the screwdriver and two of the provided screws attach the bottom shelf to the holder 1 Not shown Place the...
Page 28: ...4 Installing the Syringe Pump and Modular Valve 14 Orbitrap Tribrid Series Getting Connected Guide Thermo Scientific...
Page 29: ...minutes to allow time for the voltage potential to dissipate Mass spectrometer Be aware of the following The AC Output receptacle is not used at this time do not plug the forepump or any other applia...
Page 30: ...f press its front Remote button to exit local mode 5 1 Connect the relay control cable between the MS V65 Pump Enable and the forepumps 4 Not shown Connect the Ready Out cable not provided and contact...
Page 31: ...tions can control external devices for example autosamplers pumps and detectors from several manufacturers including Thermo Fisher Scientific Agilent Technologies and Waters Corporation When an extern...
Page 32: ...quirement you cannot use it with the MS To help prevent sample waste if the MS becomes unresponsive connect a cable between the optional LC device and the MS s Ready Out and Injection Hold pins see Ta...
Page 33: ...nd closes when the method finishes Output Maximum 24 Vdc 3 A 6 Injection Hold Provides a relay driven programmable output signal to the connected external device such as a fraction collector Output Ma...
Page 34: ...de of the MS Other connectors USB 2 ports Provides a connection for the syringe pump and modular valve Ethernet 1000 Base T Provides a connection for the Ethernet switch Table 3 Pin out descriptions f...
Page 35: ...anual Contents Syringe Pump and Modular Valve Assembly Single Mechanical Pump Kit Dual Mechanical Pumps Kit MS Setup Kit Power Cords Syringe Pump and Modular Valve Assembly Image Item Quantity Part nu...
Page 36: ...ess steel caster wheels 1 00201 99 00549 Relay control cable single pump 2 4 m 8 ft long preassembled 1 80000 63139 Single pump vacuum hose assembly KF40 preassembled exploded view shown 1 80000 60229...
Page 37: ...ac 50 60 Hz 2 00108 01 00032 Forepump oil tray stainless steel caster wheels 2 00201 99 00549 Dual relay control cable 2 4 m 8 ft long preassembled 1 80100 63146 Dual pump vacuum hose assembly includi...
Page 38: ...itch 5 port gigabit 1 00825 01 00111 Gas connections Ferrule brass back 1 4 in ID 2 00101 04000 Ferrule brass back 1 8 in ID 2 00101 02500 Ferrule brass front 1 4 in ID 2 00101 10000 Ferrule brass fro...
Page 39: ...s are provided for Thermo Fisher Scientific field service use only Plug configuration Plug rating Mass spectrometer 2 5 m 8 ft North America P N 96000 98035 NEMA 6 15 250 Vac 15 A Internationalb P N 8...
Page 40: ...A Installation Kits and Power Cords Power Cords 26 Orbitrap Tribrid Series Getting Connected Guide Thermo Scientific...
Page 41: ...iv forepump connections fume exhaust system cautions 3 vacuum hose 2 forepumps fume exhaust system cautions 10 gas ballast valve opening 3 maintenance instructions 1 G gases specifications and consum...
Page 42: ...g Connected Guide Thermo Scientific Index T T Thermo Fisher Scientific website user documents x tools 13 troubleshooting Ethernet switch 16 V valve LED 16 viewing documents x W WEEE directive v workbe...
