Thermo Scientific ESCALAB 250 Manual Download Page 12

Monochromated X-Ray Source with XR5 Electron Gun 

Issue 5 

 

Monochromator and XR5 (HA600054)

23

 

This is the active anode surface and must face towards the gun cathode.  

The anode mini-flange is marked with an "A" adjacent to the bolt hole in line with 
this flat.  

 

Make sure that the "A" is facing towards the gun source. 

x

x

Figure 5-4: XR5 Anode Orientation 

13. 

Replace all the removed items in reverse order to the removal sequence.

14. 

Place the PTFE HT shield tube over the anode and loosely refit the PTFE collar 
and retaining flange before fitting the cooling/HT conduit

15. 

Make sure the cooling pipe connectors are driven fully on to the anode-cap-
pipes.

16. 

Clamp the retaining collar and screw on the PTFE HT shield. 

17. 

Refit the HT protection cover, remembering to twist home and tighten the clamp 
screws. This operates a microswitch which is part of the safety interlocks for the 
X-Ray power supply. 

18. 

Pump down and bake the system before use. 

5.5 Replacing 

Filaments/Cathodes 

The emitter should normally give long lifetime, well in excess of 1000 hours, provided 
that it is operated in good vacuum conditions and within the recommended 
voltage/power limits. 

If the emitter condition requires its replacement, the vacuum system will have to be 
fully shut down and vented to dry nitrogen. 

As a further precaution disconnect the mains supply from the T352/NT X-Ray power 
supply.

Refer to the 

Figure 5-5: XR5 Lens and Emitter Assemblies

.

1. 

Remove the M8 x 16 hex head bolt clamping the XR5 earth strap. 

2. 

Unplug the leads from the XR5. 

3. 

Do not unbolt the 70mm/FC38 11-pin feedthrough flange. This is unnecessary 
except when replacing the feedthrough. 

4. 

Remove all the M8 x 35 hex head bolts except for 3 at well-spaced positions to 
retain the main 114mm/FC64 flange. 

5. 

Unscrew the last 3 bolts in sequence 1-turn at a time. This is to symmetrically 
release the loading from the spring-loaded emitter cup. 

6. 

After about 3mm retraction the spring-loading is released and the flange can be 
fully removed. 

 

Stand the flange on a clean work surface with the emitter facing up. 

Monochromated X-Ray Source with XR5 Electron Gun

Monochromator and XR5 (HA600054) 

 

Issue 5  

24

Figure 5-5: XR5 Lens and Emitter Assemblies 

Refer to 

Figure 5-6: XR5 Emitter Flange Assembly

.

7. 

Note the electrical connections: 1 Focus; 2 filament; 1 cathode; 1 double pin 
interlock and 1 ground.

8. 

Note the pre-set height of the emitter cup assembly from the vacuum flange 
surface.

9. 

Loosen the 3 spring loaded screws in sequence, a few turns at a time, until fully 
removed.

10. 

Using tweezers, disconnect the (2) filament and (1) cathode lead from the pin 
base.

11. 

Place the emitter cup assembly on the work surface with the leads facing up. 

Figure 5-6: XR5 Emitter Flange Assembly 

Summary of Contents for ESCALAB 250

Page 1: ...Moving the XR5 Anode 12 3 6 Monochromator Fine Tuning 12 3 6 1 Alignment of the Analysis Centre and Microscope Cross Hairs 12 3 7 T352 NT Computer Controlled Power Supply 14 4 Monochromator Operation 15 4 1 Avantage Data System Monochromator Controls 15 4 1 1 Errors and Warnings 16 4 2 Different XR5 Operating Modes 16 4 3 Switching on the Re circulated Water 17 4 4 Observing the Monochromator Spot...

Page 2: ...ing the online manual loaded with the software datasystem It does not include detail on the initial installation and setting up of the electron gun or crystals nor any troubleshooting or maintenance which would require the user to directly access high voltage It includes procedures for replacement of certain consumable items such as anodes and filaments which require the system to be vented and su...

Page 3: ...nterlocks are displayed in the software within the Trips Interlocks display as in GREEN OK or RED FAIL for the state of the interlocks Typical Trips Interlocks displays are shown in Figure 2 1 Occasionally pop up warning messages will appear After taking note of the message select the OK button Go into the details window and look at the Trips Interlocks you will see a red FAIL in the appropriate w...

Page 4: ... software they include x Temperature in T352 Power Supply rises to unacceptable levels x Current drawn from T352 Power Supply HV greater than 60 mA x Drain from HV through X ray water lines greater than 20 mA Monochromated X Ray Source with XR5 Electron Gun Monochromator and XR5 HA600054 Issue 5 8 3 Description 3 1 Introduction The Monochromated X Ray Source produces X Rays which have well defined...

Page 5: ...uit uses mains water or a re circulator as its input and then increases the flow through the X Ray source by use of a booster pump The control of the booster pump and of the solenoid valves which switch the water flow between the twin anode if fitted and mono source is by the datasystem via the T352 NT power supply Both the twin anode and mono anode are floating at high voltage and have water flow...

Page 6: ...e by 0 8 mm per turn The range of motion and the useful anode length are both 25 mm A fraction of a turn for example a half turn will usually be enough to expose a new aluminium film area 3 6 Monochromator Fine Tuning Complete alignment and set up of standard operating conditions will generally be carried out by Thermo Fisher Scientific service engineers and most operators will not need to be conc...

Page 7: ...ing Ratings Main HT 15kV 60mA Normal operating or 20kV 20mA Source conditioning Monochromator Filament 2 5A Bombard 3000V Cathode 1200V Focus 3500V Table 2 Specification Outputs for the Monochromator Gun Control is entirely from the computer no manual controls are fitted except for the rear panel mains power switch The supply requires five interlock loops Vacuum Water flow Twin anode cover Mono co...

Page 8: ...the Apply button should then be selected Monochromated X Ray Source with XR5 Electron Gun Monochromator and XR5 HA600054 Issue 5 16 4 1 1 Errors and Warnings As the monochromator is ramping up to the desired operating point the data system will check for any problems and report these as a warning window If an Error does occur the data system will display a warning dialogue and instruct the operato...

Page 9: ...upplied from the system or from a separate mains circuit in the laboratory If this is not switched on then when an attempt is made to switch on the monochromator the booster pump will run dry be much louder than normal and possibly be damaged The monochromator gun will not turn on as the water flow interlock will have failed 4 4 Observing the Monochromator Spot For fine tuning of the monochromator...

Page 10: ...nd converge as the sample is raised and lowered 4 Position each spot by moving the dispersive and non dispersive adjusters on the crystal manipulator do NOT adjust the heights of the crystal as this will change the energy of the X Ray spot from each crystal to coincide with the cross hairs on the viewing camera These adjusters are very sensitive so only small adjustments should be made Never adjus...

Page 11: ...eplacing Anodes In general the anode will need replacing only when all the aluminium coating has been degraded sufficiently to attenuate the X Ray flux below acceptable levels along its entire length If the anode condition requires its replacement the vacuum system will have to be fully shut down and vented to dry nitrogen Figure 5 3 XR5 Anode Assembly Refer to Figure 5 3 XR5 Anode Assembly 1 Unpl...

Page 12: ... vented to dry nitrogen As a further precaution disconnect the mains supply from the T352 NT X Ray power supply Refer to the Figure 5 5 XR5 Lens and Emitter Assemblies 1 Remove the M8 x 16 hex head bolt clamping the XR5 earth strap 2 Unplug the leads from the XR5 3 Do not unbolt the 70mm FC38 11 pin feedthrough flange This is unnecessary except when replacing the feedthrough 4 Remove all the M8 x ...

Page 13: ...ges Use a new FC64 copper gasket and make sure that the flange is offered to the gun in the correct orientation The main flange is labelled TOP on its circumference adjacent to the focus connection This should be in the top vertical position when refitted to the gun on the system 22 Check the pin base for filament and interlock continuity and all other pins for electrical isolation 23 Fully tighte...

Page 14: ...Issue 5 28 5 9 Fault Finding Symptom General Cause Specific Cause How to Rectify How to Fix Mains re circulated water supply switched off Booster pump will make excessive noise Check supply Look for warning messages on datasystem Switch on supply Insufficient water flow Warning message on datasystem Water flow not sufficient to satisfy flow requirement Check inlet and outlet flow Look for warning ...

Page 15: ...n still runs correctly Loss of control of the gun from the datasystem Gun still running An HT tick has effected communication Reboot the datasystem Try the gun control again Table 4 Fault Finding 5 10 Fuses Information for Service Engineers Within the digital X ray PSU T352 NT there is an 800mA T fuse on the mains input Monochromated X Ray Source with XR5 Electron Gun Monochromator and XR5 HA60005...

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