Thermo Scientific Barnstead Nanopure TOC - UV Operation Manual Download Page 1

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Barnstead Nanopure

™

TOC - UV

ultrapure water system

Operation Manual

Series 2115 and 2117

Model No.

Voltage

D11951

100V - 240V

D12421

100V - 240V

LT2115X1 • 11/23/09

Summary of Contents for Barnstead Nanopure TOC - UV

Page 1: ...Barnstead Nanopure TOC UV ultrapure water system Operation Manual Series 2115 and 2117 Model No Voltage D11951 100V 240V D12421 100V 240V LT2115X1 11 23 09 ...

Page 2: ...Resetting the TOC Lamp Timer 28 Using the TOC Analyzer 29 Setting Volumetric Dispensing 30 Setting Timed Dispensing 30 Performing a System Flush 31 Changing Purity Units 31 Temperature Compensation 31 Auto Standby 32 Unit Under Counter 32 Accessories 34 Feedwater Float or Pressure Switch 34 Dispense Overflow Cutoff Float 35 Performing an Electronic Calibration Using the Optional N I S T Calibratio...

Page 3: ...te the Nanopure TOC UV directly over equipment that requires electrical service Routine maintenance of this unit may involve water spillage and subsequent electrical shock hazard if improperly located 3 Replace fuses with those of the same type and rating 4 Disconnect from the power supply prior to main tenance and servicing To avoid personal injury 1 Do not use in the presence of flammable or com...

Page 4: ... instruc tions on labels of chemical containers and mate rial safety data sheets 7 Depressurize system prior to removing the cartridge pack 8 This unit is equipped with an ultraviolet lamp Ultraviolet radiation is harmful to the eyes and skin Do not attempt to observe the lamp directly 9 Refer servicing to qualified personnel 10 A full cartridge pack may weigh about 20 lbs 4 SAFETY INFORMATION ...

Page 5: ... cm Water resistivity is continuously monitored by a resis tivity cell and displayed on a digital display Actual system TOC values obtained by an integrated TOC analyzer can be concurrently displayed with the resistivity The electronics can be verified and calibrated utilizing a N I S T Traceable Calibration module See accessory ordering information Please read the instructions carefully to ensure...

Page 6: ... Gravity feed to 100 psig 7kg cm2 maximum Temperature Range 4 C 40 C 40 104 F TDS CaCO3 70 ppm Silica 1 ppm Silt 5 SDI Product Water Water Quality Resistivity 18 2 mΩ cm TOC Less than 5 ppb Bacteria 0 01 CFU mL Flow Rate Up to 2 lpm maximum at minimum inlet feed water pressure 10 PSIG with a new final filter Volumetric Dispense Accuracy 5 Repeatability 3 TOC Analyzer Range 1 to 250 ppb Accuracy 1 ...

Page 7: ...technical requirements of the following standards EMC EN 61000 3 2 Limits for Harmonic Current Emissions EN 61000 3 3 Limits for Voltage Fluctuations and Flicker EN 61326 1 Electrical Equipment for Measurement Control and Laboratory Use Part I General Requirements Safety EN 61010 1 Safety Requirements for Electrical Equipment for Measurement Control and Laboratory Use Part I General Requirements p...

Page 8: ... materials before discard ing Put the Nanopure TOC UV on a bench UV Lamp LMX13 Cleaning Cartridge CMX25 Wall Bracket Unit BC1190X12 Wall Bracket Remote Display BC1190X10 Accessory Parts Bag Includes Feed Water Tube 3 8 O D TU1119X7 Drain Tube 14 O D TU1190X12 Display Cable WHX20 Blank Display DL1190X18 Plug Adapter CEX42 Power Cords Also required for installation Customer Supplied Fasteners to mou...

Page 9: ...as well as fastener type must be considered when mounting this unit The mounting surface and fasteners selected must be capable of supporting a minimum of 150 lbs 68 kg Inadequate support and or fasten ers may result in damage to mounting surface and or equipment If you are unsure of mounting surface composition condition and construc tion or correct fasteners consult your building maintenance gro...

Page 10: ...d the chamber before closing and relatching the door Other Accessories Optional accessories for this unit include a float switch low pressure switch N I S T Traceable Calibration Module standard remote dispenser Accudispense volu metric remote dispenser dispense overflow cutoff float and printer If you purchased a float switch or low pres sure switch refer to page 31 of this manual If you pur chas...

Page 11: ... wall bracket slots 7 Push the locking slides on each side of the wall bracket in as far as they will go 8 Replace the locking screws 11 INSTALLATION Note Please refer to the General Specifications section for clearance requirements Warning Do not locate the Nanopure TOC UV directly over equipment that requires electrical service Routine mainte nance of this unit may involve water spillage and sub...

Page 12: ...ol panel is returned to the top cover 6 Locate the 10 ft 3 1 m 25 pin M F cable included with the unit attach the female end to the 25 pin connector on the back top right of the unit and the other end to the connector on the bottom of the control panel 7 Tighten the cable screws on each end to secure the cable to the unit and control panel 8 The control panel may now be mounted on the wall 12 INST...

Page 13: ...When the Nanopure TOC UV flushes its membrane the water used is sent to drain through this connection To install 1 Locate the drain water tubing This is the 1 4 64 cm O D tubing that is approximately 6 ft 1 9 m long The atmospheric drain fitting is located on the lower left side of the Nanopure TOC UV 2 Route the other end of the drain water tubing to an atmospherically vented drain and make a con...

Page 14: ...e tubing push collet toward fitting body and pull on tubing To reuse fitting begin assembly at step one Electrical Connections The Nanopure comes with a 120 V power cord with 2 1 6 amp fuses and 240 V power cords with 2 0 63 amp fuses The Nanopure is not shipped with fuses installed in the fuse draw of the power module Before connecting the power cord to the power module install the proper fuses i...

Page 15: ...em status as follows LED is not illuminated System is OFF or in Idle mode Solid Green LED System is recirculating and operating normally Blinking Green LED System is in Standby mode Red LED System is alerting user to an operational error or maintenance issue The control panel can be removed from the unit and remotely mounted Please refer to Installing the Control Panel in a Remote Location in the ...

Page 16: ...n the User Settings section of this manual for information UP and DOWN arrows allow you to scroll between menu options items and values BACK allows you to return to the previous menu option item Please note that use of the BACK switch from a selection screen will return you to the previous menu option item while maintaining the selection s value upon entry ENTER allows you to activate a selected m...

Page 17: ...absolute final filter Cartridge Pack Installation 1 Open front left side door Turn the cartridge pack so the caps are facing you Remove the caps 2 Verify that each of the four posts on the car tridge pack has an o ring 3 Lift unit manifold upwards insert cartridge pack and align the pack so that it mates with the unit manifold 4 Lower unit manifold until it is flush with the top of the cartridge p...

Page 18: ...ystem greeting will display the type of unit you own This greeting is UV TOC 8 The system electronics will initialize and check its calibration All units have been factory cali brated If calibration is OK the display will show Calibration passed The display will next read Self Test in progress Self Test Passed Finally the display will read 10 0 2 MΩ cm This is a reading of the calibration referenc...

Page 19: ...NTER 3 Unit display will ask if you have Disconnected Inlet Water NO 4 Disconnect feed water supply at the quick dis connect inlet valve on left side of unit 5 Press the UP or DOWN ARROW to select YES and then press ENTER Display will now read Injected Cleaner NO 6 Open front left side door to expose cartridge pack Remove solution syringe from wrapper 7 Remove luer cap on system injection port loc...

Page 20: ...e Idle mode 16 Press the START STOP switch to return the unit to the normal recirculation mode 17 Remove the new 0 2 micron filter and bell assembly from the bag and insert it into the dis penser arm manifold Gently turn it clockwise until it is fully seated 18 Remove the protective cap from the filter bell Turn the dispense knob to the left or right and flush 1 2 liters of water through the 0 2 m...

Page 21: ...he display will begin showing TOC values of the product water Initially it will read TOC ppb until valid data is available which may take up to 4 minutes after starting 7 Allow the water s resistivity to rise to the desired purity before drawing off water 8 The system should be left on or in standby during the work day See Use of Standby Mode Normal Operation Note On initial start up the purity me...

Page 22: ...the dispenser 2 Press DISPENSE Water will start dispensing immediately Display will read xx MΩ cm xx Liters Remaining or xx MΩ cm xx Seconds Remaining or AUTO DISPENSE OFF depending on which dispensing method was last chosen in the auto dispense menu Note Press any switch except ENTER to stop dispensing Display will read Auto Dispense Interrupted by User Note If the Nanopure Auto Dispense fea ture...

Page 23: ...row to choose Yes 5 Press ENTER 6 Press the UP or DOWN arrow until the desired value 100 75 50 or 25 is displayed 7 Press ENTER 8 Press BACK until you return to the Idle display Setting the Displayed Language 1 From the Idle mode when display reads Nanopure Idle xx xx xx xx xx xx press the BACK switch until the display reads LANGUAGE 2 The currently selected language is displayed on line 2 of the ...

Page 24: ...ENTER 6 Press the UP or DOWN arrow until you reach the desired month Press ENTER 7 Press the UP or DOWN arrow until you reach the desired day Press ENTER 8 Press the UP or DOWN arrow until you reach the desired year Press ENTER 9 When prompted with Set Time press the UP or DOWN arrow to choose Yes then press ENTER This is to set the time of day 10 Press the UP or DOWN arrow until you reach the des...

Page 25: ...lose and latch the right side door 5 Reconnect the power cord and turn unit ON 6 From the Idle mode when the display reads Nanopure Idle xx xx xx xx xx xx press the UP or DOWN arrow until the display reads Advanced Menu 7 Press ENTER 8 Proceed through the options by pressing ENTER until Set Cell Constant is displayed 9 Press the UP or DOWN arrow to select Yes 10 Press ENTER 11 Note that the digits...

Page 26: ...TART STOP to return to the recirculating mode Selecting the Set Point The Nanopure TOC UV electronics include a user pro grammable set point which alerts you when water quality falls below the programmed set point The set point is user selectable from 1 18 MΩ cm factory set at 10 MΩ cm 1 From the Idle mode when display reads Nanopure Idle xx xx xx xx xx xx press the UP or DOWN arrow until display ...

Page 27: ... at the factory at 10 MΩ cm Resetting the Cleaning Timer 1 From the Idle mode when the display reads Nanopure Idle xx xx xx xx xx xx press the UP or DOWN arrow until the display reads Reset Timers 2 Press ENTER Display will read Reset UV Timer NO 3 Press ENTER 4 Display will read Reset Cleaning Timer and show on the right side of the second line when the user will start receiving Clean Unit remind...

Page 28: ...n the Nanopure TOC UV is in an Idle position 1 From the Idle mode when display reads Nanopure Idle xx xx xx xx xx xx press the UP or DOWN arrow until the display reads Reset Timers Press ENTER 2 Press ENTER until the display reads Reset TOC Timer It will also read on the right side of the second line the hours of usage which have occurred since the TOC Timer was last reset 3 Press the UP or DOWN a...

Page 29: ...only resistivity conductivity readings are to be displayed 1 From the Idle display press UP or DOWN arrow until Advanced Menu is displayed 2 Press ENTER 3 Press ENTER when Printer Attached is dis played 4 Continue pressing ENTER until Use TOC Analyzer is displayed 5 Press UP or DOWN arrow to choose Yes 6 Press ENTER 7 Press BACK twice from the Date Format dis play to return to the Idle mode USER S...

Page 30: ...he UP or DOWN arrow until the display reads Auto Dispense Menu 2 Press ENTER 3 Display will read Dispense Method Press the UP or DOWN arrow to select TIME 4 Press ENTER Display will read Time Setting xx Minutes 5 Press the UP or DOWN arrows to set the desired time value Press ENTER UP arrow 1 up to 5 min then increments by 5 minutes DOWN arrow Decrement by 1 minute Maximum 40 minutes Minimum 1 min...

Page 31: ... BACK to return to the normal recirculating mode Temperature Compensation Factory set to ON 1 From the normal recirculating mode when the display is showing purity press the Up or DOWN arrow until the display reads Temperature Compensation Press ENTER 2 Press the UP or DOWN arrow to select OFF or ON Press ENTER 3 Press BACK to return to the normal recirculating mode USER SETTINGS Note Purity displ...

Page 32: ...isplay Unit Under Counter Factory set to NO This option will lock out any type of automatic dispense out of the unit Accudispense accessory D13661 will still operate normally This will prevent accidental dispensing from the unit if it is located under a counter or similar area such that the unit dispenser is not in site of the user but the display is i e remote mounted display 1 From the Nanopure ...

Page 33: ...33 until UNIT UNDER COUNTER is displayed 4 Press the UP or DOWN arrow to choose YES 5 Press ENTER 6 Press BACK until you return to the Idle dis play USER SETTINGS ...

Page 34: ...at switch follow the installation instructions included with the float switch for installation into a tank 3 If using the D2706 low pressure switch install the PVC tee supplied with D2706 in the incoming water line Screw the switch into the top of the tee then connect the inlet tubing of the Nanopure TOC UV into the remaining opening of the PVC tee 4 Route the cable from the float or low pressure ...

Page 35: ...ic dispense time or volumetric plug AY1367X1 into connector on back right side of Nanopure See Figure 13 2 Position carboy to be filled and place float assembly on open neck of carboy Position float assembly such that it will not interfere with prod uct water stream being dispensed into carboy 3 Initiate Auto Dispense as described in the Automatic Dispensing section of this manual If during the au...

Page 36: ...e to the connection point J2 To Outlet Cell on the cal ibration board PC1190X2 5 Close and latch door 6 Reconnect the power cord and turn the unit on by depressing the main power switch 7 From the Idle mode Press the UP or DOWN arrow until the display reads N I S T Calibrate Press ENTER 8 Display will show Calibration Module Installed Press the UP or DOWN arrow to select YES 9 Press ENTER 10 Displ...

Page 37: ...nd reconnect the cell 14 Reattach the cover plate and close and latch the door 15 Reconnect the power cord The calibration procedure is complete Manual Remote Dispenser and Accudispense Volumetric Remote Dispenser Refer to the Operating Instructions for your manual or Accudispense volumetric remote dispenser LT1366X11 ...

Page 38: ...o the computer once per minute If Use TOC Analyzer has been set to Yes the TOC data will also be sent 7 Run your Microsoft Windows program Open Hyperterminal located in the accessories direc tory give your setting a name and choose a symbol 8 In the Connect Using box select direct to COM2 or COM1 as port depending on your computer and click OK 9 Using the selection boxes in the next screen configu...

Page 39: ...e display reads Advanced Menu 3 Press ENTER 4 From the Printer Attached display Press the Up or DOWN arrow for NO 5 Press ENTER 6 The unit will now during the normal Recirculation mode send a purity and temperature reading to the computer once per minute If Use TOC Analyzer has been set to Yes the TOC data will also be sent 7 Open DOS window and change directory to pro comm directory 8 Open procom...

Page 40: ...nd the optional TOC data once every minute Connecting and Starting the Printer 1 Make sure the printer and Nanopure are turned OFF 2 Connect the Nanopure to the printer via the RS232 port Use the tan printer cable included with the Epson printer Plug the printer power cord into an electrical outlet 3 Turn the Nanopure ON 4 Turn the printer ON 5 From the Idle display press the UP or DOWN arrow unti...

Page 41: ...et to Yes the TOC data will also be printed Printer Setup Power Switch Located on the front of the printer AY1137X1 this switch turns power to the printer ON and OFF The POWER light will illuminate when the printer is ON For additional setup and operation refer to the instruction manual included with the printer 41 COMPUTER PRINTER SETUP ...

Page 42: ...handling procedure This may be done in an ultrasonic cleaner or with a soft brush 6 Thoroughly rinse the cell in deionized or distilled water following the detergent or acid cleaning 7 After cleaning check the o ring replace if nec essary 8 Reinstall the cell into the cell well and hand tighten 9 Reroute the cable and reconnect to J2 on circuit board 10 Replace pc board cover and close door 11 Rec...

Page 43: ...ly inject the solution into the system and remove syringe Avoid injecting air into system 10 Replace luer cap on injection port Close door 11 Press the UP or DOWN arrow to select YES and then press ENTER Display will now read Reconnected Water NO 12 Attach feed water supply removed in step 4 13 Press the UP or DOWN arrow to select YES MAINTENANCE AND SERVICING Note The cleaning timer will display ...

Page 44: ...essurization This should be done prior to removing a cartridge pack The unit needs to be plugged in and operating to correctly perform this depressurization step 1 IMPORTANT Disconnect inlet water from the left back of unit 2 From the Idle display press ENTER 3 From Air Purge press the UP arrow 4 From Depressurize press the UP arrow to select YES 5 Press ENTER Display will show System Flushing and...

Page 45: ...ice Catalog Number CMX25 This is used to effect a complete cleaning 1 Remove the feed water line by depressing the stainless steel thumb pad 2 Depressurize the system according to System Depressurization under the Maintenance and Servicing section 3 Shut power OFF to the unit and disconnect the electrical service to the unit 4 Open the front left side door 5 Loosen the wing head screws on the cart...

Page 46: ...he dispense arm mani fold Gently turn it clockwise until it is fully seat ed 3 Remove the protective cap from the filter bell 4 Rinse 1 2 liters of water through the filter to drain prior to using the product water MAINTENANCE AND SERVICING Caution Do not overtighten the 0 2 micron filter or use excessive force in seating it The filter can be damaged by over tightening or excessive force Note If a...

Page 47: ... between the normal and Standby modes during the workday this will result in a shorter lamp life Therefore it is recommended that the Nanopure be left in the normal recirculating mode during regular working hours To replace the UV lamp 1 Turn the Nanopure TOC UV OFF and discon nect power cord from unit 2 Access the left side of the unit by unlatching the screw securing the door with a flathead scr...

Page 48: ...new lamp chamber be sure to carefully insert pins of chamber into left side row of sockets on TOC board See Chamber Replacement photo 6 Finish installing the new lamp chamber by securing with clips Clips may need to be pushed apart so the chamber will snap back into place 7 Reconnect power cord and reset the TOC lamp timer See Resetting the TOC Lamp Timer Fuse Replacement 1 Turn off the Nanopure T...

Page 49: ... cord 6 Operate normally Shutdown If the Nanopure TOC UV is to be shut down for an extended period of time the unit should be completely drained and the cartridge pack removed to prevent the growth of bacteria If the system has remained inactive and full of water for more than 96 hours the unit should be drained cleaned and new cartridge pack installed prior to use 49 MAINTENANCE AND SERVICING ...

Page 50: ...un feed water line pressure switch plug or pressure switch cord to the or jumper plug not connected to receptacle located on the upper left pump interlock hand section of the Nanopure Insufficient feed water pressure Open feed water line shut off connect or volume to satisfy the Nanopure feed water line to Nanopure and ensure sufficient pressure or sufficient water level in the feed water reservoi...

Page 51: ...pense more water through the OVERRANGE Nanopure to purge air from the unit Bad cell connection Check the connection of the cell as it attaches to the meter circuit board mounted on the inside of the right door Incorrect N I S T calibration offset If you have a N I S T module perform a N I S T calibration If you do not have a N I S T module perform the calibration function WITHOUT the calibration m...

Page 52: ... Debris on o ring or bottom of Inspect o rings and bottom of unit unit manifold manifold Remove any objects with a lint free cloth Water is leaking at Tubing not fully inserted Insert tubing into connection until atmospheric drain connection it bottoms out Upon system startup the PC board communication Turn the NANOpure OFF I O Switch message TOC Comm Error and restart the unit 0A is displayed No ...

Page 53: ...tivity sensor Cycle power and place TOC analyzer in hour long clean mode under Diagnostics if still shorted replace TOC Analyzer 011 TOC UV lamp error Verify TOC lamp is connected Replace TOC lamp See TOC Lamp Replacement All other error codes Contact technical customer service 53 TROUBLESHOOTING ...

Page 54: ...s kit Check with your cus tomer service representative for additional information on the expendables kit Recommended Description Catalog No Quantity DIamond Kit Organic Free R O Distilled Feed D50280 1 DIamond Kit Organic Free Deionized Feed D50281 1 Final Filter D3750 2 Main Fuse 120 Volt Slow Blow 1 6 Amp 250V FZX47 2 Main Fuse 230 Volt Type T Time Lag 0 63 Amp 250V FZX54 2 PTFE Tape Roll 06078 ...

Page 55: ...ower Supply PC Board TNX116 1 Calibration PC Board PC1190X2 1 Resistivity Meter PC Board PC896X2 1 Check Valve PMX214 1 Wire Harness UV Bulb WH1191X1 1 Flow Sensor ME1190X1 1 Flush Solenoid RY1190X3 1 Cartridge Pack Manifold BK1190X3 1 Dispenser Manifold w Solenoid BK1367X1 1 Dispense Switch SW1190X1 1 Cell O ring GSX29 1 TOC Analyzer PCX54 1 Optional Accessory Ordering Information Description Cat...

Page 56: ... back key pressed force print line Arrow Legend Keypress Options Automatic Entry Menu Wrap around power switch turned on Depressurize Optional Printer Remote Gun Date Format Use TOC Analyzer Set Date Set Time Set Cell Constant Set Display Brightness Unit Under Counter Auto Standby Adjust Set Point Set Unit Type Language Change Units Temperature Compensation System Flush Auto Dispense Menu Clean Un...

Page 57: ...2 CHASSIS GND WH3 BRN RED BLK RED BLK RED BLK BRN RED BLK B C BLK RED WHT WHT BLU BLU RED BLK A MODULE SWITCH POWER ENTRY C1 GND CHASSIS GND L1 L2 NEUTRAL LINE 120V 2 FZX47 FUSES 230V 2 FZX54 SPG SW1190X2 C REMOTE DISPLAY CONNECTOR E2 NIST MODULE E896X5 E896X5 1 2 3 4 CONNECTION POINT FOR ANY ONE OF THE FOLLOWING JUMPER PLUG 04247 PRESSURE SWITCH 02706 FLOAT SWITCH 08964 NOTE PINS 2 AND 3 ON CP1 A...

Page 58: ...ientific dealer from whom you purchased this unit or can be obtained promptly from the factory When service or replacement parts are needed we ask that you check first with your dealer If the dealer cannot handle your request then contact our Customer Service Department at 1 866 9 thermo Prior to returning any materials please contact our Customer Service Department for a Return Materials Authoriz...

Page 59: ...59 ...

Page 60: ...e including use inconsistent with written operating instructions for the product mishandling contamination overheating modification or alteration of the product by any customer or third party or iii use of replacement parts that are obtained from a party who is not an authorized dealer of Thermo Scientific prod ucts Heating elements because of their susceptibility to overheating and contamination ...

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