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Clarity Controls

Teledyne Foxy 200

ENG

Code/Rev.: M165/70B

Date: 12/21/2016

Phone: +420 251 013 400

DataApex Ltd.

Fax: +420 251 013 401

Petrzilkova 2583/13

[email protected]

158 00 Prague 5

www.dataapex.com

The Czech Republic

Summary of Contents for Foxy 200

Page 1: ...trols Teledyne Foxy 200 FC ENG Code Rev M165 70B Date 12 21 2016 Phone 420 251 013 400 DataApex Ltd Fax 420 251 013 401 Petrzilkova 2583 13 clarity dataapex com 158 00 Prague 5 www dataapex com The Czech Republic ...

Page 2: ...demarks of DataApex Ltd Microsoft and WindowsTM are trademarks of Microsoft Corporation DataApex reserves the right to make changes to manuals without prior notice Updated manuals can be downloaded from www dataapex com Author DM ...

Page 3: ...Teledyne Foxy 200 fraction collector communication 3 3 2 Clarity Configuration 4 4 Using the control module 6 4 1 Method Setup FC Fraction Table 7 4 2 Method Setup FC Vial Numbers 12 4 3 Hardware Configuration 14 4 4 Device Monitor 15 4 5 Data Acquisition window 17 4 6 DataApex UNI Setup 18 5 Report Setup 20 6 Troubleshooting 21 i ...

Page 4: ...RK1 capitals indicates the name of the file and or directory ACTIVE capitalitalics marks the state of the station or its part The bold text is sometimes also used for important parts of the text and the name of the Clarity station Moreover some sections are written in format other than normal text These sections are formatted as follows Note Notifies the reader of relevant information Caution Warn...

Page 5: ... direct control of the instrument over serial line Fig 1 Teledyne Foxy 200 fraction collector Direct control means that the fraction collector can be completely controlled from the Clarity environment The Instrument method controlling the analysis conditions will be saved in the measured chromatograms The control is performed via the UNI Ruby control module and the Teledyne Foxy 200 script 1 ...

Page 6: ...ve only one if any serial COM port installed To use more devices requiring the RS232 port the MultiCOM adapter p n MC01 is available l Serial DB9F DB25M cable p n SK12 Note Cables are not part of Clarity Control Module It is strongly recommended that you order the required cables together with the Control Module 2 ...

Page 7: ... p n SK12 described in the picture below Fig 2 Serial DB9F DB25M cable On top of that the fraction collector must be switched to the same Baud Rate as set in Clarity and the ID 5 to work with the control module To do so start the fraction collector and load the Program A then select the Edit A option Select page 3 from the Edit submenu and set the Serial function then set the Baud Rate as desired ...

Page 8: ...tation by clicking on the icon on the desktop l Invoke the System Configuration dialog accessible from the Clarity window using the System Configuration command l Press the Add button on Fig 3 on pg 4 to invoke the Available Control Modules dialog l You can specify the search filter to simplify the finding of the driver 4 ...

Page 9: ...to establish communication with the device l You may fill in the custom Device Name Note The DataApex UNI Setup dialog is described in detail in the chapter DataApex UNI Setup on pg 18 l The Teledyne Foxy 200 item will appear in the Setup Control Modules list of the System Configuration dialog l Drag the appropriate item from the Setup Control Modules list on the left side to the desired Instrumen...

Page 10: ...etting up the new device one or more new tabs will appear in the Method Setup dialog depending on the type of the instrument A new Teledyne Foxy 200 fraction collector section enabling the monitoring of the current fraction collector state will be also created in the Device Monitor window 6 ...

Page 11: ...ction Volume parameter from the Fraction Table helps to prevent collection vial overflowing Flow rate units are taken from the Instrument Method Sending dialog Delay Volume Detector Valve Sets the volume of the tubing between the detector and waste collect valve of the fraction collector Volume units are devised from the Flow Rate Units set in the Instrument Method Sending dialog The delayed volum...

Page 12: ...low Fraction Volume Collected amount can be collected to one or more vials fractions The Fraction Volume value should be lower or equal to the vial volume to prevent vial overflow If the collected volume exceeds the set value the vial will be automatically changed Fraction Volume units are devised from the Flow Rate Units set in the Instrument Method Sending dialog Detector Signal Selects the dete...

Page 13: ...on points and the course of the first derivative before it reaches these End Fraction points Fig 6 Fist derivate course Note It is strongly recommended not to use Slope Signal Condition for fraction collection based on noisy detector signal Start L S End L S The fraction collection l starts when both start signal conditions are fulfilled simultaneously detector signal increases above Level Start v...

Page 14: ... above Slope Start value If none of the start signal conditions is fulfilled the fraction collection does not start l stops when both stop signal conditions are fulfilled simultaneously detector signal decreases below Level Stopvalue and also the first derivative of the detector signal first decreases and then increases above the negative of the Slope Stop value If only one of the stop signal cond...

Page 15: ...n will be delayed the higher the Filter value is set mainly on detectors with low data rate Note Filter settings influence the value that should be set the Slope Start and Slope Stop columns To get the correct trigger value for the Slope Start or Slope Stop using the Show Slope Level tool in the Chromatogram window it is necessary to set the Global Bunching value in the Integration Table to the sa...

Page 16: ...ted The vial number is stored in the Results Table Reset at Specifies the conditions of the current vial number setting to Start Vial Number in three different situations l Each Run the vial number is reset at the start of each acquisition l Start Sequence the vial number is reset only at the start of a sequence l Open Instrument the vial number is reset only once when the Instrument is opened Las...

Page 17: ...the vial is automatically swapped when the peak top is detected during collection Be aware this option is not applied if the active row in the Fraction Table is set to None in the Signal Condition column Collect All When checked fractions are collected during the whole course of the analysis regardless of the settings in the Fraction Table The FC module then sends the Next Vial command only which ...

Page 18: ...ware Configuration The Hardware Configuration dialog invoked by using the FC Status button from the Method Setup FC dialog displays the configuration of the Teledyne Foxy 200 namely the communication type and its parameters Fig 8 Hardware Configuration 14 ...

Page 19: ...on on the button changes according to the state in which the fraction collector is while it is collecting the Waste button forces the fraction collector to stop collecting while it is in a waste cycle the Collect button will force the collector to start collecting Using any of the two actions while the collector is performing the program set on the Method Setup FC Fraction Table tab during an anal...

Page 20: ...Teledyne Foxy 200 4 Using the control module moment it will start a waste cycle and then resume the function of the fraction table 16 ...

Page 21: ...lect Properties to open the Graph Properties dialog and check the Show Events checkbox When the Fraction Delay is set there will be two colors present in the graph lighter and darker red The lighter red color shows the expected duration of the fraction which Clarity only presumes based on data points it got so far while the darker red color shows the placement of the real fractions Note The Fracti...

Page 22: ...lation folder C CLARITY BIN by default Port Defines the communication port used possible values dependent on the type of communication of the device and or available ports in the PC AutoDetect It is used for verifying the device communication over the serial port selected above Instrument Name Allows you to set the custom name of the instrument This name entered into the Value column will be used ...

Page 23: ...Teledyne Foxy 200 fraction collector The Teledyne Foxy 200 fraction collector supports two racks but both settings can be read from the fraction collector itself by using the Autodetect button Note The setting of the racks to be used is performed in the Method A of the fraction collector and cannot be changed from the side of Clarity this is the limitation of the fraction collector communication p...

Page 24: ... by checking the Instrument Control checkbox on the Method tab of the Report Setup dialog Fig 12 Report Setup All of the parameters set in the Method Setup FC Fraction Table and Method Setup FC Vial Numbers tabs are reported as well as the custom FC Name and other parameters set in the DataApex UNI Setup dialog 20 ...

Page 25: ...ection should be edited or added COM1 echo on textmode on filename CommDrvCOM1_ D txt reset off Note Instead of COM1 type the communication port used to communicate with the Teledyne Foxy 200 fraction collector This port number is displayed when the FC Status button in the Method Setup FC dialog is invoked Note D or d in the filename parameter means that the log will be created separately for each...

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