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Seres OL TOPAZ Total Alkalinity Operator'S Manual Download Page 40

SOL-96.110.041 / 290621

TOPAZ Total Alkalinity

Maintenance

38

 

6.6. Manual Measurement and Calibration

Methods of

Calibration

The TOPAZ Total Alkalinity supports two methods of calibration: A 

standard calibration or an online calibration. Seres OL recommends 

to use the standard calibration. 

If you want to use the online calibration, contact customer service for 

details.

Entering the

maintenance

menu

1

To stop the current measuring cycle, press the   button on the 

main screen and enter the password “0712”. In the next dialog, 

confirm with “OK”.

2

From the main screen, open the <TOOLS> tab and press the 

<Maintenance>

 

button.

The <MAINTENANCE> menu shows the following entries:

MEASURE

DIAGNOSTIC

+

TOOLS

Maintenance

Electrical test

Maintenance

Maintenance

Electrical test

MAINTENANCE

DIAGNOSTIC

Stopped

Zero calibration

Calibration

Calibration in line

Manual Measure

Summary of Contents for TOPAZ Total Alkalinity

Page 1: ...TOPAZ Total Alkalinity Operator s Manual TOPAZ Total Alkalinity SOL 96 110 041 290621...

Page 2: ...staff of technical specialists around the world For any technical question contact your nearest Seres OL representa tive or the manufacturer Seres OL SAS ZA de la Sipi re 219 Avenue de Provence FR 13...

Page 3: ...tions on I O Board 14 3 4 2 Cable thicknesses 18 3 4 3 AC power 19 3 4 4 Jbus via RS485 20 3 4 5 Jbus via TCP IP Option 21 4 Startup 22 4 1 Installing the Reagent Bottles 22 4 2 Starting Sample Flow 2...

Page 4: ...kalinity 2 6 6 3 Standard Calibration 40 6 7 Longer Stop of Operation 41 7 Configuration of the Analyzer 42 8 Troubleshooting 46 8 1 What To Do If 46 8 2 List of Errors and Alarms 50 8 3 Saving Diagno...

Page 5: ...safety instructions are given throughout this manual at the respective locations where observation is most important Strictly follow all safety instructions in this publication Target audience Operato...

Page 6: ...llow the prevention instructions carefully WARNING Severe injuries or damage to the equipment can occur if such warnings are ignored Follow the prevention instructions carefully CAUTION Damage to the...

Page 7: ...290621 TOPAZ Total Alkalinity Safety Instructions 5 Warning signs The warning signs in this manual have the following meaning Electrical shock hazard Corrosive Harmful to health Flammable Hot surface...

Page 8: ...accordance with the local regula tions of the respective country WARNING Electrical shock hazard If proper operation is no longer possible the instrument must be disconnected from all power lines and...

Page 9: ...alyzer and check it for visible damage If the analyzer shows any visible damage do not connect it to power and contact customer service immediately 1 4 International Symbols Used The symbols found on...

Page 10: ...he following configurations Three measuring ranges 5 to 50 ppm CaCO3 10 to 200 ppm CaCO3 10 to 500 ppm CaCO3 Available with one two four or six measuring channels common measuring range Signal outputs...

Page 11: ...nnel soft tubing D INT 12 Sample requirements Flow rate Temperature Inlet pressure Outlet pressure Particle size min 30 l h opt 40 l h 5 40 C 0 1 2 bar pressure free 20 m Air cleaning Inlet Required a...

Page 12: ...21 TOPAZ Total Alkalinity Product Description 10 Wall cabinet Material Screws Weight Protection degree Stainless steel SS316L 4x M6 6x M6 with reagent shelf 35 kg IP55 Reagent shelf made of SS316L ava...

Page 13: ...t Description 11 2 2 Instrument Overview A B C D E F G H I J K Power switch Touchscreen Cable glands Peristaltic pumps Photometer Air cleaning inlet Pressure reducing device Calibration vessel Sample...

Page 14: ...cifica tions p 9 3 2 Mounting the Wall Cabinet Mounting requirements Mount the instrument in vertical position The display should be at eye level to simplify operation and maintenance For dimensions s...

Page 15: ...ate the instrument from a power outlet which has a protec tive earth connection Overview of electrical connections 1 In multi channel instruments there is an I O board for each measuring channel The I...

Page 16: ...used to control internal components of the analyzer Do not connect anything else to these contacts Analog signal output OUT_ANA2 is reserved for customized versions of the analyzer that provide a sec...

Page 17: ...Leave pins 1 and 4 unconnected Analog signal outputs 4 20 mA Name Available on Description IN_DIG1 all measuring channels Activates or deactivates the measuring channel Open contact Measuring channel...

Page 18: ...f the Analyzer p 42 Name Available on Description OUT_DIG2 all measuring channels Sample flow alarm OUT_DIG3 all measuring channels Threshold 1 OUT_DIG4 all measuring channels Threshold 2 OUT_DIG5 all...

Page 19: ...be configured as normally open or normally closed by setting the corresponding jumpers on the I O board The default setting is normally open jumper in the right position A Location of jumpers on I O b...

Page 20: ...Alkalinity Installation 18 3 4 2 Cable thicknesses In order to comply with IP55 use the following cable thicknesses Note Seal cable glands that are not in use A B Outer diameter of cable 7 5 13 mm Ou...

Page 21: ...TOPAZ Total Alkalinity Installation 19 3 4 3 AC power Ferrite Wrap the mains cable two times around the supplied ferrite A B C Protective earth PE terminal 3 Neutral conductor terminal 2 Phase conduc...

Page 22: ...SOL 96 110 041 290621 TOPAZ Total Alkalinity Installation 20 3 4 4 Jbus via RS485 Terminals Terminal 1 data B terminal 2 data A A RS485 interface A...

Page 23: ...analyzer The connection is made via the Ethernet port located on the right side of the analyzer exterior Mount the supplied connector onto the Ethernet cable and connect it to the port Addressing mod...

Page 24: ...le This will prevent the tube ends from lying flat on the bottom of the bot tles 2 Check that there are two holes in the lid of each reagent bottle one hole to feed the reagent tube through and one sm...

Page 25: ...TOPAZ Total Alkalinity Startup 23 4 2 Starting Sample Flow Open the sample tap C so that a part of the sample overflows into the pressure reduction device A A B C Pressure reduction device Inner tube...

Page 26: ...umps are automatically readjusted and the panel PC starts 2 Stop the measuring cycle by pressing the button and entering the password 0712 3 Open the TOOLS tab and press the Electrical test button Che...

Page 27: ...OFF 6 Open the PUMPS tab 7 Press the ON button next to P1 TAC 8 Let the pump run until the fluid has reached the photometer and there is no more air in the tube This takes approximately 2 5 minutes T...

Page 28: ...the ACTUATOR tab 11 Set SV Emptying to ON and SV Filling to OFF and wait until the instrument is empty 12 Remove the lid from the photometer 13 Check that the stirrer bar is turning 14 Reinstall the l...

Page 29: ...is necessary 2 Calibrate the analyzer if required For detailed descriptions see Manual Measurement and Calibration p 38 4 6 Programming Program the following parameters if applicable Concentration val...

Page 30: ...fined access levels User access Allows viewing data in the main window Access with extended permissions Allows stopping the measurement changing settings and performing maintenance tasks The password...

Page 31: ...last manual measurement C Measured value D Trend E Measuring cycle information Stream that is being measured Number and description of step in measurement cycle Total number of steps to be completed...

Page 32: ...tion is needed If necessary calibrate the instrument Every 3 months Replace all peristaltic pump tubes After replacement of peristaltic pump tubes perform a manual measurement with a standard solution...

Page 33: ...et tap is open To avoid chemical reactions in the photometer flush the reagent tubes one after the other not simultaneously Proceed as follows 1 Remove all reagent tubes from their bottles and place t...

Page 34: ...the ACTUATOR tab and set SV Filling to ON 7 Wait until the photometer has been filled with fresh water Then set SV Filling to OFF ON ON ON ON OFF OFF OFF OFF Stirrer SV Emptying Heating SV Filling ACT...

Page 35: ...t interval approximately 0 6 liters of TAC indicator is consumed per month The consumption of sulfuric acid is proportional to the measured total alkalinity The consumption is 10 liters per month in t...

Page 36: ...Maintenance 34 Reagent tube numbering No Reagent type 11 TAC indicator PTFE 1 6 3 2 12 TAC indicator PTFE 1 6 3 2 21 Sulfuric acid PTFE 1 6 3 2 22 Sulfuric acid PTFE 1 6 3 2 1 2 11 12 22 21 U1 V1 SVB...

Page 37: ...SVB NC Silicone 5 8 Calibration vessel B SVB NO Silicone 5 8 SVB C Sample inlet right of photometer D Silicone 5 8 Water fault sensor U1 Silicone 2 5 Photometer sample outlet left SVA NC Tygon 5 8 SVA...

Page 38: ...ls Wear appropriate protective equipment gloves glasses protective clothing 1 Flush the reagent tubes with deionized water as described in Stop of Operation for Maintenance p 31 2 Turn the power switc...

Page 39: ...oll the tube around the rotor while turning it 6 Connect the other tube end to the left side fitting 7 Install the front cover on the pump 8 Insert the reagent tubes all the way to the bottom of the c...

Page 40: ...ation contact customer service for details Entering the maintenance menu 1 To stop the current measuring cycle press the button on the main screen and enter the password 0712 In the next dialog confir...

Page 41: ...ssel A with the standard 3 Wait until the calibration vessel is empty and the message Add standard appears again 4 Repeat steps 2 and 3 until the measurement starts automatically 5 When the measuremen...

Page 42: ...mple stream 1 Procedure The procedure is similar to the manual measurement procedure described in Manual Measurement p 39 Begin calibration by entering the reference value of the standard used Pay att...

Page 43: ...eed as follows 1 Prime the reagent system with deionized water as described in Stop of Operation for Maintenance p 31 2 Clean the photometer thoroughly with diluted hydrochloric acid Note Do not use a...

Page 44: ...o so by Seres OL customer service pressure setting Setpoint of the water fault sensor Adjust this value only if instructed to do so by Seres OL customer service Gain setpoint Setpoint of the electroni...

Page 45: ...tween mea surement cycles Note Since the analyzer is designed for continuous operation a maximum duration of 15 minutes is recommended for pauses 1 Press the Add button and select one of the following...

Page 46: ..._DIG3 and OUT_DIG4 are high or low thresholds The combinations high high low high and low low are possible The threshold values can be set in the parameter menu see 45 DATE TIME tab Set time and date...

Page 47: ...eshold value is made in the THRESHOLD tab of the OPTIONS menu Threshold 2 Threshold value for relay OUT_DIG4 The definition as high or low threshold value is made in the THRESHOLD tab of the OPTIONS m...

Page 48: ...error message Water default although there is sample flow Possible cause Corrective action No power on the socket Check mains power supply Power supply defective Check output voltage of the internal 2...

Page 49: ...r Emptying solenoid valve SVA does not switch Check that the solenoid valve is plugged in correctly If necessary change the membrane Possible cause Corrective action Pump does not work properly Check...

Page 50: ...has passed or if the reagents have been stored incorrectly If necessary replace the reagents Check that the reagents are of Analysis Use quality ask supplier Tubes connected to the wrong reagent cont...

Page 51: ...em is working correctly if present If no filter system is installed it might be necessary to install one Water does not drain Check that the drain is pressure free and not blocked Check condition of e...

Page 52: ...ain If the error persists contact customer support 5 Error reading cycle zero configuration Reset analyzer configuration to factory defaults by pressing the Recover button in the tab 6 Error writing c...

Page 53: ...e Live optical measure value in the DIAGNOSTIC tab With a functioning measuring card the value changes continuously If the value does not change restart the analyzer and check again If the error persi...

Page 54: ...n the INPUT tab and test the digital inputs If the error persists contact customer support 20 Error reading on IO card Check if all I O boards work properly Navigate to TOOLS Electrical test Open the...

Page 55: ...er button in the tab 25 Error reading on JBUS slave card Check request compliance with JBUS protocol 26 Error treatment on JBUS slave card Check request compliance with JBUS protocol 27 Error reading...

Page 56: ...sary replace the membrane Check sample tubes 33 Optical setting Default Info setting not received Observe the Live optical measure value in the DIAGNOSTIC tab With a functioning measuring card the val...

Page 57: ...o Concentration after linearization 0 or Calibra tion Coeff 0 Check if the calibration coefficient is equal to zero In this case make a new calibration Check if the final absorbance is equal to zero I...

Page 58: ...Value out of range Check that the analyzer is well calibrated check standard solution concentration by a manual measure cycle 45 Division by zero Absorbance 999998 0 Check that the optical fibers are...

Page 59: ...ct G 255 analyzer cannot adjust the optical gain Check that the optical fibers are well connected to their holder on the door Check that the photometer is not dirty Check that the analyzer is supplied...

Page 60: ...the USB stick into the USB port A on the back of the panel PC 3 Open the TOOLS tab and press the Log files copy button Enter the password 0712 if necessary 4 On the next screen press OK to start data...

Page 61: ...TOPAZ Total Alkalinity Notes SOL 96 110 041 290621 59 9 Notes...

Page 62: ...s O i l G a s Seres OL SAS FR 13730 Saint Victoret www seres ol com info seres ol com Seres OL Products Analytical Instruments for Seres OL is represented worldwide by subsidiary companies and distrib...

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