Quantum Turret 6 Manual & Product Overview Download Page 11

11

 

 

F.

   

DRY

 

GAS

 

TO

 

MINIMIZE

 

CONDENSATION

 

Dry

 

gas

 

flows

 

into

 

the

 

Turret 

6

 

via

 

the

 

stainless

 

1/8

inch

 

hose

 

barb

 

on

 

the

 

rear

 

side.

  

The

 

gas

 

passes

 

through

 

small

 

channels

 

in

 

the

 

base

 

of

 

the

 

Turret

 

body,

 

to

 

partially

 

equilibrate

 

in

 

temperature,

 

before

 

passing

 

up

 

through

 

small

 

holes

 

on

 

both

 

the

 

inside

 

and

 

outside

 

cuvette

 

surfaces.

  

A

 

flow

 

of

 

dry

 

gas

 

to

 

prevent

 

condensation

 

is

 

necessary

 

any

 

time

 

the

 

Turret 

6

 

is

 

controlled

 

below

 

the

 

dew

 

point

 

temperature

 

present

 

on

 

the

 

inside

 

of

 

the

 

sample

 

compartment

 

of

 

the

 

spectrometer.

  

For

 

ambient

 

air,

 

this

 

would

 

typically

 

be

 

about

 

5

 

°C.

 

G.

  

EXTERNAL

 

TEMPERATURE

 

PROBE

 

A

 

¼

inch

 

phone

 

jack

 

labeled

 

“Probe”

 

can

 

be

 

found

 

on

 

the

 

back

 

panel

 

of

 

TC

 

1

 

Temperature

 

Controller.

  

This

 

jack

 

will

 

accept

 

the

 

plug

 

on

 

a

 

standard

 

Series

 

400

 

or

 

Series

 

500

 

thermistor

 

probe.

  

When

 

a

 

probe

 

is

 

plugged

 

into

 

the

 

jack,

 

the

 

probe

 

temperature

 

is

 

presented

 

on

 

the

 

display

 

of

 

the

 

TC

 

1.

  

Place

 

the

 

probe

 

in

 

a

 

sample

 

to

 

measure

 

the

 

actual

 

temperature

 

of

 

the

 

sample,

 

which

 

will

 

lag

 

in

 

time

 

from

 

the

 

temperature

 

of

 

the

 

cuvette

 

tower.

 

 

We

 

do

 

not

 

sell

 

the

 

probe,

 

but

 

there

 

are

 

many

 

Series

 

400

 

and

 

500

 

probes

 

on

 

the

 

market.

  

Quantum

 

Northwest’s

 

preferred

 

probe

 

is

 

the

 

YSI

 

423

 

available

 

from

 

Cole

 

Parmer.

  

The

 

YSI

 

423

 

is

 

reasonably

 

resistant

 

to

 

immersion

 

and

 

responds

 

rapidly

 

to

 

temperature

 

changes.

  

Also,

 

the

 

fine,

 

coiled

 

wires

 

of

 

the

 

YSI

 

423

 

conduct

 

very

 

little

 

ambient

 

heat

 

to

 

the

 

thermistor

 

at

 

the

 

end.

 

 

Excellent

 

Series

 

500

 

probes

 

can

 

be

 

obtained

 

with

 

diameters

 

less

 

than

 

a

 

mm,

 

providing

 

access

 

to

 

small

 

volumes.

  

A

 

disadvantage

 

of

 

these

 

probes

 

is

 

that

 

they

 

are

 

not

 

pre

calibrated.

 

H.

  

EXTERNAL

 

COMPUTER

 

CONTROL

 

All

 

functions

 

may

 

be

 

accessed

 

either

 

through

 

a

 

Serial

 

(RS

 

232)

 

or

 

a

 

USB

 

located

 

on

 

the

 

back

 

of

 

TC

 

1

 

Temperature

 

Controller.

  

You

 

may

 

write

 

your

 

own

 

program

 

or

 

purchase

 

our

 

application

 

program

 

T

App.

  

T

App

 

will

 

plot

 

temperatures

 

of

 

the

 

probe,

 

cuvette

 

tower

 

or

 

even

 

the

 

Peltier

 

element

 

heat

 

exchanger

 

vs

 

time.

  

It

 

will

 

also

 

permit

 

you

 

to

 

set

 

up

 

temperature

 

ramps.

  

If

 

you

 

wish

 

to

 

do

 

your

 

own

 

programming,

 

please

 

see

 

the

 

Appendix

 

for

 

communication

 

instructions

 

and

 

the

 

set

 

of

 

text

 

commands

 

that

 

may

 

be

 

used

 

and

 

responses

 

to

 

the

 

commands.

 

 
 

4.

  

ERROR

 

CODES

 

When

 

errors

 

occur,

 

the

 

line

 

1

 

of

 

the

 

display

 

presents

 

an

 

error

 

code.

  

Line

 

3

 

of

 

the

 

display

 

identifies

 

the

 

error

 

and

 

line

 

4

 

of

 

the

 

display

 

presents

 

possible

 

solutions.

 

The

 

most

 

common

 

events

 

that

 

cause

 

errors

 

to

 

be

 

displayed

 

are

 

loose

 

cables

 

or

 

inadequate

 

coolant

 

flow.

  

For

 

errors

 

not

 

easily

 

solved,

 

please

 

contact

 

us

 

through

 

our

 

website,

 

www.qnw.com.

 

E5–

 

cell

 

out

 

of

 

range

 

warnings:

 

loose

 

cable,

 

sensor

 

failure

 

The

 

temperature

 

controller

 

is

 

not

 

receiving

 

a

 

reasonable

 

response

 

from

 

the

 

sensor

 

on

 

the

 

cuvette

 

tower.

  

Either

 

the

 

sensor

 

has

 

failed

 

or

 

a

 

cable

 

is

 

not

 

making

 

a

 

good

 

connection.

 

Summary of Contents for Turret 6

Page 1: ...19 8606 Tel 509 624 9290 Fax 509 624 9488 E mail quantum qnw com Web www qnw com Turret 6 6 Position Temperature Controlled Cuvette Turret for UV Vis Spectrophotometry Manual Product Overview 3 18 201...

Page 2: ...g the MenU BUTTON 6 3 Features of the Turret 6 8 A GENERAL DESCRIPTION 8 B CUVETTE HOLDER 9 C CUVETTE Z HEIGHT 9 E COOLING WATER FOR THE PELTIER 10 F DRY GAS TO MINIMIZE CONDENSATION 11 G EXTERNAL TEM...

Page 3: ...spectrophotometer 2 TC 1 Temperature Controller 3 power cable 4 USB cable 5 6 magnetic stir bars 6 vinyl tubing to connect water and gas B DEPENDING ON YOUR ORDER THE SHIPMENT MAY ALSO CONTAIN BATH 1...

Page 4: ...to the back of the TC 1 Temperature Controller on the 15 pin connectors labeled Sample and reference 5 Plug the power cable into the back of the TC 1 Temperature Controller and into a wall socket The...

Page 5: ...age push the left arrow once to get to the Set Position page Once there use the top and bottom arrows to choose a position e g position 5 Press the SET button The cuvette holder will move to position...

Page 6: ...lowly When it has locked onto a new target temperature the green LED will remain lit A rapidly flashing red LED usually means a loose electrical cable or inadequate water flow for the Peltier unit Not...

Page 7: ...own arrows and press SET The page will update to show the Current rate in min to be the same as the Ramp rate With ramping set turning on temperature control will generate a linear ramp to the target...

Page 8: ...to six cuvettes The center of the tower is hollow permitting light to pass into the entrance hole through the tower through a cuvette and exit the opposite side from the entrance A plastic cover enclo...

Page 9: ...be light tight CAUTION Accidently attaching a water line to the dry gas barb will severely damage the instrument Attach the lines with care B CUVETTE HOLDER The Turret 6 holds standard 10 x 10 mm cuve...

Page 10: ...tap for brief use You will need a flow of 100 300 ml minute This flow should require a pressure of about 3 5 psi 0 2 0 3 bar Do not exceed an input water pressure of 25 psi 1 7 bar as damage may occu...

Page 11: ...to temperature changes Also the fine coiled wires of the YSI 423 conduct very little ambient heat to the thermistor at the end Excellent Series 500 probes can be obtained with diameters less than a mm...

Page 12: ...he temperature controller is not receiving a reasonable response from the sensor on the heat exchanger Either the sensor has failed or a cable is not making a good connection E8 inadequate coolant war...

Page 13: ...10 C temperature precision 0 05 C cuvette size outside dimensions 12 5 x 12 5 mm minimum cuvette height 30 mm magnetic stirring speed 0 to 1700 rpm cuvette z height 8 5 or 15 mm specified when orderin...

Page 14: ...be established through a USB connection between the computer and the controller In this case the controller includes electronics which convert the USB connection to a serial communications port Howeve...

Page 15: ...stirrer speed F1 MS 300 The lowest stirrer speed is 300 rpm F1 SS S 1000 Set stirrer speed to 1000 rpm F1 SS S 0 Turn stirrer off and set the speed to zero F1 SS Turn stirrer on and set it to the most...

Page 16: ...us F1 IS R The controller has been powered off and back on again 7 Current Sample Temperature F1 CT What is the current temperature of the holder F1 CT 22 84 The current temperature is 22 84 C F1 CT 3...

Page 17: ...n F1 PA Start automatic reporting of probe temperature every temperature increment set by the command above F1 PT 30 5 The current probe temperature is 30 5 degrees F1 PA Stop automatic reporting of p...

Page 18: ...l send a response of the form F1 TT as a notification of the end of the ramp This response can be blocked at any time by previously sending the command F1 TT see command class 5 11 Heat Exchanger Temp...

Page 19: ...buttons and the display on the front When a computer program is in use the TC 1 will automatically send reports to the program whenever a manual change has been made The commands in this section are i...

Page 20: ...20 R1 TT R Stop reporting manual changes for the reference target temperature R1 RR R Stop reporting manual changes for the reference ramp...

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