PerkinElmer AAnalyst 700 User Manual Download Page 101

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0993-5255

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Introduction . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

6-3

Operating conditions . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

6-3

Space requirements for the spectrometer system . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

6-5

Electrical requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

6-8

Gas supply requirements . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .

6-9

Burner gases . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-10
Furnace gases . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . 6-14

Cooling the spectrometer system   . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .  6-16
Lamps . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .  6-18
Computer and printer . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . . .  6-18

Laboratory Requirements

6Laboratory Requirements

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Contents

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Summary of Contents for AAnalyst 700

Page 1: ...ATOMIC SPECTROMETRY User s Guide AAnalyst 700 Atomic Absorption Spectrometer Return to Document Menu...

Page 2: ......

Page 3: ...ATOMIC SPECTROMETRY AAnalyst 700 Atomic Absorption Spectrometer User s Guide...

Page 4: ...that is protected by copyright All rights are reserved No part of this document may be reproduced in any form whatsoever or translated into any language without the prior written permission of Perkin...

Page 5: ...ty practices for flame atomization 1 16 Safety practices for electrothermal atomization 1 22 Safety practices for FIAS and mercury hydride systems 1 24 References for laboratory safety practice 1 26 R...

Page 6: ...onnections 2 22 Chapter 3 Preparing the System for Analyses Switching on the system 3 3 Installing lamps 3 7 Installing sample trays 3 11 Shutting down the system 3 12 Emergency shutdown 3 14 Chapter...

Page 7: ...ner gases 6 10 Furnace gases 6 14 Cooling the spectrometer system 6 16 Lamps 6 18 Computer and printer 6 18 Chapter 7 Spectrometer System Description The AAnalyst 700 Spectrometer System 7 3 The optic...

Page 8: ...Contents C 4 0993 5255...

Page 9: ...for electrothermal atomization 1 22 Safety practices for FIAS and mercury hydride systems 1 24 References for laboratory safety practice 1 26 Regulatory information 1 27 IEC 1010 compliance 1 27 Elect...

Page 10: ...1 2 0993 5255...

Page 11: ...ed does not cover every safety procedure that should be practiced Ultimately maintenance of a safe laboratory environment is the responsibility of the user and the user s organization Possible hazards...

Page 12: ...ent in a manner not specified in the guide or if you use it for a purpose other than that intended you may damage the instrument or compromise your own or someone else s safety This instrument should...

Page 13: ...PerkinElmer service engineer or similarly trained and authorized person should be permitted to service the instrument Do not attempt to make adjustments replacements repairs or modifications to this...

Page 14: ...ible damage Fails to perform the intended measurement Has been subjected to prolonged storage under unfavorable conditions Has been subjected to severe transport stresses Note The spectrometer is prov...

Page 15: ...he location must be free of dust smoke and corrosive fumes You can store the instrument safely under the following conditions Ambient temperature 20 C to 60 C 4 F to 140 F Ambient relative humidity 20...

Page 16: ...smoking in the work area Smoking is a source of significant contamination and also a potential route for ingesting harmful chemicals Do not store handle or consume food in the work area Laboratory ven...

Page 17: ...ropriate eye protection at all times while handling chemicals Depending on the types of chemicals you are handling wear safety glasses with side shields or goggles or a full face shield Wear suitable...

Page 18: ...mental regulatory requirements Please note that PerkinElmer does not take back defective lamps for disposal In addition hollow cathode lamps and deuterium lamps are maintained under reduced pressure H...

Page 19: ...fically instructed to do so in the guide since otherwise you may be exposed to potentially hazardous UV radiation Always wear UV absorbing eye protection when viewing any of these sources The flame es...

Page 20: ...t has cooled to room temperature Do not attempt to inject a sample into the graphite tube when the furnace is hot You may be subjected to fumes from the sudden vaporization of the sample and may damag...

Page 21: ...ng detailed information on the potential hazards associated with the gas Identifying cylinders Legibly mark cylinders to clearly identify the contents and status full empty etc Use the chemical name o...

Page 22: ...strike or fall against them Use and store cylinders away from exits and exit routes Locate gas cylinders away from heat sources including heat lamps Compressed gas cylinders should not be subjected to...

Page 23: ...ck Use only approved regulators tubing and hose connectors Arrange gas hoses where they will not be damaged or stepped on and where things will not be dropped on them Do not attempt to refill gas cyli...

Page 24: ...connections constitutes a serious fire hazard Make sure that there are no breaks or leaks in any of these systems and that all the seals are correctly installed and in good condition Regularly check...

Page 25: ...ir can cause a flashback of the flame Never use oxygen as the oxidant since this can cause an explosion Nitrous oxide dinitrogen monoxide N2O Tubing and fittings carrying nitrous oxide must be free of...

Page 26: ...ck for the presence of acetylene in the laboratory atmosphere especially near the ceiling For acetylene set an outlet gauge pressure of between 90 kPa and 100 kPa 0 9 1 0 bar 13 14 5 psig Never allow...

Page 27: ...oor is closed The pH of the liquid in the drain vessel is greater than pH 10 if you intend to aspirate cyanide solutions Do not leave the flame unattended Always make sure that there is a fire extingu...

Page 28: ...m Check the condition of the drain tube regularly especially if you use organic solvents Replace the drain tube when it first shows signs of cracking or discoloration Flashbacks A flashback is an expl...

Page 29: ...mizer compartment door closed when the flame is burning and never directly view the flame unless you are wearing UV absorbing glasses Acetylides If you have aspirated high concentrations of copper sil...

Page 30: ...ise your own or someone else s safety Inert gas The graphite furnace requires a supply of inert gas PerkinElmer recommends argon Although nitrogen can be used it is not recommended for the inert gas s...

Page 31: ...duced when the furnace temperature is above 2300 C High temperatures The HGA graphite furnace can generate temperatures of up to 3000 C To avoid serious burns never touch the graphite components until...

Page 32: ...ory fume ventilation system is operating The tubing in the fluid system is not constricted since this could lead to a pressure build up in the system The drain tubing is inserted in the waste containe...

Page 33: ...igh temperatures The QTA cell used for the hydride generation technique can reach temperatures of up to 1000 C Do not touch any part of the heating mantle electrically heated systems or the cell holde...

Page 34: ...edition Furr K ed The Chemical Rubber Co Press Florida USA 1990 Prudent Practices for Handling Hazardous Chemicals in Laboratories National Research Council National Academic Press Washington D C USA...

Page 35: ...96 IEC 1010 2 061 1995 Particular requirements for laboratory atomic spectrometers with thermal atomization and ionization Electrical protection Insulation Class I as defined in IEC 1010 1 Installatio...

Page 36: ...found to comply with the limits of a Class A digital device pursuant to Part 15 of the FCC Rules These limits are designed to provide reasonable protection against harmful interference when the equipm...

Page 37: ...symbol indicates the risk of hot surfaces This symbol indicates the off position of the main power switch or circuit breaker With the switch in this position the instrument is disconnected entirely fr...

Page 38: ...nes parties en mouvement de l instrument sont accessibles en fonctionnement normal Tenir les mains v tements et autres objets loign s des parties en mouvement de l instrument Warnung Bewegliche Teile...

Page 39: ...the moving parts of the instrument Danger Parties en mouvement Risque d accident corporel Certaines parties en mouvement de l instrument sont accessibles en fonctionnement normal Tenir les mains v te...

Page 40: ...B ren nerga se 90 0 9 13 0 100 1 0 14 5 kP a bar psig Furnace Gases G az du Fo ur O fen gase Pmi n 350 3 5 50 0 P max 400 4 0 58 0 kP a bar psig Special Gas Gaz Sp cial Spezialgas Normal Gas Ar N2 Ga...

Page 41: ...is utiliser d oxyg ne ou d air suroxyg n avec les syst mes de br leurs PerkinElmer N utiliser que l air comprim Warnung Sauerstoff und mit Sauerstoff angereicherte Luft Verwenden Sie f r PerkinElmer B...

Page 42: ...a bar psig Pmi n Pmi n Pmi n 450 4 5 65 0 Pmax Pmax Pmax 500 5 0 72 5 kP a bar psig A l l f i e l d w i ri ng mus t hav e i ns ul a t i on sui t abl e f o rat l e ast 3 00 V Le ca bl age pi ed d ou v...

Page 43: ...operates at high voltage To avoid electrical shock disconnect the line power cord before opening the cover Risque d lectrocution Pout viter les chocs lectriques d brancher le cordon d alimentation av...

Page 44: ...Safety Regulatory Information 1 36 0993 5255...

Page 45: ...spectrometer 2 5 Reinstalling the spectrometer 2 6 Connecting the burner gases 2 7 Connecting the furnace gases 2 10 To connect the drain system to the burner 2 15 To install the furnace autosampler...

Page 46: ...Spectrometer Installation 2 2 0993 5255...

Page 47: ...on system and the necessary gas supply lines and regulators are installed Although you should not perform the initial installation yourself we recommend that you read the installation instructions to...

Page 48: ...ransport the spectrometer over a longer distance contact your local PerkinElmer office since internal shipping locks must be set via the service software inside the spectrometer Preparing the spectrom...

Page 49: ...ting techniques and always use the handles to lift or move the instrument Caution Risk of damage to the instrument The spectrometer is a precision optical instrument Move the spectrometer very careful...

Page 50: ...e will be enough space at the rear and sides of the spectrometer system for air to circulate freely 2 Remove the handles Save the handles and screws Insert the plastic plugs provided B015 3803 into th...

Page 51: ...ectrometer Gas hose assemblies for acetylene air and nitrous oxide The fittings on the gas hose assemblies are suitable for connection to most commercially available pressure regulators These are R 3...

Page 52: ...Air Luft on the rear panel of the spectrometer Nitrous oxide 1 Make sure that the nitrous oxide supply is turned off 2 Use the blue N2O hose assembly to connect a source of clean dry nitrous oxide to...

Page 53: ...a bar psig Speci al Gas Gaz Sp cial Spezi algas Normal G as Ar N 2 G az Normal Normalgas 450 4 5 65 0 500 5 0 72 5 kPa bar psi g Pmin Pmin Pmin 450 4 5 65 0 Pma x Pma x Pma x 500 5 0 72 5 kPa bar psig...

Page 54: ...gas The gases must conform with the requirements listed in Chapter 6 Laboratory Requirements Suitable pressure regulators and on off valves near to the spectrometer for the inert and special gas suppl...

Page 55: ...adapter suitable for the gas regulator Make sure that all the connections are secure 4 Pass the gas tube to the rear of the spectrometer Make sure that it cannot be damaged or strained 5 Push the two...

Page 56: ...bar psig Speci al Gas Gaz Sp cial Spezi algas Normal G as Ar N 2 G az Normal Normalgas 450 4 5 65 0 500 5 0 72 5 kPa bar psi g Pmin Pmin Pmin 450 4 5 65 0 Pma x Pma x Pma x 500 5 0 72 5 kPa bar psig...

Page 57: ...regulators Use the R screw connectors provided or use a connector or adapter suitable for the gas regulator Make sure that all the connections are secure 4 Pass the gas tubes to the rear of the spectr...

Page 58: ...400 4 0 58 0 kPa bar psig Speci al Gas Gaz Sp cial Spezi algas Normal G as Ar N 2 G az Normal Normalgas 450 4 5 65 0 500 5 0 72 5 kPa bar psi g Pmin Pmin Pmin 450 4 5 65 0 Pma x Pma x Pma x 500 5 0 72...

Page 59: ...ing the drain system to the burner are described in Maintaining the drain system in the Burner System User s Guide To install the furnace autosampler Procedures for demounting and reinstalling the fur...

Page 60: ...he floor underneath the spectrometer Do not place the cooling system on the same bench as the spectrometer since vibrations can adversely influence the spectrometer Make sure that You can reach the on...

Page 61: ...0 1 00 1 0 1 4 5 kPa b ar psig Furnace Gases Gaz du Four Ofengase Pmin 350 3 5 50 0 Pmax 400 4 0 58 0 kPa bar psi g Sp ecial G as Gaz Sp cial Sp ezialg as No rma l Gas Ar N2 Gaz No rm al No rma lg as...

Page 62: ...tains 0 5 L glycerol when it leaves the factory See Cooling system maintenance procedures in the Graphite Furnace User s Guide for the procedure to follow when you empty and refill the cooling system...

Page 63: ...ressure is as given in Table 2 1 Figure 2 5 Connecting the Main Water Supply A water hose kit with pressure relief valve is provided with the spectrometer system which you must install in the water su...

Page 64: ...eer will connect the pressure relief valve to the water tap faucet 2 Make sure that the drain hose from the pressure relief valve hangs down into a suitable laboratory sink or drain 3 Connect the inle...

Page 65: ...5 0 kPa b ar psig Instrume nt Commu n icatio n Cooling System S yst me de Refroidisse ment Umlaufk h lu ng 23 0 V 50 60 Hz 23 0 V 50 60 Hz 23 0 V 5 0 60 Hz F4 4 A T F3 4 A T F2 4 A T F1 4 A T 23 0 V 5...

Page 66: ...uments that you will connect to the spectrometer or computer See the guides for the individual instruments for the procedure to use 4 Disconnect the line power cords of the spectrometer and all other...

Page 67: ...4 A T 230 V 50 60 Hz Connections panel on the rear of the spectrometer Monitor Computer Communication cable Communication interface Printer Spectrometer line power cord Cooling system Use these power...

Page 68: ...Spectrometer Installation 2 24 0993 5255...

Page 69: ...on the system 3 3 Installing lamps 3 7 Installing sample trays 3 11 Shutting down the system 3 12 Emergency shutdown 3 14 Preparing the System for Analyses 3 3Preparing the System for Analyses Marker...

Page 70: ...Preparing the System 3 2 0993 5255...

Page 71: ...ly since air pressure is required for the internal pneumatic system If you intend to work with only one atomizer you only need to additionally turn on the gas supplies for that atomizer 6 Turn on the...

Page 72: ...such as installed a different autosampler or added or removed any accessories use the Reconfigure utility to reconfigure the software see the Online Help in AA WinLab 13 Start AA WinLab In the AA WinL...

Page 73: ...nce air pressure is required for the spectrometer s pneumatic system Table 3 1 Required Pressures for the Burner Gases Gas Outlet Gauge Pressure kPa bar psig Pmin Pmax Pmin Pmax Pmin Pmax Acetylene C2...

Page 74: ...Furnace Gases Gas Outlet Gauge Pressure kPa bar psig Pmin Pmax Pmin Pmax Pmin Pmax Argon 350 400 3 5 4 0 50 0 58 0 Nitrogen 350 400 3 5 4 0 50 0 58 0 Special 350 400 3 5 4 0 50 0 58 0 W6 1 Warning To...

Page 75: ...esigned to operate with PerkinElmer Lumina hollow cathode lamps HCLs and coded electrodeless discharge lamps EDLs The lamp compartment has holders for up to eight lamps You can install Lumina HCLs in...

Page 76: ...spectrometer 1 Open the lamp compartment cover by lifting it at the front and swinging it back 2 Slide the Lumina lamp for the required element into the selected lamp holder and make sure that the int...

Page 77: ...nd make sure that the locking pin extends through the locating hole in the sleeve 3 Slide the lamp carefully into the selected lamp holder until it butts up against the end stop inside the holder 4 In...

Page 78: ...contamination can reduce the intensity of the radiation If you install more than one lamp containing a particular element for example a single element copper lamp and a multi element lamp containing c...

Page 79: ...to the standby position at the right you can install a tray in front of the atomizer compartment The sample trays are robust and can support an accessory such as a diluter or a flame autosampler or a...

Page 80: ...system see Extinguishing the flame in the Burner System User s Guide for detailed information Either aspirate the solutions manually or use the flame autosampler 2 Extinguish the flame and bleed the...

Page 81: ...accessories 4 If you do not want to use the computer for other tasks shut down the computer and printer as described in their user s guides 5 Empty the burner drain vessel see Emptying the drain vesse...

Page 82: ...you return to the spectrometer proceed as follows to shut down the system properly 3 If you were previously running concentrated salt solutions organic solvents or solutions containing cyanide copper...

Page 83: ...es 4 5 Cleaning the windows of the optical system 4 5 Maintaining the electrical components 4 7 Changing the air filters 4 10 Replacing the deuterium lamp 4 11 Maintaining the acetylene supply 4 14 Sp...

Page 84: ...System Maintenance 4 2 0993 5255...

Page 85: ...nochromator and all other optical system components Before the service engineer arrives 1 Make sure that the instrument and work area are clean 2 Empty corrosive solutions from the burner drain vessel...

Page 86: ...ime make sure that all the components are clean Fume ventilation Make sure that the main fume ventilation system functions correctly Always switch it on when you are using the instrument Environmen ta...

Page 87: ...tical parts that are exposed are The atomizer compartment windows The windows of the lamps The furnace windows Cleaning the furnace windows is described under System Maintenance in the Graphite Furnac...

Page 88: ...ir before you attempt to clean them Do not rub the surfaces 2 Clean the window surfaces with a soft lint free cloth moistened with spectroscopic grade alcohol The window must dry quickly to avoid leav...

Page 89: ...can maintain yourself If there is a problem contact your local PerkinElmer office If any fuses blow frequently or if the automatic circuit breaker switch is activated frequently contact your local Pe...

Page 90: ...on the rear panel of the spectrometer to the off position marked 3 Disconnect the spectrometer s line power cord from the line power supply 4 Disconnect all the line power cords from the sockets at t...

Page 91: ...Bruleur Brennergase 90 0 9 13 0 100 1 0 14 5 kPa bar psi g Furnace Gases Gaz du Four Ofengase Pmin 350 3 5 50 0 Pm ax 400 4 0 58 0 kPa bar psig Speci al Gas Gaz Sp cial Spezi algas Normal G as Ar N 2...

Page 92: ...ngang Out Out Sortie Sortie Ausgang Ausgang Pmin H O 2 Furnace Cooling Refroidissement du Four Ofenk hlung P 250 2 5 36 P Pmax 350 3 5 50 kPa bar psig C H 2 2 N O 2 Air Luft Burner Gases Gaz du Bruleu...

Page 93: ...replacement lamp is fitted in a prealigned mount Figure 4 2 Location of Deuterium Lamp inside the Spectrometer 1 Switch off the spectrometer at the operational on off switch on the front panel 2 Swit...

Page 94: ...rium lamp cover 2 Carefully lift up the deuterium lamp cover The deuterium lamp assembly is attached to a bracket underneath the cover 3 Carefully place the complete assembly on top of the black optic...

Page 95: ...ric and can only be inserted in one direction 11 Reinstall the lamp assembly 1 Carefully lower the deuterium lamp assembly into the lamp compartment until the lamp cover fits in place 2 Screw in the t...

Page 96: ...acetylene is dissolved in a solvent and a pressure of 600 kPa 6 bar 85 psig at ambient temperature indicates that the cylinder is nearly empty For this reason replace acetylene cylinders when the cyl...

Page 97: ...0993 5255 5 1 Parts provided 5 3 Replacement parts 5 4 Obtaining supplies replacement parts and accessories 5 4 Parts and Supplies 5 5Parts and Supplies Marker for header Contents page...

Page 98: ...Parts and Supplies 5 2 0993 5255...

Page 99: ...autosampler are listed under Parts and Supplies in the Graphite Furnace User s Guide 1 Fuel hose assembly red B015 4984 1 Air hose assembly black B015 4987 1 Nitrous oxide hose assembly blue B015 4990...

Page 100: ...der for supplies and many replacement parts request a free catalog or ask for information If you are located within the U S call toll free 1 800 762 4002 8 a m to 8 p m EST Your order will be shipped...

Page 101: ...the spectrometer system 6 5 Electrical requirements 6 8 Gas supply requirements 6 9 Burner gases 6 10 Furnace gases 6 14 Cooling the spectrometer system 6 16 Lamps 6 18 Computer and printer 6 18 Labo...

Page 102: ...Laboratory Requirements 6 2 0993 5255...

Page 103: ...Elmer Operating conditions The instrument will operate correctly under the following conditions Indoors Ambient temperature 15 C to 35 C 59 F to 95 F with a maximum change not exceeding 2 8 C 5 F per...

Page 104: ...tion the system so that the atomizer compartment is located beneath a suitable fume ventilation system Make sure that there is space at the rear and sides of the system for air to circulate freely Mak...

Page 105: ...stem The illustrations on the following pages show the dimensions of the spectrometer and the space that you require to accommodate the spectrometer computer and ancillary equipment Computer and print...

Page 106: ...0993 5255 Figure 6 1 Space Requirements for the Spectrometer System 1 865 mm 655 mm 565 mm approx 350 mm Fume ventilation Lamp compartment cover in open position Cooling system Atomizer compartment d...

Page 107: ...Laboratory Requirements 0993 5255 6 7 Figure 6 2 Space Requirements for the Spectrometer System 2 Atomizer Sample tray Furnace autosampler 330 mm 660 mm 260 mm 1095 mm...

Page 108: ...tween the electrical outlet and the instrument The power demand of the graphite furnace is approximately 3600 VA the maximum graphite tube temperature is 3000 C Monitoring of the energy required for e...

Page 109: ...supplies regulators connectors and valves A double stage or heated regulator is recommended for nitrous oxide Either the gas supplier or PerkinElmer can supply the correct regulators and valves You mu...

Page 110: ...er set the outlet pressure to a value exceeding the maximum pressure Pmax Table 6 1 Specifications and Requirements of the Burner Gases Gas Purity Outlet Gauge Pressure kPa bar psig Pmin Pmax Pmin Pma...

Page 111: ...mpressor meeting the air supply requirements is recommended The use of an air dryer filter is strongly recommended to remove entrained water oil water aerosols and solid particles from compressed air...

Page 112: ...hours Flash Arrestor PerkinElmer recommends the use of the Flash Arrestor P N N930 0068 The flash arrestor provides a positive shutoff of gas by checking the reverse flow under all conditions It also...

Page 113: ...oxide is rapidly removed from the cylinder the expanding gas causes cooling of the cylinder pressure regulator and the regulator diaphragm can freeze This can create erratic flame conditions or in the...

Page 114: ...at temperatures above 2000 C Nitrogen can also react with the samples and the graphite tube at typical atomization temperatures Special gas For some applications you may want to use a special gas A t...

Page 115: ...a value exceeding the maximum pressure Pmax Table 6 2 Specifications and Requirements of the Furnace Gases Gas Purity Outlet Gauge Pressure Max Flowrate kPa bar psig L min Pmin Pmax Pmin Pmax Pmin Pm...

Page 116: ...ater see Cooling the furnace in the Graphite Furnace User s Guide This cooling system includes a pressure sensitive safety device that opens a bypass if the internal pressure in the circulatory system...

Page 117: ...of damage to the water hoses and hose fittings in the system through excess water pressure The water pressure to the system should be at least 2 5 bar 36 psig If the pressure is lower the flow rate o...

Page 118: ...for Atomic Absorption contains descriptions of all the lamps that are available This brochure is available from PerkinElmer Computer and printer PerkinElmer offers a suitable computer for controlling...

Page 119: ...lyst 700 Spectrometer System 7 3 The optical system 7 6 Switches and connectors on the spectrometer 7 8 Technical data 7 14 Spectrometer System Description 7 7Spectrometer System Description Marker fo...

Page 120: ...Spectrometer System Description 7 2 0993 5255...

Page 121: ...res of the AAnalyst 700 System Double beam optical system optimized for maximum radiation throughput Two fully integrated atomizers a burner system for flame atomization and a graphite furnace for ele...

Page 122: ...design in the Graphite Furnace User s Guide for more information The optional furnace cooling system see Cooling the furnace in the Graphite Furnace User s Guide for more information The computer and...

Page 123: ...scription 0993 5255 7 5 Accessories PerkinElmer offers autosamplers for operation with the burner system flow injection systems diluters and much more Please contact your local PerkinElmer office to o...

Page 124: ...reference beam passes around the atomizer and is conducted by a fiber optic The sample and reference beams are measured simultaneously The Littrow configuration monochromator has a large area reflect...

Page 125: ...on 0993 5255 7 7 Figure 7 1 Optical System Lamp holder with positions for up to 8 source lamps Movable mirror Deuterium lamp Atomizer Beam splitter Slits Detector Grating Collimating mirror Fiber opti...

Page 126: ...on off switch on the front panel of the spectrometer Note The spectrometer is provided with an operational on off switch and with a circuit breaker The operational on off switch turns the instrument o...

Page 127: ...nal power source You can leave the on off switch on the cooling system in the on position since the system is controlled from the spectrometer Accessory ports Three accessory ports are located on the...

Page 128: ...ot connect other equipment to this power outlet 4 230 V 50 60 Hz Power outlet for a printer 5 230 V 50 60 Hz Power outlet for a computer 6 230 V 50 60 Hz Power outlet for a monitor 7 Circuit breaker A...

Page 129: ...Ar N2 Gaz Normal Normalgas 450 4 5 65 0 500 5 0 72 5 kP a bar psig Pmi n Pmi n Pmi n 450 4 5 65 0 Pmax Pmax Pmax 500 5 0 72 5 kP a bar psig A l l f i e l d w i ri ng mus t hav e i ns ul a t i on sui...

Page 130: ...the normal gas supply to the furnace argon or nitrogen 4 Special Gas Connector for the connection of the special gas supply to the furnace If you are not using a special gas you must also connect the...

Page 131: ...r Gases Gaz du Bruleur Brennergase 90 0 9 13 0 100 1 0 14 5 kPa bar psig Furnace Gases Gaz du Four Ofengase Pmin 350 3 5 50 0 Pmax 400 4 0 58 0 kPa bar psig Special Gas Gaz Sp cial Spezialgas Normal G...

Page 132: ...2 0 7 and 2 0 nm Wavelength range 190 870 nm Reciprocal linear dispersion 1 6 nm mm nominal Detector Segmented discrete solid state detector with CMOS charge amplifier array software controlled autom...

Page 133: ...zero or non zero intercept Analyte addition technique Zero or non zero intercept Additions calibrate zero intercept Application program Special application program AA WinLab Online help function Hard...

Page 134: ...nts of Canadian Standards Association CSA and Underwriters Laboratory UL as listed in File No LR 45111 Certificate of Approval and GS mark from the LGA Bavaria FRG Institute of Equipment Safety Testin...

Page 135: ...0993 5255 8 1 Translations of Warnings 8 3 Symbols used on the instrument 8 45 Translations of Warnings 8 8Translations of Warnings Marker for header Contents page...

Page 136: ...Translations of Warnings 8 2 0993 5255...

Page 137: ...n contiene traducciones de las advertencias utilizadas en el presente manual italiano Traduzione dei simboli di avvertenza La presente sezione contiene la traduzione dei simboli di avvertenza utilizz...

Page 138: ...s dommages corporels l utilisateur ou d autres personnes Les d tails sur ces circonstances sont donn es dans un encadr semblable celui ci italiano Questo simbolo segnala situazioni che possono generar...

Page 139: ...s dommages corporels l utilisateur ou d autres personnes Les d tails sur ces circonstances sont donn es dans un encadr semblable celui ci italiano Questo simbolo vi mette in guardia da folgorazione ch...

Page 140: ...corporels l utilisateur ou d autres personnes Les d tails sur ces circonstances sont donn es dans un encadr semblable celui ci italiano Questo simbolo vi mette in guardia da superfici molto calde che...

Page 141: ...l sions oculaires l utilisateur ou d autres personnes Les d tails sur ces circonstances sont donn es dans un encadr semblable celui ci italiano Questo simbolo vi mette in guardia da radiazione ultrav...

Page 142: ...ung Der Ausdruck CAUTION ACHTUNG warnt vor Situationen die eine ernste Besch digung des Ger ts oder anderer Systemteile zur Folge haben k nnen Einzelheiten dar ber sind auf die gleiche Weise wie diese...

Page 143: ...tandigheden worden beschreven in een mededeling gelijk aan portugu s Aten o O termo CAUTION ATEN O alerta para situa es que poder o causar danifica o do aparelho Detalhes referentes a estas circunst n...

Page 144: ...aturarbeiten oder Justierungen die in der Benutzerdokumentation zum Ger t nicht beschrieben sind d rfen nur vom PerkinElmer Kundendienst oder von entsprechend ausgebildeten und autorisierten Fachkr ft...

Page 145: ...everd is portugu s Aviso Trabalhos n o permitidos no aparelho Trabalhos de manuten o apenas podem ser executados pelo Servi o T cnico da PerkinElmer ou por pessoal especializado devidamente formado e...

Page 146: ...Translations of Warnings 8 12 0993 5255...

Page 147: ...as explosivas fran ais Danger Atmosph re explosive Cet instrument n est pas con u pour fonctionner dans une atmosph re explosive italiano Pericolo Atmosfera esplosiva Questo strumento non concepito pe...

Page 148: ...r schweren Last Das Ger t hat eine Masse von ca 150 kg Falsches Anheben kann schmerzhafte und unter Umst nden bleibende R ckensch den zur Folge haben Wenden Sie zum Anheben oder Bewegen des Ger ts nur...

Page 149: ...of verzet het instrument op de juiste manier portugu s Aviso Risco de ferimento ao levantar o aparelho O aparelho pesa aprox 150 kg O seu levantamento incorrecto poder causar ferimentos dolorosos e po...

Page 150: ...eller fjernelse af beskyttelseslederen jord stel kan g re apparatet farligt Bevidst afbrydelse er forbudt Der er livsfarlige sp ndinger i apparatet Selv n r hovedafbryderen er sl et fra kan der stadig...

Page 151: ...M me lorsque l interrupteur est sur arr t des tension r siduelles peuvent encore tre pr sentes dans l instrument Lorsque l instrument est reli au secteur les raccords peuvent tre sous tension et des p...

Page 152: ...an tevoorschijn komen Ook bij uitgeschakeld instrument en in een onderbroken netvoeding kunnen condensatoren in het instrument nog een gevaarlijke lading bevatten portugu s Aviso Perigo por electricid...

Page 153: ...kanssa poikkeuksena osat joihin p see k siksi ilman ty kaluja Laitteen sis ss olevat kondensaattorit voivat olla viel varautuneita vaikka laite olisikin kytketty irti kaikista j nnitel hteist svenska...

Page 154: ...Gef hrdung durch Elektrizit t Um Verletzungsgefahr durch elektrische Spannung und Besch digungsgefahr der Ger te zu vermeiden schalten Sie alle Ger te des Me platzes AUS und trennen Sie die Netzverbi...

Page 155: ...nstrumenten UIT en ontkoppelt U de netvoeding portugu s Aviso Perigo por electricidade A fim de evitar o perigo de ferimento por tens o el ctrica e o perigo de danifica o dos aparelhos DESLIGUE todos...

Page 156: ...Deutsch Warnung Gef hrdung durch elektrischen Strom Verwenden Sie nur Sicherungen des gleichen Typs und mit der angegebenen Belastbarkeit Verwenden Sie keine Behelfssicherung und schlie en Sie nicht...

Page 157: ...k geen noodzekeringen en sluit de zekeringhouders niet kort portugu s Aviso Perigo por electricidade Ao substitu los use apenas fus veis com a amperagem correcta e do tipo especificado N o use fus vei...

Page 158: ...Strahlung in unterschiedlicher St rke und k nnen dadurch Augensch den verursachen Nicht mit ungesch tzten Augen direkt in die leuchtenden Lampen schauen Tragen Sie eine Schutzbrille die die emittierte...

Page 159: ...t kijken portugu s Aviso Radia o UV perigo para os olhos As l mpadas emitem uma radia o UV com intensidades diferentes podendo assim provocar ferimentos aos olhos N o olhar directamente para uma l mpa...

Page 160: ...eindre de tr s hautes temp ratures Ne pas toucher la t te de br leur avant qu elle ait refroidi la temp rature ambiante italiano Pericolo Alte temperature Rischio di ustioni La testa del bruciatore pu...

Page 161: ...iculier les composants en graphite avant qu ils n aient refroidi la temp rature ambiante italiano Pericolo Alte temperature Rischio di ustioni Il forno a grafite pu generare temperature estremamente e...

Page 162: ...losionsgefahr Stellen Sie f r Acetylen keinen h heren Ausgangsdruck als 103 kPa 1 03 bar ein Bei h heren Dr cken kann Acetylen spontan zerfallen und explodieren espa ol Advertencia Acetileno Peligro d...

Page 163: ...n deze waarde uitkomt portugu s Aviso Acetileno perigo de explos o Se a press o for superior a 103 kPa 1 03 bar 15 psig o acetileno poder desintegra se de repente e explodir Assegure se de que o man m...

Page 164: ...stoff oder sogenannte Atemluft sind nicht zul ssig Bei Verwendung von Sauerstoff besteht Explosionsgefahr Mit Sauerstoff angereicherte Luft kann einen Flammenr ckschlag verursachen espa ol Advertencia...

Page 165: ...rslucht portugu s Aviso Retrocesso da chama Os sistemas de queimadores PerkinElmer s o concebidos para o uso com ar comprimido O uso de oxig nio poder causar uma explos o no sistema do queimador Ar en...

Page 166: ...Zustand explosionsartig zerfallen k nnen Sp len Sie nach dem Einbringen von L sungen mit hohen Silber Kupfer oder Quecksilbergehalten Brenner und Ablaufsystem gr ndlich mit entionisiertem Wasser durc...

Page 167: ...nc ndio e de explos o Podem formar se acetilas inst veis na c mara de pulveriza o quando se aspira solu es de prata cobre ou merc rio para uma chama de ar acetileno Em estado seco acetilas podem desin...

Page 168: ...g von Stickstoff als Inertgas bildet sich bei Ofentemperaturen ber 2300 C giftiges Dicyan CN 2 Es mu sichergestellt sein da die aus dem Graphitofen austretenden Abgase von der Haupt Absauganlage siche...

Page 169: ...de grafietoven komen door de hoofdafzuiging worden afgezogen portugu s Aviso G s de escape venenoso Ao utilizar nitrog nio como g s inerte a uma temperatura de forno superior a 2300 C forma se cianet...

Page 170: ...n giftige Blaus ure frei Wenn Sie cyanidhaltige L sungen messen m chten zuvor den pH Wert im Ablaufsystem und der Abfall sung auf ber 10 einstellen um sicherzustellen da keine Blaus ure freigesetzt we...

Page 171: ...giftig waterstofcyanidegas gevormd wordt portugu s Aviso G s de escape venenoso Em contacto com cidos as solu es de cianeto liberam g s cian drico t xico Antes de aspirar solu es de cianeto assegure...

Page 172: ...kal opfylde alle nationale statslige og stedlige sundheds og sikkerhedsforskrifter og love Deutsch Warnung Gef hrliche Stoffe Manche Chemikalien die beim Betrieb des Ger ts benutzt werden m ssen sind...

Page 173: ...prendere le opportune precauzioni per assicurare che l area di lavoro sia sicura e che l operatore non sia esposto a concentrazioni nocive di sostanze tossiche chimiche o biologiche come definito nell...

Page 174: ...htia tarpeellisista varotoimenpiteist jotta ty paikkaymp rist on varmasti turvallinen ja ett laitteen k ytt j t eiv t joudu alttiiksi vaaralliselle m r lle myrkyllisi aineita kemiallisia tai biologisi...

Page 175: ...EC 1010 1 Betreiber Anweisungsperson oder gruppe die f r die Anwendung und Wartung von Ger ten sowie die entsprechende Schulung der Benutzer Bediener verantwortlich ist Benutzer Person die das Ger t f...

Page 176: ...die apparatuur bedient zoals bedoeld portugu s Defini es referentes ao aviso supra referido da CEI 1010 1 Respons vel indiv duo ou grupo respons vel pela utiliza o e manuten o de equipamentos que deve...

Page 177: ...g Bewegliche Teile Verletzungsgefahr Bei normalem Betrieb sind bewegliche Teile des Ger ts zug nglich H nde Kleidung und andere Gegenst nde von den beweglichen Teilen des Ger ts fernhalten espa ol Adv...

Page 178: ...orwerpen uit de buurt van de bewegende delen van het instrument houden portugu s Aviso Pe as m veis perigo de ferimento Algumas pe as m veis do aparelho podem ser acedidas durante o funcionamento norm...

Page 179: ...siguientes pictogramas fran ais Symboles utilis s sur l instrument Tous les symboles suivants peuvent tre utilis s sur l instrument italiano Contrassegni utilizzati sullo strumento Qualsiasi dei segu...

Page 180: ...nger potentiel et invite l usager consulter le manuel d utilisation pour obtenir un expos de ce danger et les moyens de l viter italiano Questo simbolo indica un pericolo potenziale e che l operatore...

Page 181: ...choques el ctricos suomea T m symboli varoittaa s hk iskun vaarasta svenska Symbolen inneb r fara f r elektriska st tar This symbol indicates the risk of hot surfaces dansk Dette symbol angiver risik...

Page 182: ...t Quand l interrupteur est dans cette position l instrument est compl tement d connect de l alimentation secteur italiano Questo simbolo indica la posizione di spento dell interruttore principale di...

Page 183: ...nstrument est connect l alimentation secteur mais n est pas n cessairement en circuit et op rationnel italiano Questo simbolo indica la posizione di acceso dell interruttore principale di alimentazion...

Page 184: ...aan portugu s Este s mbolo indica o interruptor de ligar desligar o funcionamento suomea T m symboli tarkoittaa p lle pois k ytt kytkint svenska Symbolen visar apparatens till fr n knapp This symbol...

Page 185: ...0993 5255 In 1 Index...

Page 186: ...Index In 2 0993 5255...

Page 187: ...breaker see automatic cir cuit breaker cleaning windows 4 5 compressed gases 1 13 connecting acetylene 2 8 air 2 8 argon 2 11 burner drain system 2 15 burner gases 2 7 external cooling sources 2 19 f...

Page 188: ...cations and require ments 6 15 fuses changing 4 8 G gas connectors 7 12 gas hazards 1 13 gas supply requirements 6 9 acetylene 6 12 air 6 11 burner gases 6 10 furnace gases 6 14 nitrous oxide 6 13 H h...

Page 189: ...1 18 6 12 air 1 17 6 11 nitrous oxide 1 17 6 13 safety compressed gases 1 13 correct use of the instrument 1 4 cyanide solutions 1 21 electrical safety 1 5 handling chemicals 1 9 high temperatures 1 1...

Page 190: ...ene explosion hazard 6 12 acetylene pressure 6 12 air supply 6 11 nitrous oxide 6 13 warnings in guide translations 8 3 waste disposal contents of waste containers 1 10 defective lamps 1 10 water cool...

Page 191: ...uides provided with the instrument e ssentials PerkinElmer Instruments on line catalog your single source for quality supplies and accessories http essentials perkinelmer com PerkinElmer s catalog ser...

Page 192: ......

Page 193: ......

Page 194: ...PerkinElmer Instruments 761 Main Avenue Norwalk CT 06859 0010 U S A Tel 1 800 762 4000 or 1 203 762 4000 Fax 1 203 762 4050 Internet http www perkinelmer com Part Number 0993 5255 Release 5...

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