Parr Instrument 4703 Operating Instructions Manual Download Page 9

General Purpose Pressure Vessels

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9

OTHER VESSEL HEAD FITTINGS

Gage Block Assemblies

Parr gage block assemblies combine the function of 
an inlet valve, a pressure gage and a safety rupture 
disc in a compact assembly on a block which can 
be attached to the head of a pressure vessel with a 
single connecting tube.  There is a threaded socket 
in the block for a gas connection with a pressure 
hose or tubing using a Type A coned pressure fitting. 
Coned pressure fittings are also used on the tube 
which connects the block to the pressure vessel.  
The valve in this assembly controls the flow of gas 
into the vessel and the gage shows the internal 
pressure when the valve is closed.  Two styles are 
offered:  The 4316 gage block assembly has a 3-1/2” 
dia. pressure gage and a Type A socket connector.  
This unit is normally used on smaller vessels where 
space is limited. 

The 4317 gage block assembly has a 4-1/2” dia. gage 
and a Type B connector.  It is typically furnished on 
vessels one liter and larger.

Pressure Gages

Pressure gages display in both psi and bar in vari-
ous ranges for use on Parr gage block assemblies.  
The available ranges are shown in the gage block 
parts list.  All of these gages have stainless steel 
cases with T316SS Bourdon tubes and ¼” NPT male 
connections.  Gages constructed of Alloy 400 are 
available on special order.

Safety Rupture Discs

Detailed instructions for the safety rupture disc 
installed in Parr gage blocks and heads are provided 
in a separate Instruction Sheet No. 231M.  The user 
should review these instructions carefully.  Please 
note that the operating pressures in the vessel 
should not exceed 90% of the range of the pressure 
gage and rupture disc.  Also note the warning that 
the discharge port from the rupture disc must always 
be directed away from all operating personnel.  A 
compression fitting for use with 3/8” O.D. tubing is 
attached to the rupture disc body.  It is recommend-
ed that tubing be attached to this connector to carry 
any discharge to a fume hood or safe area in the 
event of an over-pressure.  The free or discharge end 
of any attached tubing must be anchored securely.

Coned Pressure Fittings

The coned pressure fittings used to connect gage 
blocks, pressure hoses and other detachable parts 
to Parr pressure vessels are illustrated below.  These 
fittings have a sleeve with a left-handed thread 
which screws onto the end of a thick-walled tube 
plus a compression nut to complete the assembly.  
When screwed into a matching socket, these parts 
form a rigid joint which will remain tight over a wide 
temperature and pressure range, yet the joint can be 
made and broken repeatedly without destroying the 
sealing faces.  No gasket is required.

4316 Gage 

Block 

Assembly

4317 Gage 

Block 

Assembly

Summary of Contents for 4703

Page 1: ...239M 4600 4700 General Purpose Pressure Vessels Operating Instruction Manual...

Page 2: ...e Block Assemblies 9 Pressure Gages 9 Safety Rupture Discs 9 Coned Pressure Fittings 9 Tapered Pipe Threads 10 MAINTENANCE 10 General Maintenance Notes 10 Periodic Pressure Tests 11 HEAD ASSEMBLY GUID...

Page 3: ...Assurance Certification Intended Usage This system has been designed for use as a high pressure reactor system It has been designed built and tested to strict physical and electrical standards However...

Page 4: ...e deliver ing carriers The vessel motor heater and tem perature controller may be packed separately for convenience in shipping but these parts are easily reassembled Examine the components closely fo...

Page 5: ...hout a pressure venting device it is the cus tomer s responsibility to provide pressure relief in order to protect the operator and the equip ment from destructive high pressures If you need more info...

Page 6: ...mL Vessel with Split Ring Closure and 4316 Gage Block Assembly 2 Before Closing the Vessel examine the head seal carefully to be sure that it is in good condition The seal should not have any nicks or...

Page 7: ...ded choice for many applications since PTFE materi als are inert to most chemicals PTFE gaskets will provide good seals under repeated opening and closing of the vessel if the gasket temperature does...

Page 8: ...lue This will compensate for any tendency of the PTFE gasket to flow under the loading Note It may be possible to extend the life of the Flexible Graphite gasket by coating both sealing surfaces of th...

Page 9: ...e connections Gages constructed of Alloy 400 are available on special order Safety Rupture Discs Detailed instructions for the safety rupture disc installed in Parr gage blocks and heads are provided...

Page 10: ...ring and pres sure connections for excessive corrosion Sus pect parts should be replaced by components only supplied by Parr Instrument Company 2 Always use appropriate wrenches on all fittings and va...

Page 11: ...t regular intervals during the life of each cylinder and particularly whenever the user suspects that the equipment has been over stressed or damaged Some laboratories maintain hydraulic test faciliti...

Page 12: ...ns for Alloys other thanT316SS For parts made from alternate materials use the codes shown below as a suffix to the standard part number CM Alloy 400 CC Alloy 20Cb3 CH Alloy C 276 CT Alloy 600 CAD Tit...

Page 13: ...l fittings per page 12 Recommended BoltTorque PTFE Gasket 500 PSI 15 ft lbs 1000 PSI 20 ft lbs 1500 PSI 30 ft lbs 1700 PSI 40 ft lbs Part No Description Flat Gasket Seal 7AC7 Head A socket 7AC8 Head o...

Page 14: ...l fittings per page 12 Required for maximum working pressure of 7900 psi 544 bar at 538 C for vessel of T316SS Part No Description Flat Gasket Seal 1827HC Head A Socket opening A1828HC Cylinder 75 mL...

Page 15: ...Head two 1 8 NPT 428HC11 Head A socket 1 8 NPT 428HC22 Head A socket 1 8 NPT for thermowell 425HC Cylinder 125 mL 4 44 deep 425HC3 Cylinder 200 mL 6 94 deep 429HC2 Gasket PTFE 429HC2KL Gasket Flexibl...

Page 16: ...et 25 ft lbs Flexible Graphite 35 ft lbs Part No Description Flat Gasket Seal 453HC Head A Socket opening 453HC5 Head A Socket 1 8 NPT 453HC79 Head A Socket 1 8 NPT for thermowell 818HC45 Head VGR 452...

Page 17: ...A122VB STRAIGHT VALVE 526HC SERIES R D 832HC4 DIP TUBE W NUT 836HC GAGE ADAPTER 818HC45 HEAD 452HC CYLINDER 300mL 288VBAD MALE CONNECTOR 366VBA_ HEX COUPLING A455HC SPLIT RING ASSY 457HC2 GASKET 454HC...

Page 18: ...CE orders Maximum WorkingTemperature with FKM O ring with FFKM O ring 225 C 300 C Part No Description O ring Seal 2321HC2 Head A socket opening 2321HC3 Head A socket 1 8 NPT 2340HC11 Head VGR 2342HC...

Page 19: ...T RING ASSY A456HC DROP BAND W SCREW 2341HCJV O RING 832HC4 DIP TUBE W NUT 288VBAD MALE CONNECTOR A472E THERMOCOUPLE 366VBA_ HEX COUPLING A888HC2 R D HOLDER ASSY 2342HC CYLINDER 300mL A122VB STRAIGHT...

Page 20: ...429HC2KL Gasket Flexible Graphite 454HC Compression Ring A455HC Split Ring A456HC Drop Band 232HCFDE Bolt for Split Ring 1443HC2 DIP TUBE 50mL 1443HC DIP TUBE 25mL 593HC SERIES PRESSURE GAGE 836HC GAG...

Page 21: ...i A122VB Valve Straight 1 8 NPT M Recommended BoltTorque PTFE or Flexible Graphite 15 ft lbs max Part No Description A146VB Valve Angle 1 8 NPT M A472E4 Thermocouple 5 1 2 A472E Thermocouple 7 1 2 A83...

Page 22: ...ng Limits Maximum Working Pressure T316SS 1900 psi 131 bar Maximum WorkingTemperature with PTFE confined flat gasket 350 C Recommended BoltTorque PTFE Gasket 25 ft lbs Flexible Graphite 35 ft lbs Note...

Page 23: ...hermowell for 2000 mL vessel 265HC7 Thermowell for 1000 mL vessel 48HC Thermowell Gasket silver 48HCCN Thermowell Gasket nickel 48HCFG Thermowell Gasket gold plated A472E2 Thermocouple 9 1 2 1000mL A4...

Page 24: ...0mL Part No Description Flat Gasket Seal 2330HC12 Head B socket 2330HC13 Head B socket thermowell 2300HC19 Head VGR thermowell 2302HC Cylinder 600 mL 2302HC10 Cylinder 1200 mL 2304HC Compression Ring...

Page 25: ...e ratings please consult Parr Instrument Company Series 4650 Model Size Head Style 4651 250 mL VGR thermowell 4652 500 mL VGR thermowell 4653 1000 mL VGR thermowell Working Limits Maximum Working Pres...

Page 26: ...1 4 NPT M A129VB Valve Straight 1 4 NPT M X 1 4 T A147VB Valve Straight 1 4 NPT M 658HC Valve Extension 208HC15 Gage Adapter 2 1 4 NPTF 94CA Plug Hex Head 1 4 NPT Brass 686HC DipTube 1 G 686HC3 DipTub...

Page 27: ...AngleValve 1 4 NPT M A147VB Valve Straight 1 4 NPT M A707HC2 Rupture Disc Assembly See Manual 231M 708HCP10CT Rupture disc Inconel 1000psi 708HCP20CT Rupture disc Inconel 2000 psi 708HCP30CT Rupture...

Page 28: ...or above 16 req 265HC4 Thermowell 7 75 deep 265HC10 Thermowell 11 87 deep 48HC Thermowell Gasket silver 48HCCN Thermowell gasket nickel 48HCFG Thermowell Gasket gold plated A472E6 Thermocouple 15 1 2...

Page 29: ...T M T316SS A279VBAD Valve angle 3 8 NPT M T316SS 265HC15 Thermowell 15 94 48HC Thermowell Gasket silver 48HCCN Thermowell gasket nickel 48HCFG Thermowell Gasket gold plated 1571HC Head Lift Rings 1593...

Page 30: ...e PTFE or Flexible Graphite 500 PSI 25 ft lbs 1000 PSI 50 ft lbs 1500 PSI 75 ft lbs 1900 PSI 100 ft lbs Part No Description Flat Gasket Seal 2957HC11 Head VGR two valves thermowell 2955HC Cylinder 10...

Page 31: ...mowell gasket gold plated 265HC6 Thermowell 5 75 deep 265HC8 Thermowell 10 19 deep 36HC5 Handles 1368HC TorqueWrench 1369HC Torque Adapter A472E2 Thermocouple 9 1 2 SS A472E6 Thermocouple 15 1 2 SS 25...

Page 32: ...3 8 tube 35HC Compression nut short 365HC Connecting tube 3 8 OD x 3 length 366HC Collar L H thread 3 8 tube 4VB3 Packing ring PTFE 2 required 4VB4KL Packing ring Flexible Graphite 40HC Collar L H thr...

Page 33: ...i 56HCPD 0 1000 psi 56HCPF 0 2000 psi 56HCPG 0 3000 psi 56HCPH 0 5000 psi 56HCPK 0 10000 psi Series 593HC Pressure Gages 3 1 2 diameter T316SS Part No Description 593HCP1AD 0 100 psi 593HCP2AD 0 200 p...

Page 34: ...325HC COMPRESSION PACKING GASKET NUT SEE NOTE 1 51HC TUBE INLET NUT SEE NOTE 2 40HC BUSHING 366HC BUSHING 35HC SEE NOTE 1 326HC COMPRESSION NUT SEE NOTE 1 365HC COMPRESSION 366HC BUSHING 427HC GAGE BL...

Page 35: ...C SERIES PRESSURE GAGE 302VBAD HANDLE VALVE PACKING 8VB2 123VB2 NUT NEEDLE 20VBHB 112VB4AK VALVE ORIFICE RING 527HC 126VB 6VBAA PACKING LANTERN RING BLOCK GAGE BUSHING 40HC COMPRESSION 325HC 427HC2 SE...

Page 36: ...2 3 9 M R 1 1 0 4 1 8 1 7...

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