Parr Instrument 4703 Operating Instructions Manual Download Page 10

General Purpose Pressure Vessels

P a r r   I n s t r u m e n t   C o m p a n y

10

TUBING

NUT
BUSHING

D

E

Coned Pressure Fittings

Type

A

B

Tube Size

1/4”

3/8”

Thread (D) 9/16-18 3/4-16

Bore (E)

3/32”

1/8”

Nut No.

35HC

326HC

Bushing No. 40HC

366HC

When using these coned connectors, screw the 
bushing onto the tube as far as it will go; then insert 
the end of the tube into the head or gage block and 
tighten the compression nut firmly while holding the 
block stationary with the gage facing in the desired 
direction.  Note that this assembly behaves like a 
pipe union, allowing the connecting tube or hose to 
remain stationary while the joint is tightened.  

Note: 

 PTFE tape is not required on these connectors.

Tapered  Pipe Threads

The pressure gage, needle valves and other fixed 
attachments on Parr vessel heads have tapered pipe 
threads which are not to be disturbed after they 
have been screwed into place.  If it becomes neces-
sary to remove any of these fittings, the pipe threads 
must be coated with PTFE tape, flexible graphite 
tape, or similar luting material on reassembly.

The ID of a pipe or pipe fitting can be enlarged to 
accommodate a tubing feed-thru. Note that, in some 
cases, this may cause a reduction of the pressure 
rating. The port below a female pipe connection can 
also be opened up to a larger size. 

The maximum openings are shown in the table below.

A

B

C

Tapered Pipe Threads

Nominal Size 1/8”

1/4”

Pipe OD (A)

0.405” 0.540”

Maximum 
Feed-thru (B)

1/4”

3/8”

Maximum Exit 
Port (C)

0.339” 0.438”

MAINTENANCE

General Maintenance Notes

1.  Periodically inspect all electrical wiring and pres-

sure connections for excessive corrosion.  Sus-
pect parts should be replaced by components 
only supplied by Parr Instrument Company.

2.  Always use appropriate wrenches on all fittings 

and valves.  Never use pliers or pipe wrenches.

3.  Head and cylinder service fixtures are available 

for convenience and protection of components 
during maintenance of your reactor.

Note: 

 For more information about available 

service fixtures, reference TechNote 307.

4.  A light coating of thread lubricant, such as Parr 

High Temperature Anti-Seize Lubricant, (424HC2) 
should be applied to the straight threads of 
coned pressure connections as well as to the 
nose of the mating piece this will help to obtain 
a tight joint.  

Note: 

 PTFE tape should be used only on 

all tapered (NPT) threads not NPS straight 
threads.

5.  NPT (National Pipe Taper) threads should not be 

disassembled any more than necessary.  It will 
become increasingly difficult to maintain a tight 
seal with these tapered threads if the joint is 
made and broken repeatedly.

6.  Do not use oil or anti-seize lubricant on threads 

or fittings if the vessel is to be used with oxygen.

7.  If your vessel is equipped with a loose compres-

sion ring be sure that it is in place on the head 
before attaching any head fittings.  The compres-
sion ring cannot be installed after fittings have 
been screwed into the head. 

8.  Clean all threads and gas passages thoroughly 

and remove all tape fragments when overhaul-
ing a vessel.  An ultrasonic bath is excellent for 
cleaning metal parts, but do not place a thermo-
couple probe, pressure gage, face seals or ball 
bearings in an ultrasonic bath.  Periodic cleaning 
may be performed on the exterior surfaces of 
the reactor stand with a damp cloth.  All power 
should be disconnected when cleaning.

Summary of Contents for 4703

Page 1: ...239M 4600 4700 General Purpose Pressure Vessels Operating Instruction Manual...

Page 2: ...e Block Assemblies 9 Pressure Gages 9 Safety Rupture Discs 9 Coned Pressure Fittings 9 Tapered Pipe Threads 10 MAINTENANCE 10 General Maintenance Notes 10 Periodic Pressure Tests 11 HEAD ASSEMBLY GUID...

Page 3: ...Assurance Certification Intended Usage This system has been designed for use as a high pressure reactor system It has been designed built and tested to strict physical and electrical standards However...

Page 4: ...e deliver ing carriers The vessel motor heater and tem perature controller may be packed separately for convenience in shipping but these parts are easily reassembled Examine the components closely fo...

Page 5: ...hout a pressure venting device it is the cus tomer s responsibility to provide pressure relief in order to protect the operator and the equip ment from destructive high pressures If you need more info...

Page 6: ...mL Vessel with Split Ring Closure and 4316 Gage Block Assembly 2 Before Closing the Vessel examine the head seal carefully to be sure that it is in good condition The seal should not have any nicks or...

Page 7: ...ded choice for many applications since PTFE materi als are inert to most chemicals PTFE gaskets will provide good seals under repeated opening and closing of the vessel if the gasket temperature does...

Page 8: ...lue This will compensate for any tendency of the PTFE gasket to flow under the loading Note It may be possible to extend the life of the Flexible Graphite gasket by coating both sealing surfaces of th...

Page 9: ...e connections Gages constructed of Alloy 400 are available on special order Safety Rupture Discs Detailed instructions for the safety rupture disc installed in Parr gage blocks and heads are provided...

Page 10: ...ring and pres sure connections for excessive corrosion Sus pect parts should be replaced by components only supplied by Parr Instrument Company 2 Always use appropriate wrenches on all fittings and va...

Page 11: ...t regular intervals during the life of each cylinder and particularly whenever the user suspects that the equipment has been over stressed or damaged Some laboratories maintain hydraulic test faciliti...

Page 12: ...ns for Alloys other thanT316SS For parts made from alternate materials use the codes shown below as a suffix to the standard part number CM Alloy 400 CC Alloy 20Cb3 CH Alloy C 276 CT Alloy 600 CAD Tit...

Page 13: ...l fittings per page 12 Recommended BoltTorque PTFE Gasket 500 PSI 15 ft lbs 1000 PSI 20 ft lbs 1500 PSI 30 ft lbs 1700 PSI 40 ft lbs Part No Description Flat Gasket Seal 7AC7 Head A socket 7AC8 Head o...

Page 14: ...l fittings per page 12 Required for maximum working pressure of 7900 psi 544 bar at 538 C for vessel of T316SS Part No Description Flat Gasket Seal 1827HC Head A Socket opening A1828HC Cylinder 75 mL...

Page 15: ...Head two 1 8 NPT 428HC11 Head A socket 1 8 NPT 428HC22 Head A socket 1 8 NPT for thermowell 425HC Cylinder 125 mL 4 44 deep 425HC3 Cylinder 200 mL 6 94 deep 429HC2 Gasket PTFE 429HC2KL Gasket Flexibl...

Page 16: ...et 25 ft lbs Flexible Graphite 35 ft lbs Part No Description Flat Gasket Seal 453HC Head A Socket opening 453HC5 Head A Socket 1 8 NPT 453HC79 Head A Socket 1 8 NPT for thermowell 818HC45 Head VGR 452...

Page 17: ...A122VB STRAIGHT VALVE 526HC SERIES R D 832HC4 DIP TUBE W NUT 836HC GAGE ADAPTER 818HC45 HEAD 452HC CYLINDER 300mL 288VBAD MALE CONNECTOR 366VBA_ HEX COUPLING A455HC SPLIT RING ASSY 457HC2 GASKET 454HC...

Page 18: ...CE orders Maximum WorkingTemperature with FKM O ring with FFKM O ring 225 C 300 C Part No Description O ring Seal 2321HC2 Head A socket opening 2321HC3 Head A socket 1 8 NPT 2340HC11 Head VGR 2342HC...

Page 19: ...T RING ASSY A456HC DROP BAND W SCREW 2341HCJV O RING 832HC4 DIP TUBE W NUT 288VBAD MALE CONNECTOR A472E THERMOCOUPLE 366VBA_ HEX COUPLING A888HC2 R D HOLDER ASSY 2342HC CYLINDER 300mL A122VB STRAIGHT...

Page 20: ...429HC2KL Gasket Flexible Graphite 454HC Compression Ring A455HC Split Ring A456HC Drop Band 232HCFDE Bolt for Split Ring 1443HC2 DIP TUBE 50mL 1443HC DIP TUBE 25mL 593HC SERIES PRESSURE GAGE 836HC GAG...

Page 21: ...i A122VB Valve Straight 1 8 NPT M Recommended BoltTorque PTFE or Flexible Graphite 15 ft lbs max Part No Description A146VB Valve Angle 1 8 NPT M A472E4 Thermocouple 5 1 2 A472E Thermocouple 7 1 2 A83...

Page 22: ...ng Limits Maximum Working Pressure T316SS 1900 psi 131 bar Maximum WorkingTemperature with PTFE confined flat gasket 350 C Recommended BoltTorque PTFE Gasket 25 ft lbs Flexible Graphite 35 ft lbs Note...

Page 23: ...hermowell for 2000 mL vessel 265HC7 Thermowell for 1000 mL vessel 48HC Thermowell Gasket silver 48HCCN Thermowell Gasket nickel 48HCFG Thermowell Gasket gold plated A472E2 Thermocouple 9 1 2 1000mL A4...

Page 24: ...0mL Part No Description Flat Gasket Seal 2330HC12 Head B socket 2330HC13 Head B socket thermowell 2300HC19 Head VGR thermowell 2302HC Cylinder 600 mL 2302HC10 Cylinder 1200 mL 2304HC Compression Ring...

Page 25: ...e ratings please consult Parr Instrument Company Series 4650 Model Size Head Style 4651 250 mL VGR thermowell 4652 500 mL VGR thermowell 4653 1000 mL VGR thermowell Working Limits Maximum Working Pres...

Page 26: ...1 4 NPT M A129VB Valve Straight 1 4 NPT M X 1 4 T A147VB Valve Straight 1 4 NPT M 658HC Valve Extension 208HC15 Gage Adapter 2 1 4 NPTF 94CA Plug Hex Head 1 4 NPT Brass 686HC DipTube 1 G 686HC3 DipTub...

Page 27: ...AngleValve 1 4 NPT M A147VB Valve Straight 1 4 NPT M A707HC2 Rupture Disc Assembly See Manual 231M 708HCP10CT Rupture disc Inconel 1000psi 708HCP20CT Rupture disc Inconel 2000 psi 708HCP30CT Rupture...

Page 28: ...or above 16 req 265HC4 Thermowell 7 75 deep 265HC10 Thermowell 11 87 deep 48HC Thermowell Gasket silver 48HCCN Thermowell gasket nickel 48HCFG Thermowell Gasket gold plated A472E6 Thermocouple 15 1 2...

Page 29: ...T M T316SS A279VBAD Valve angle 3 8 NPT M T316SS 265HC15 Thermowell 15 94 48HC Thermowell Gasket silver 48HCCN Thermowell gasket nickel 48HCFG Thermowell Gasket gold plated 1571HC Head Lift Rings 1593...

Page 30: ...e PTFE or Flexible Graphite 500 PSI 25 ft lbs 1000 PSI 50 ft lbs 1500 PSI 75 ft lbs 1900 PSI 100 ft lbs Part No Description Flat Gasket Seal 2957HC11 Head VGR two valves thermowell 2955HC Cylinder 10...

Page 31: ...mowell gasket gold plated 265HC6 Thermowell 5 75 deep 265HC8 Thermowell 10 19 deep 36HC5 Handles 1368HC TorqueWrench 1369HC Torque Adapter A472E2 Thermocouple 9 1 2 SS A472E6 Thermocouple 15 1 2 SS 25...

Page 32: ...3 8 tube 35HC Compression nut short 365HC Connecting tube 3 8 OD x 3 length 366HC Collar L H thread 3 8 tube 4VB3 Packing ring PTFE 2 required 4VB4KL Packing ring Flexible Graphite 40HC Collar L H thr...

Page 33: ...i 56HCPD 0 1000 psi 56HCPF 0 2000 psi 56HCPG 0 3000 psi 56HCPH 0 5000 psi 56HCPK 0 10000 psi Series 593HC Pressure Gages 3 1 2 diameter T316SS Part No Description 593HCP1AD 0 100 psi 593HCP2AD 0 200 p...

Page 34: ...325HC COMPRESSION PACKING GASKET NUT SEE NOTE 1 51HC TUBE INLET NUT SEE NOTE 2 40HC BUSHING 366HC BUSHING 35HC SEE NOTE 1 326HC COMPRESSION NUT SEE NOTE 1 365HC COMPRESSION 366HC BUSHING 427HC GAGE BL...

Page 35: ...C SERIES PRESSURE GAGE 302VBAD HANDLE VALVE PACKING 8VB2 123VB2 NUT NEEDLE 20VBHB 112VB4AK VALVE ORIFICE RING 527HC 126VB 6VBAA PACKING LANTERN RING BLOCK GAGE BUSHING 40HC COMPRESSION 325HC 427HC2 SE...

Page 36: ...2 3 9 M R 1 1 0 4 1 8 1 7...

Reviews: