4590 Micro Reactors
w w w . p a r r i n s t . c o m
3
PREFACE
4
Scope
4
Related Instructions
4
Intended Usage
4
Safety Information
4
General Specifications
4
Electrical Ratings
4
Explanation of Symbols
5
Environmental Conditions
5
Unpack Carefully
5
Provisions for Lifting and Carrying
5
Cleaning & Maintenance
5
User’s Responsibility
6
Fixed Head or Removable Head Vessel Design
7
Flat Gasket or Self Sealing O-Ring Closure
7
INSTALLATION
8
Pressure and Temperature Limits
8
Assemble The Reactor
9
IDENTIFY THE VALVES
10
Gas Inlet Valve
10
Gas Release Valve
10
Liquid Sampling Valve
10
OTHER VESSEL HEAD FITTINGS
11
Safety Rupture Disc
11
Type J Thermocouple
11
Pressure Gage
11
ACCESSORIES AND OPTIONS
11
Liners
11
Spare Parts Kit
11
Air Motor
12
HOW TO USE THE VESSEL
14
To open the Vessel
14
Before Closing the Vessel
14
Sealing Vessels with PTFE Gaskets
14
Sealing with Flexible Graphite Gaskets
14
O-Ring Closures
14
Gas Connections
15
Pressurizing the Vessel
15
Do Not Overfill the Vessel
15
Releasing Pressure
15
Withdrawing Liquid Samples
15
Initial Operating Test
15
MAINTENANCE
16
General Maintenance Notes
16
Periodic Pressure Tests
17
Technical Support
17
SERIES 4590 VESSEL PARTS LISTS
18
Standard Reaction Vessel Parts List
18
High Pressure Reaction Vessel Parts List
21
HP/HT Reaction Vessel Parts List
23
Overarm and Stand Parts List
24
Support Stands
25
Customer Service
Questions concerning the installation or operation
of this instrument can be answered by the Parr
Customer Service Department:
1-309-762-7716 • 1-800-872-7720
Fax: 1-309-762-9453
E-mail: [email protected]
http://www.parrinst.com
Artisan Technology Group - Quality Instrumentation ... Guaranteed | (888) 88-SOURCE | www.artisantg.com