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4560 Mini Bench Top Reactors
Parr Instrument Company
Revision 6-28-02
TABLE OF CONTENTS
Related Instructions.......................2
Customer Service..........................2
Preface ...............................................3
Scope ............................................3
User’s Responsibility .....................3
Unpack Carefully ...........................3
Fixed Head or Removable
Head Vessel Design......................4
Flat PTFE Gasket or Self-
Sealing O-Ring Closure.................4
Installation .........................................5
Pressure and Temperature
Limits.............................................5
Assemble the Reactor ......................6
Heaters ...........................................7
Identify the Valves ............................8
Gas Inlet Valve ..............................8
Gas Release Valve........................8
Liquid Sampling Valve...................8
Other Vessel Head Fittings ..............9
Safety Rupture Discs.....................9
Type J Thermocouple....................9
Pressure Gage ..............................9
How to Use the Vessel .....................10
Removable Head Vessels .............10
Fixed Head Vessels ......................10
Gas Connections...........................11
Pressurizing the Vessel.................11
Do Not Overfill the Vessel .............11
Releasing Pressure .......................11
Withdrawing Liquid Samples .........12
Initial Operating Test .....................12
Internal Cooling Loop ....................12
Air Motor ......................................13
Explosion Proof Operation ..............14
Periodic Pressure Tests .................. 15
Accessories ...................................... 15
Liners ............................................ 15
Spare Parts Kits............................ 15
General Maintenance Notes ............ 16
Parts List ........................................... 17
Standard Internal Parts List .......... 17
Reaction Vessel Parts List ............ 18-20
Overarm Parts List ........................ 21
Vessel Heater Parts List ............... 7
Support Stand .............................. 22,23
Related Instructions
The following Parr publications are
also included to further your understanding
of this instrument and its component parts:
No. Description
230M Safety Precautions to be observed
when operating Pressure Reaction
Equipment
231M Operating Instructions for Parr Safety
Rupture Discs
232M Operating Instructions for Series
4840 Temperature Controllers
234M Operating and Maintenance
Instructions for Parr Magnetic Drives
323M Operating Instructions for Parr
Pressure Relief Valves
201M Limited Warranty
Customer Service
Questions concerning the installation
or operation of this instrument can be
answered by the Parr Customer Service
Department:
309-762-7716
800-872-7720
Fax: 309-762-9453
www.parrinst.com
[email protected]