Nic MERCURY/MA-3000 Operation Manual Download Page 8

NIC-600-2233-06

 

 

7.4. How to mount the samples 

Sample amount is depending on the sample kind, form, but 200mg for solid and 200

μL for liquid are 

usually  recommended.  Be  careful  not  to  be  spilled  out  of  the  boats  during  loading  in  the  sample 

changer. 

Wear the gloves

 

or use the tweezers, when weighing samples and handling sample boats. 

If  the  liquid  samples  may  contain  organic  mercury,  add  additive  B  or  L-cysteine  solution  not  to 

vaporize during standby in the sample changer. Add small amount of additive B in the boat bottom 

or add 10

μ

L of 100ppm L-cysteine solution. 

 

 

 

 

 

 

 

 

 

 

When you use additive B, please put small amount of additive into sample boat before sample 

weighting. 

  The

 

volatile high liquid 

Add more additive the level of liquid samples 

  The sample which melt after measurement 

(Ex. Aluminum, Pyrex and so on) 

Put additive at the bottom.   

 

  The sample which burns rapidly 

Put  additive  at  the  bottom  on  the  boat.  And  put  sample 

several  points  on  additive,  and  then  cover  it  with  another 

additive. 

 

Summary of Contents for MERCURY/MA-3000

Page 1: ...MERCURY MA 3000 Simplified Operation manual NIC 600 2233 06 Nippon Instruments Corporation...

Page 2: ...hat incorrect handling could result in death or severe injury to the operator Caution Indicates that incorrect handling could result in moderate or minor injury to the operator or damage to property 1...

Page 3: ...the discharge If you don t turn on MA 3000 for a long time the sample heating tube might be obstructed or break by moisture absorption If you don t turn on MA 3000 more than 2 weeks please turn on th...

Page 4: ...essage will be displayed if abnormal condition is observed Software will be terminated when OK is clicked Turn off MA 3000 and then fixing them 4 After the check is completed heat conditioning start H...

Page 5: ...method for STD The default method is already set for standard solution but selects the proper method for using SRM Standard Reference Materials Select Flow rate 0 1L min High sensitivity 1pg 10ng 0 2L...

Page 6: ...Solid or Liquid Select a sample feature This is not related to Measuring method Calibration curve Usually please select y ax blank 7 Measurements 7 1 Registration of standard Click the tab of STD 1 C...

Page 7: ...Click the icon and switch to the Analyze screen Review the calibration curve in CALIB tab When some abnormalities are observed on a calibration curve all values of the calibration become red and WARNI...

Page 8: ...e B or L cysteine solution not to vaporize during standby in the sample changer Add small amount of additive B in the boat bottom or add 10 L of 100ppm L cysteine solution When you use additive B plea...

Page 9: ...Standard solution Liquid sample with additive B STD 200 L 1 Biological sample Solid Fish tissue plant tissue ORGANISM SOLID 200 mg 2 Soil sediment sludge SOIL SLUDGE 200 mg 3 Urine Blood URINE BLOOD...

Page 10: ...t of sample or to change the heating conditions Inject 200 L of Distilled Water for several times if high concentration samples are measured Inject 200 L of Standard Solution repeatedly if the sensiti...

Page 11: ...turn on MA 3000 for a long time the sample heating tube might be obstructed by moisture absorption If you don t turn on MA 3000 more than 2 weeks please turn on the MA 3000 power switch and do conditi...

Page 12: ...33 06 11 Nippon Instruments Corporation 14 8 Akaoji cho Takatsuki shi Osaka 569 1146 Japan Please contact the distributor or the following Technical Service E mail info nic rigaku co jp URL https www...

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