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Milli-Q Millipore User Manual Download Page 3

Milli-Q® Reference System

3

About this User Manual

Purpose

This User Manual is intended for use with a Milli-Q® Reference Water Purification

System.
This User Manual is a guide for use during the installation, normal operation and
maintenance of a Milli-Q® Reference Water Purification System. It is highly
recommended to completely read this manual and to fully comprehend its contents
before attempting installation, normal operation or maintenance of the Water

Purification System.
If this User Manual is not the correct one for your Water Purification System, then
please contact Millipore SAS.

Terminology

The term “Milli-Q® Reference Water Purification System” is replaced by the term
“System” for the remainder of this User Manual unless otherwise noted.

Document

FTPF11373 - V 2.0, 03/2013

About Millipore SAS

Internet Site

Address

The Internet site can be used to find addresses, telephone/fax numbers and other
information.
Internet Site Address:

www.millipore.com

www.millipore.com/techservice
www.millipore.com/lab_water

Manufacturing

Site

Millipore SAS
67120 Molsheim
FRANCE

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Summary of Contents for Millipore

Page 1: ...1 User Manual Milli Q Reference System...

Page 2: ......

Page 3: ...aintenance of the Water Purification System If this User Manual is not the correct one for your Water Purification System then please contact Millipore SAS Terminology The term Milli Q Reference Water...

Page 4: ...listed in this publication may be found at http www millipore com ec cp3 terms within the Terms and Conditions of Sale applicable to your purchase transaction Trademarks Elix Q Gard Quantum Milli Q Bi...

Page 5: ...t be worn This UV RADIATION sticker is used to refer to a position on the water system Cabinet or inside of it where exposure to UV light is possible This DANGER sticker is used to refer to a position...

Page 6: ......

Page 7: ...andby Mode 38 General information 38 Description of Standby Menu 39 Manager Menu 41 Description 41 Ready Mode 44 General information 44 Description of Ready Menu 45 Using the Milli Q System 48 Overvie...

Page 8: ...8 Milli Q Reference System Alerts 82 Overview 82 Alert information 83 Summary of Alert messages 88 Ordering Information 90 Consumables Accessories and Systems 90...

Page 9: ...ed to the System Some of the more important topics in this chapter are installation requirements consumable information and dimensions of various components of the System Contents This chapter contain...

Page 10: ...Delivery POD B POD Pak C POD Arm D Connections for tubings power cord level sensor and other cables E Q Gard Pack F POD Mast G Main Display H Quantum Cartridge Main Display function The Main Display i...

Page 11: ...of the Right Keypad button is shown below It is used to move to the next screen In this example the system is changed from STANDBY Mode to READY Mode Diagram 1 Action Diagram 2 Press Left The use of t...

Page 12: ...menu Diagram 1 Action Diagram 2 Press Down The use of the Down Keypad button is shown below It is used to scroll down in a menu Diagram 1 Action Diagram 2 Press Validate The use of the Validate Keypad...

Page 13: ...nd therefore does not display a TOC value Should you wish to have a display of the TOC value please contact Millipore SAS and inquire about availability of the TOC Indicator Upgrade Kit In this exampl...

Page 14: ...connections are explained below Item Description Item Description 1 Feedwater port 4 Termination Plug connection maximum 5 VDC 2 Ethernet connection maximum 5 VDC 5 Accessories connection maximum 24 V...

Page 15: ...feedwater is the water coming from either a RiOs System or Elix Water Purification System This type of feedwater typically has some ions but contains little organic particulate and colloidal contamina...

Page 16: ...f ions is critical Quantum TEX Cartridge The Quantum TEX Cartridge contains ion exchange resin and synthetic carbon These purification media are used when the Milli Q Water needs to have both trace le...

Page 17: ...may not be achieved at start up Weight The various weights are found in the table below Item Operating Weight Dry Weight Shipping Weight Milli Q Reference System 19 5 kg 14 5 kg 19 kg Electrical The e...

Page 18: ...pecifications and requirements Continued Dimensions Materials of construction Please contact Millipore SAS for a list of the Materials of Construction Continued on next page 360 mm 416 mm 552 mm 783 m...

Page 19: ...ere Parameter Value Altitude 3000 metres Ambient operating temperature 4 40 C Ambient storage temperature 4 40 C Installation Category II Location The System is intended for indoor use only Pollution...

Page 20: ...p timer 32 Calibrating the Flowrate 34 Summary list The steps shown below outline the sequence and major actions of a System installation Please refer to this list throughout the installation Step Act...

Page 21: ...s generated In order to advance during the installation these alarms should be cancelled for a limited time Q GARD PACK OUT message This alarm occurs because the Q Gard Pack is not installed This alar...

Page 22: ...ery by cutting and removing the tape that holds them together POD Arm Place the POD and POD Arm onto the POD Mast as shown below Feedwater tubing The Feedwater tubing is connected to either a Reservoi...

Page 23: ...m Cabinet Follow the steps below Step Action Diagram 1 Plug one end of the feedwater tubing to the Cabinet Open the valve on the other end of the feedwater tubing to allow water flow later 2 Plug in t...

Page 24: ...e System is configured to have a Level Sensor Cancel Alarms When an Alarm message is displayed follow the instructions on the screen to cancel the text display of the Alarm Check the date When the Ala...

Page 25: ...own at this time By following the instructions earlier in this manual the alarm was cancelled 2 Open the left door of the System Cabinet Remove the 2 protective caps located on the ports inside 3 Remo...

Page 26: ...Gard Pack Continued Procedure continued Step Action Diagram 5 Push the bottom of the Q Gard Pack inwards 6 Push the pack locking handle down Close the left door 7 One minute later the Main LCD shows...

Page 27: ...Open the right door of the System Cabinet Remove the 2 protective caps located on the ports inside 2 Remove the covers on the 2 ports of the Quantum Cartridge Wet the O rings with water 3 Install the...

Page 28: ...of the clear tubing onto the end of the barbed fitting Place the other end of the clear tubing into a sink NOTE Do not use any white tape on the threads of the barbed fitting An O ring located inside...

Page 29: ...Q Reference System 29 Rinsing the System Continued Procedure continued Step Action Diagram 5 Push the POD Plunger all the way down and then release it to stop dispensing water Leave the System in READ...

Page 30: ...t and registering the installation of a specific POD Pak Placing and flushing Follow the instructions delivered with the POD Pak Registering Follow the steps below to register the installation of the...

Page 31: ...Milli Q Reference System 31 Installing a POD Pak Continued Registering continued Step Action Diagram 5 Press 6 Press 7 In this example you choose Millipak Press 8 Press 9 Press 10 Press 3 times on...

Page 32: ...ating that a Lamp replacement is needed is shown too early NOTE Before doing this make sure that the date and time have been checked for accuracy Procedure This procedure shows how to reset the timer...

Page 33: ...Milli Q Reference System 33 Registering UV Lamp timer Continued Procedure continued Step Action Diagram 5 Press 6 Press 7 Press 8 Press 3 times on...

Page 34: ...stalled A 1 Litre graduated cylinder is needed Procedure Follow the steps below to perform a Flow Calibration Step Action Diagram 1 Go to STANDBY Mode 2 Select Menu Press 3 Enter the Manager Menu See...

Page 35: ...ated Cylinder under the POD Unit Press 7 Press 8 Water dispenses automatically from the POD Unit Wait until it stops dispensing water 9 Measure the amount of water in ml that was dispensed Suppose 870...

Page 36: ...e Overview Introduction The purpose of this chapter is to explain the various software used in the System Contents This chapter contains the following topics Topic See Page Software Map 37 Standby Mod...

Page 37: ...Milli Q Reference System 37 Software Map M a p...

Page 38: ...eference System Standby Mode General information Purpose STANDBY mode is used primarily for maintenance actions and going to the Manager Menu Display READY Mode from STANDBY Mode Diagram 1 Action Diag...

Page 39: ...Q Gard Used to see general information about the Q Gard Pack exchange Install UV 185 Lamp Used to reset Alert message REPLACE 185 NM LAMP Install Quantum Used to see general information about the Qua...

Page 40: ...40 Milli Q Reference System Description of Standby Menu Continued Language Diagram 1 Diagram 2 Item Description Language Change the displayed language...

Page 41: ...ager Menu it is necessary to input a Login and a Password The Software Map indicates how to input a Login and a Password Change ID and Password Diagram 1 Diagram 2 Item Description CHANGE ID PASSWORD...

Page 42: ...Q GARD AND QUANTUM Milli Q Product Res Change set point controlling the message MILLI Q RES SP REPLACE Q GARD AND QUANTUM Milli Q Product TOC Change set point controlling the message MILLI Q TOC SP M...

Page 43: ...tem automatically recirculates every hour in READY Mode POD Flow Stop Change the amount of time that the POD Unit dispenses continuously before it automatically stops Temp Comp Change the Temperature...

Page 44: ...screen display is explained below READY Mode screen Explanation In this example the water being dispensed has a resistivity of 18 2 M cm temperature compensated TC to 25 C a temperature of 24 9 C and...

Page 45: ...Diagram 1 Diagram 2 Item Description System Operation View operating parameters operating mode status of pump and status of UV Lamp System Alerts View a list of active Alert messages See the Alert Cha...

Page 46: ...processed catalogue number and serial number NOTE The five items listed above may not be shown in each Consumable Status screen UV 185 nm Lamp Quantum POD Pak Call Millipore SAS Diagram 1 Diagram 2 I...

Page 47: ...ng service NOTE This information is entered by a Millipore SAS Representative Repair Service Contract Contract Expires Next Service Next Calibration Next Qualification Information Diagram 1 Diagram 2...

Page 48: ...t water can be dispensed from the System and how to view information operating parameters and other things about the System Contents This chapter contains the following topics Topic See Page Dispensin...

Page 49: ...fore dispensing it This helps optimise water quality Follow the steps below to do this Step Action Diagram 1 Start in READY Mode NOTE The Resistivity and temperature values may or may not be shown at...

Page 50: ...Low Flow push slightly M Medium Flow push slightly H High Flow push down and hold release when done H Continuous high flow push down and release push down again to stop Volumetric dispensing Follow t...

Page 51: ...ntinued Volumetric dispensing continued Step Action Diagram 3 Select the desired volume of water to be delivered Press 4 When the volumetric dispensing is finished the System recirculates water for 3...

Page 52: ...quality Step Action Diagram 1 Make sure the System is in READY Mode NOTE The Resistivity Res and Temperature T are seen in the main READY Mode screen 2 To see Tank Level indicator select Menu Press 3...

Page 53: ...Operation LCD the following items can be selected System Operation System Alerts System Alarms and System Measures System Operation Follow the steps below to go to the System Operation LCD Step Actio...

Page 54: ...e timer for the UV 185 nm Lamp is reset then this Alert is no longer shown on the SYSTEM ALERTS LCD System Alarms An example Alarm is shown here This is an Alarm that is currently displayed on the Mai...

Page 55: ...consumables Procedure Follow the steps below to view Consumables Status Step Action Diagram 1 Start in READY Mode 2 Select Menu Press 3 Select Consumables Status Press 4 Select the consumable that you...

Page 56: ...ipore SAS Service Representative can enter this information into the System Procedure Follow the steps below to view information under Call Millipore SAS Step Action Diagram 1 Start in READY Mode 2 Se...

Page 57: ...sion information and serial number and other information Procedure Follow the steps below to see information about the System Step Action Diagram 1 Start in READY Mode 2 Select Menu Press 3 Select Inf...

Page 58: ...Information The Catalogue Number Serial Number and other information are shown here The Serial Number is something you should reference when you contact Millipore SAS This LCD shows information such a...

Page 59: ...to explain the common maintenance needed for a System Contents This chapter contains the following topics Topic See Page Maintenance Schedule 60 Replacing the Q Gard Pack 61 Replacing the Quantum Car...

Page 60: ...ervice Representative change the UV Lamp in the system The replacement of this lamp involves removing the cover of the system The instructions for replacing these lamps are not included in this User M...

Page 61: ...LACE Q GARD AND QUANTUM Alert message REPLACE Q GARD PACK Removing Remove the used Q Gard Pack by following the steps below Step Action Diagram 1 Place the system into STANDBY Mode 2 Push the POD Plun...

Page 62: ...s removed in a few moments Placing Follow the steps below to install a new Q Gard Pack Step Action Diagram 1 Remove the covers on the 2 ports of the Q Gard Pack Look inside the ports Make sure the rub...

Page 63: ...ction Diagram 3 Push the Pack Locking Handle down Close the left door Quantum Cartridge The Quantum Cartridge should be replaced whenever the Q Gard Pack is replaced in order to ensure optimal water q...

Page 64: ...rtridge should be replaced whenever the Q Gard Pack is replaced Removing Follow the steps below to remove the used Quantum Cartridge Step Action Diagram 1 Place the System into STANDBY Mode 2 Push the...

Page 65: ...ction Diagram 1 Remove the covers on the 2 ports of the Quantum Cartridge Wet the O rings with water 2 Install the Quantum Cartridge until it is fully seated Close the right door 3 When a new Quantum...

Page 66: ...e System accessories bag Screw the barbed fitting onto the POD Unit NOTE Do not use any white tape on the threads of the barbed fitting An O ring is located inside the POD Unit Push one end of the cle...

Page 67: ...d Rinsing continued Step Action Diagram 4 Dispense water for about 10 minutes This flushes out any trapped air in the System This also rinses off the purification media located in the Q Gard Pack and...

Page 68: ...f there is any trapped air Close the vent after this Basing on LCD message The POD Pak needs replacement when the following Alert message is displayed Alert message REPLACE POD PAK Placing and flushin...

Page 69: ...tem 69 Replacing a POD Pak Continued Registering continued Step Action Diagram 4 Scroll down to Install POD Pak 5 Press 6 Press 7 In this example the replacement POD Pak is a Millipak Press 8 Press Co...

Page 70: ...70 Milli Q Reference System Replacing a POD Pak Continued Registering continued Step Action Diagram 9 Press 10 Press 3 times on...

Page 71: ...clogged Procedure Follow the steps below to clean the Inlet Strainer Step Action 1 Go to STANDBY Mode 2 Shut off the feedwater supply 3 Unscrew the Inlet Strainer from the feedwater supply 4 Detach t...

Page 72: ...System Cleaning the Inlet Strainer Continued Registering continued Step Action Diagram 2 Select Menu Press 3 Select Maintenance Press 4 Select Clean Strainer Press 5 A picture is shown Press 6 Press C...

Page 73: ...Milli Q Reference System 73 Cleaning the Inlet Strainer Continued Registering continued Step Action Diagram 7 Press 3 times on 8 Go to READY Mode...

Page 74: ...led such as a POD Pak or Q Gard Pack and Quantum Cartridge sensor or major component is changed feedwater parameter has changed such as the pressure setting of pressure regulator larger or smaller Res...

Page 75: ...he Alarm messages shown on a System Specifically this chapter explains how an Alarm message is displayed to read an Alarm message to cancel an Alarm and shows a list of Alarm messages Contents This ch...

Page 76: ...automatically stop the System from dispensing water An example of this is the Alarm message QUANTUM CARTRIDGE OUT The text display of this type of Alarm can be cancelled for one hour by using the Keyp...

Page 77: ...isted under the System Alarms LCD See the section View Operation for information on how to access this LCD Viewing an Alarm Message Follow the steps below to view an Alarm message Step Action Diagram...

Page 78: ...hour Alarm before cancelling In this example the Alarm message is MILLI Q T MAX Main Display LEDs Main Display Cancelling an Alarm message procedure Follow the steps below to cancel an Alarm message...

Page 79: ...79 Alarm Information Continued Alarm after cancelling the text display Main Display LEDs Main Display Alarm fixed Now suppose a Millipore SAS Service Representative fixes the cause of the Alarm Main D...

Page 80: ...FEED C MAX The feedwater conductivity is out of measurement range Contact Millipore SAS MILLI Q FEED T MIN The feedwater temperature is out of measurement range Contact Millipore SAS MILLI Q FEED T M...

Page 81: ...ot installed correctly or it has been removed The System stops operating Verify that the Q Gard Pack is installed correctly Contact Millipore SAS if the problem continues QUANTUM CARTRIDGE OUT The Qua...

Page 82: ...he Alert messages shown on a System Specifically this chapter explains how an Alert message is displayed to read an Alert message to cancel an Alert and shows a list of Alert messages Contents This ch...

Page 83: ...an immediate maintenance request Examples An example of a minor alert message would be REPLACE POD PAK IN 15 DAYS An example of a major alert message would be REPLACE POD PAK Main Display An Alert me...

Page 84: ...ystem Alert information Continued Viewing an Alert Message Follow the steps below to view an Alert message Step Action Diagram 1 Start in either READY or STANDBY Mode 2 Press 3 Press 4 Press 5 Press C...

Page 85: ...onsumable using the Keypad see below or a Major Alert message is shown This eliminates the Minor Alert message Example Before cancelling the Minor Alert message is Replace POD Pak in 15 Days Main Disp...

Page 86: ...cedure A Major Alert message can be cancelled by performing the maintenance action i e replace consumable or using the Keypad This cancels the display of the Major Alert message for 24 hours Example B...

Page 87: ...t after cancelling The Alert message has been cancelled but the cause of the message is still active Main Display LEDs Main Display Major Alert consumable replaced The Alert message has been cancelled...

Page 88: ...llipore SAS about ordering a replacement Q Gard Pack and Quantum Cartridge NEXT CALIBRATION VISIT IN XX DAYS The System is prompting you that a Calibration Visit should be scheduled Contact Millipore...

Page 89: ...XX DAYS The System has determined that the Quantum Cartridge should be replaced in XX days where XX is 15 1 Replace the Quantum Cartridge REPLACE UV 185 NM LAMP The System has determined that the UV...

Page 90: ...le EDS Pak uses EDSKIT001 Q Gard T1 Pack QGARDT1X1 Q Gard T2 Pack QGARDT2X1 Q Gard T3 Pack QGARDT3X1 Quantum TEX Cartridge QTUM0TEX1 Quantum TIX Cartridge QTUM0TIX1 UV 185 nm Lamp ZMQUVLP01 Accessorie...

Page 91: ...onsists of a Milli Q Reference System Cabinet and Q Gard Pack Quantum Cartridge and POD Pak Note Regularly scheduled preventive maintenance calibration will help you obtain the best performance from y...

Page 92: ...Milli Q Reference System FTPF11373 V 2 0 03 2013...

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