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Metrohm 917 Coulometer, Manual - Short Instructions

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Metrohm AG
CH-9100 Herisau
Switzerland
Phone +41 71 353 85 85
Fax +41 71 353 89 01
[email protected]
www.metrohm.com

917 Coulometer

Manual – Short Instructions

8.917.8002EN / 2019-11-20

 

Summary of Contents for 917 Coulometer

Page 1: ...917 Coulometer Manual Short Instructions 8 917 8002EN 2019 11 20...

Page 2: ......

Page 3: ...Metrohm AG CH 9100 Herisau Switzerland Phone 41 71 353 85 85 Fax 41 71 353 89 01 info metrohm com www metrohm com 917 Coulometer Manual Short Instructions 8 917 8002EN 2019 11 20...

Page 4: ...echcom metrohm com This documentation is protected by copyright All rights reserved This documentation has been prepared with great care However errors can never be entirely ruled out Please send comm...

Page 5: ...ront of the instrument 8 4 2 Rear of the instrument 9 5 Installation 10 5 1 Setting up the instrument 10 5 1 1 Packaging 10 5 1 2 Checks 10 5 1 3 Location 10 5 2 Setting up the titration cell for coul...

Page 6: ...e 26 5 6 5 Connecting a PC keyboard 27 5 6 6 Connecting a barcode reader 27 5 7 Connecting the Coulometer to a network 28 6 Operation 29 6 1 Switching the instrument on and off 29 6 2 Fundamentals of...

Page 7: ...7 Connecting the power supply unit 16 Figure 8 Unscrewing the protective cap from the generator electrode 18 Figure 9 Screwing the electrode cable to the generator electrode 18 Figure 10 Connecting a...

Page 8: ......

Page 9: ...al contains important information concerning the 917 Coulometer In addition to an introduction safety instructions and an overview of the instrument you will also find information about the installati...

Page 10: ...s storage medium you can not only store your methods and determinations but also create a backup together with all of the data and settings of your system The integrated Ethernet connector is availabl...

Page 11: ...connecting tubing for replacing reagent using the built in pump 2 1 3 Intended use The 917 Coulometer is designed for usage as a titrator in analytical labora tories Its main application field is coul...

Page 12: ...ameter in the software File New Menu or menu item Next Button or key WARNING This symbol draws attention to a possible life threat ening hazard or risk of injury WARNING This symbol draws attention to...

Page 13: ...cal safety when working with the instrument is ensured as part of the international standard IEC 61010 WARNING Only personnel qualified by Metrohm are authorized to carry out service work on electroni...

Page 14: ...ions well by hand Avoid applying excessive force to tubing con nections Damaged tubing ends lead to leakage Appropriate tools can be used to loosen connections Check the connections regularly for leak...

Page 15: ...U WEEE Waste Electrical and Electronic Equipment The correct disposal of your old instrument will help to prevent negative effects on the environment and public health More details about the disposal...

Page 16: ...pens the print dialog 6 Key Pressing the key pumps air into the solvent bottle The overpressure in the solvent bottle pushes solvent into the titration cell 7 Key Pressing the key aspirates air out of...

Page 17: ...rature sensors Pt1000 or NTC Two B sockets 2 mm 5 MSB connector MSB 1 and MSB 2 Metrohm Serial Bus For connecting external dosing devices stirrers or a Remote Box Mini DIN 8 pin 6 Generator electrode...

Page 18: ...pt check whether the shipment has arrived com plete and without damage by comparing it with the delivery note 5 1 3 Location The instrument has been developed for operation indoors and may not be used...

Page 19: ...ell on the magnetic stirrer as follows 1 Attach the 6 2047 040 titration vessel holder to the magnetic stirrer 2 Insert the 6 1464 320 titration cell into the titration vessel holder 5 2 2 Preparing t...

Page 20: ...the cotton too tightly 2 Fill the molecular sieve up to of the height 3 Place a small cotton plug on the molecular sieve Do not pack the cotton too tightly 4 Seal the adsorber tube with the appropria...

Page 21: ...lows 1 Place the 6 1903 030 stirring bar in the titration cell 2 Cut the 6 2713 0x0 ground joint sleeves to the correct length and attach them to the ground joints of the inserts electrodes adsorber t...

Page 22: ...Proceed as follows when using a generator electrode without a dia phragm 1 Fill approximately 100 mL of reagent into the titration cell using the 6 2738 000 funnel 2 Close the remaining ground joint...

Page 23: ...dition and aspiration tube 3 Attach the 6 2713 000 ground joint sleeve that has been cut to size to the ground joint of the addition and aspiration tube 4 Insert this assembly into the ground joint op...

Page 24: ...DC This is connected to the power socket of the coulometer WARNING An incorrect supply voltage can damage the instrument Operate the instrument only with the supply voltage specified for it Use the su...

Page 25: ...switch before you disconnect the electricity supply If this is not done then there is a danger of data loss 5 4 Connecting sensors The measuring interface contains the following measuring inputs Gen f...

Page 26: ...m the generator elec trode 2 Tighten the 6 2104 120 electrode cable to the generator electrode 2 6 2104 120 Figure 9 Screwing the electrode cable to the generator electrode Connecting the electrode ca...

Page 27: ...tection If you wish to pull out the plug again you first need to pull back the outer plug sleeve 5 4 2 Connecting indicator electrodes Screwing the electrode cable to the indicator electrode 1 Unscrew...

Page 28: ...er 2 6 2104 020 Figure 12 Screwing the electrode cable to the indicator electrode Connecting the electrode cable to the coulometer 1 Plug the electrode plug into the Ind socket of the coulometer Figur...

Page 29: ...back the outer plug sleeve 5 4 3 Connecting a temperature sensor A temperature sensor of the Pt1000 or NTC type can be connected to the Temp connector Connect the temperature sensor as follows 1 Inse...

Page 30: ...pin Mini DIN socket and be controlled simultaneously by the Coulometer In addition to the connec tion cable stirrers and the Remote Box are each equipped with their own MSB socket for this purpose NO...

Page 31: ...ng on the MSB connector see figure 15 page 23 Figure 15 MSB connector CAUTION Switch off the Coulometer before you plug in MSB devices When it is switched on the Coulometer automatically recognizes wh...

Page 32: ...via the 6 2148 010 Remote Box In addition to Metrohm other instrument manufacturers also use similar connectors that make it possible to connect different instruments together These interfaces are al...

Page 33: ...with its own power supply Connect the USB hub as follows 1 With the help of the 6 2151 030 cable length 0 6 m or the 6 2151 020 cable length 1 8 m connect the USB connector of the Coulometer Type A wi...

Page 34: ...nce Mettler AM PM PE with interface option 016 or Mettler AJ PJ with interface option 018 6 2146 020 6 2125 010 Also from Mettler ME 47473 adapter and either ME 42500 hand switch or ME 46278 foot swit...

Page 35: ...r 6 Enter and configure the balance in the device manager of the Coul ometer 7 Make sure that the parameters of the USB RS 232 adapter config ured in the device manager match those of the balance 5 6...

Page 36: ...r 02 STX or Ctrl B is sent as the first character This first character is normally referred to as the Preamble or Prefix Code 5 Program the barcode reader in such a way that the ASCII character 04 EOT...

Page 37: ...ICE English is set as the default dialog language when the instrument is switched on for the first time Information about changing the dialog language can be found in the chapter Selecting the dialog...

Page 38: ...are function The preparing of the buret unit is described in the chapter Manual control of the detailed manual Confirm the message with OK The main dialog is displayed Switching off the instrument CAU...

Page 39: ...mply touch a few of the buttons on the interface to learn how a touch sensitive screen reacts You can always return to the main dialog by touching In order to activate an element on the 917 Coulometer...

Page 40: ...dialog displayed Print opens the printing dialog Manual opens the manual control Stop cancels the running determination Start starts a determination The file name of the loaded method the time and the...

Page 41: ...check box can also be activated or deactiva ted by tapping on it 6 2 3 Status display The current status of the system is displayed in the upper right hand cor ner of the title bar Table 3 Status dis...

Page 42: ...g the modification Delete entry The content of the input field is deleted com pletely The character in front of the cursor is deleted The cursor within the input field is shifted to the left by one ch...

Page 43: ...field is deleted com pletely off If not only numbers but also special values e g off can be entered then the corresponding but tons will be shown to the right of the numerical keypad R1 For many para...

Page 44: ...ve regarding the precise terms and conditions involved in concluding a corresponding maintenance agreement For detailed information on this topic please visit www metrohm com Cleaning Cleaning the sur...

Page 45: ...ment Switch off 30 Switch on 29 K Keyboard Connect 27 KFC 2 M Metrohm Serial Bus 9 Metrohm Serial Bus MSB see also MSB 22 Molecular sieve Replace 12 MSB Connect devices 22 MSB connector 9 N Network co...

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