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3 Installation

867 pH Module

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21

Balance

Cable

Ohaus Voyager, Explorer, Analyti-
cal Plus

Cable AS017-09 from Ohaus

Precisa balances with RS-232-C
interface

6.2125.080 + 6.2125.010

Sartorius MP8, MC, LA, Genius,
Cubis

6.2134.060

Shimadzu BX, BW

6.2125.080 + 6.2125.010

Operation with Touch Control

Connect the balance as follows:

 

1

Plug in the USB plug of the USB/RS-232 adapter at the USB connec-
tor of the 867 pH Module.

 

2

Connect the RS-232 interface of the USB/RS-232 adapter with the
RS-232 interface of the balance (see table for cable).

 

3

Switch on the Touch Control.

 

4

Switch on the balance.

 

5

Activate the RS-232 interface of the balance if necessary.

 

6

Configure the RS-232 interface of the USB/RS-232 adapter in the
device manager of the Touch Control (see Touch Control manual).

3.4.5 

Connecting a PC keyboard (only for operation with Touch Con-
trol)

The PC keyboard is used as an aid for text and numerical input.

Connect the PC keyboard as follows:

 

1

Insert the USB plug of the keyboard into one of the USB sockets of
the 867 pH Module.

 

2

Switch on the Touch Control.

The keyboard is recognized automatically and entered in the device
manager.

Summary of Contents for 867 pH Module

Page 1: ...867 pH Module Manual 8 867 8003EN 2020 03 03...

Page 2: ......

Page 3: ...Metrohm AG CH 9100 Herisau Switzerland Phone 41 71 353 85 85 Fax 41 71 353 89 01 info metrohm com www metrohm com 867 pH Module Manual 8 867 8003EN 2020 03 03...

Page 4: ...echcom metrohm com This documentation is protected by copyright All rights reserved This documentation has been prepared with great care However errors can never be entirely ruled out Please send comm...

Page 5: ...roller 9 3 2 1 Operation 9 3 3 Connecting MSB devices 14 3 3 1 Connecting a dosing device 15 3 3 2 Connecting a stirrer or titration stand 16 3 3 3 Connecting a Remote Box 17 3 4 Connecting USB device...

Page 6: ...5 1 General 30 6 Appendix 32 6 1 Remote interface 32 6 1 1 Pin assignment of the remote interface 32 7 Technical specifications 36 7 1 Measuring interface 36 7 1 1 Potentiometry 36 7 1 2 Temperature 3...

Page 7: ...11 Connecting a printer 20 Figure 12 Connecting a pH metal or ion selective electrode 23 Figure 13 Connecting a reference electrode 24 Figure 14 Connecting a polarizable electrode 24 Figure 15 Connec...

Page 8: ......

Page 9: ...Barcode Reader U S B R S 2 3 2 C o n v e r t e r Touch Control USB Sample Processor Robotic Titrosampler USB Hub Relay Box Remote Box Balance Dosing Interface Dosino Stirrer Ti Stand Dosimat On Statu...

Page 10: ...de readers or additional control instruments USB Sample Processor Titrando Dosing Interface etc can be connected Measuring interface One measuring input each for a potentiometric electrode pH metal or...

Page 11: ...listed separately only in tiamo In Touch Control the electrode test is part of the CAL calibration mode Dosing commands The following commands for dosing can be selected PREP rinsing the cylinder and...

Page 12: ...ard due to heat or hot instrument parts WARNING This symbol draws attention to a possible biological hazard CAUTION This symbol draws attention to possible damage to instruments or instrument parts NO...

Page 13: ...ous injury if live components are touched There are no parts inside the housing which can be serviced or replaced by the user Supply voltage WARNING An incorrect supply voltage can damage the instrume...

Page 14: ...their disposal 1 5 4 Recycling and disposal This product is covered by European Directive 2012 19 EU WEEE Waste Electrical and Electronic Equipment The correct disposal of your old instrument will hel...

Page 15: ...2 Overview of the instrument 867 pH Module 7 2 Overview of the instrument Figure 2 Front 867 pH Module 1 On LED Lights up when the pH Module is ready for operation...

Page 16: ...ecting polarizable electrodes e g double Pt wire electrodes Socket F 5 Electrode connector iConnect For connecting electrodes with integrated data chip iTrodes 6 Connector Controller For connecting a...

Page 17: ...nt in a location of the laboratory which is suitable for operation and free of vibrations and which provides protection against corrosive atmosphere and contamination by chemicals The instrument shoul...

Page 18: ...Control connection cable into the Controller socket Figure 4 Connecting the Touch Control 2 Connect the MSB devices see chapter 3 3 page 14 Connect the USB devices see chapter 3 4 page 18 3 Connect t...

Page 19: ...ermitted is 5 m 3 2 1 2 Connecting the instrument to the power grid WARNING Electric shock from electrical potential Risk of injury by touching live components or through moisture on live parts Never...

Page 20: ...ter Cable connection and driver installation A driver installation is required in order to ensure that the 867 pH Module is recognized by the computer software To accomplish this you must comply with...

Page 21: ...completed and the instrument is ready for oper ation If problems should occur during installation contact your company s IT support team NOTICE The plug on the instrument end of the 6 2151 000 control...

Page 22: ...four connectors on what is referred to as the Metrohm Serial Bus MSB Various kinds of peripheral devices can be connected in sequence in series as a Daisy Chain at a single MSB connector 8 pin Mini D...

Page 23: ...zes which device is connected to which MSB connector The operating unit or the control software enters the connected MSB devices into the system configuration device manager MSB connections can be ext...

Page 24: ...c stirrer stirring from above 804 Ti Stand with rod stirrer 802 Stirrer Connect a stirrer or a titration stand as follows 1 Connecting the stirrer or titration stand Exit the control software Connect...

Page 25: ...are also frequently given the designations TTL Logic I O Control or Relay Control and they generally have a signal level of 5 volts Control signals are understood to be electrical line statuses or ele...

Page 26: ...concerning the pin assignment of the interface on the Remote Box in the appendix 3 4 Connecting USB devices 3 4 1 General The 867 pH Module has two USB connectors type A sockets for periph eral device...

Page 27: ...manual for the hub 3 Switch on the Touch Control The USB hub is recognized automatically 3 4 3 Connecting a printer Printers that are connected to the 867 pH Module with Touch Control must meet the fo...

Page 28: ...lances that you can use together with the 867 pH Module and of which cable you will need for connection to the RS 232 interface Balance Cable AND ER FR FX with RS 232 inter face OP 03 6 2125 020 6 212...

Page 29: ...r with the RS 232 interface of the balance see table for cable 3 Switch on the Touch Control 4 Switch on the balance 5 Activate the RS 232 interface of the balance if necessary 6 Configure the RS 232...

Page 30: ...Touch Control see Touch Control manual Settings on the barcode reader Program the barcode reader as follows see also the manual for the bar code reader 1 Switch the barcode reader to programming mode...

Page 31: ...a polarizable electrode iConnect for an iConnect measuring interface for electrodes with integrated data chip so called iTrodes 3 5 1 Connecting a pH metal or ion selective electrode Connect the pH m...

Page 32: ...ce electrode 3 5 3 Connecting a polarizable electrode Connect the polarizable electrode as follows 1 Plug the electrode plug into the Pol socket of the 867 pH Module Figure 14 Connecting a polarizable...

Page 33: ...a temperature sensor or an electrode with integrated temperature sensor NOTICE Always insert the red plug into the red socket This is the only way that shielding against electrical interference can be...

Page 34: ...ni USB adapter cable is connected to the instru ment The 854 iConnect can also be connected while the instrument is switched on 1 Plug the plug of the 854 iConnect 3 into the socket of the mini USB ad...

Page 35: ...recess in the 854 iConnect 4 Figure 19 Aligning the guide pin 3 Attach the electrode to the 854 iConnect Figure 20 Attaching the electrode The guide pin guarantees correct connection in such a way th...

Page 36: ...le the instrument is switched on 1 Unplug the 854 iConnect 3 from the socket of the mini USB adapter cable 2 Figure 21 Unplugging the 854 iConnect 2 Leave the mini USB adapter cable 2 plugged into the...

Page 37: ...TION Although this is largely prevented by design measures the power plug should be unplugged immediately if aggressive media have found their way into the interior of the instrument to prevent seriou...

Page 38: ...Replace the measuring chain No or heavily fluctu ating measuring sig nal The measuring chain is not connected Connect the measuring chain Air is trapped in or in front of the diaphragm Remove the air...

Page 39: ...er measurements in water free solutions Between measurements place separate elec trodes in distilled water and combined elec trodes in reference electrolyte The buffer or standard solutions are old Us...

Page 40: ...te Box 1 Cable For connecting to the pH Module 2 MSB connector Metrohm Serial Bus For connecting external dosing devices or stirrers 3 Remote connector For connecting instruments with a remote interfa...

Page 41: ...bles offer information concerning the assignment of the individual pins and their function Table 1 Inputs and outputs of the remote interface Assignment Pin No Function Input 0 21 Start Input 1 9 Stop...

Page 42: ...e time of activation tpulse 100 ms Quit The current command in the determination run will be canceled at the time of activation tpulse 100 ms Ready The instrument is ready to receive a start signal Co...

Page 43: ...6 Appendix 867 pH Module 35 Function Explanation Warning The line is set for warning message display...

Page 44: ...for separate reference electrodes Input resistance 1 1012 Offset current 1 10 12 A under reference conditions Measuring mode pH Measuring range 13 20 pH Resolution 0 001 pH Measuring accuracy 0 003 p...

Page 45: ...uring range 10 40 C 1 digit without sensor error under reference conditions 7 1 3 Polarizer One measuring input Pol for polarizable electrodes Measuring mode Ipol Determination with adjustable polariz...

Page 46: ...60 Hz Power consump tion 45 W Fuse 2 x 1 6 ATH 7 3 Ambient temperature Nominal function range 5 45 C at a maximum of 85 humidity Storage 20 60 C Transport 40 60 C 7 4 Reference conditions Ambient temp...

Page 47: ...pply Mini DIN socket for connecting Touch Control or computer for controlling the 867 pH Module Touch Control With integrated Touch Control cable Computer With 6 2151 000 cable MSB connectors Metrohm...

Page 48: ...r Internet browser 2 Enter the article number e g 867 into the search field The search result is displayed 3 Click on the product Detailed information regarding the product is shown on various tabs 4...

Page 49: ...trode test ELT 3 Electrostatic charge 5 EMPTY 3 I Installation Driver software 12 Instrument description 2 Instrument type 8 K Keyboard Connect 21 L LQH 3 M Maintenance 29 MEAS 2 Measured value 30 Uns...

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