Koehler K12212 Operation And Instruction Manual Download Page 7

K12212 / K12219 12-Unit Oxidation Bath 

Operation and Instruction Manual 

 

K12212-Manual 

 

 

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1  Introduction 

 

The  Koehler  12-Unit  Oxidation  Bath  is  a 

constant  temperature  oil  bath  with  solid  state 
temperature  control,  calibrate  flow  meters  and  a 
condenser  water  manifold  for  oxidation  stability 
tests on fuels and lubricants. The unit is composed 
of  an  oxidation  bath  with  an  eight-unit  test  holder 
conforming  to  ASTM  D943,  D2274,  D2893, 
D4310,  D6158,  AOCS  CD12-57,  DIN  51586,  DIN 
51587,  ISO  and  DIN  51587  specifications,  which 
evaluates  the  oxidation  characteristics  of  oils  in 
the  presence  of  oxygen  and  catalysts  at  elevated 
temperatures.  
 

This  manual  provides  important  information 

regarding  safety,  technical  reference,  installation 
requirements,  operating  condition  specifications, 
user  facility  resource  requirements,  and  operating 
instructions  for  the  12-Unit  Oxidation  Bath  and 
Data  Acquisition  Software.  This  manual  should 
also  be  used  in  conjunction  with  applicable 
published  laboratory  procedures.  Information  on 
these procedures is given in section 1.2. 

 

1.1 

Koehler’s 

Commitment 

to 

Our 

Customers 

 

Providing  quality  testing  instrumentation  and 

technical support services for research and testing 
laboratories  has  been  our  specialty  for  more  than 
50  years.  At  Koehler,  the  primary  focus  of  our 
business  is  providing  you  with  the  full  support  of 
your  laboratory  testing  needs.  Our  products  are 
backed  by  our  staff  of  technically  knowledgeable, 
trained  specialists  who  are  experienced  in  both 
petroleum products testing and instrument service 
to  better  understand  your  requirements  and 
provide  you  with  the  best  solutions.  You  can 
depend on Koehler for a full range of accurate and 
reliable instrumentation as well as support for your 
laboratory  testing  programs.  Please  do  not 
hesitate  to  contact  us  at  any  time  with  your 
inquiries  about  equipment,  tests,  or  technical 
support. 

 

Toll Free: 1-800-878-9070 (US only) 
Tel: +1 631 589 3800 
Fax: +1 631 589 3815 
 
Email: [email protected] 
http://www.koehlerinstrument.com 

 

1.2  Recommended 

Resources 

and 

Publications 

 

1.  American  Society  for  Testing  and  Materials 

(ASTM) 
100 Barr Harbor Drive 
West  Conshohocken,  Pennsylvania  19428-
2959, USA 
Tel: +1 610 832 9500  
Fax: +1 610 832 9555 

http://www.astm.org

 

email: [email protected] 

 

ASTM Publication: 

  ASTM D943: Oxidation Characteristics of 

Inhibited Mineral Oils 

  ASTM D2274: Oxidation Stability of Distillate 

Fuel Oil 

  ASTM D2893: Oxidation Characterisitics of 

Extreme Pressure Lubrication Oils 

  ASTM D4310: Determination of Sludging 

and Corrosion Tendencies of Inhibited 
Mineral Oils 

  ASTM D6158: Standard Specification for 

Mineral Hydraulic Oils 

 
2.  International  Organization  for  Standardization 

(ISO) 
1, rue de Varembé 
Case postale 56 
CH-1211 Geneva 20, Switzerland 
Tel: 41 22 749 01 11  
Fax: 41 22 733 34 30 
http://www.iso.org 

 

ISO Publication: 

 

ISO  4263:  Petroleum  and  Related 
Products 

–  Determination  of  the  ageing 

behavior  of  inhibited  oils  and  fluids 

– 

TOST test  

 

ISO  12205:  Petroleum  Products 

– 

Determination of the Oxidation Stability of 
Middle Distillate Fuels 

 
3.  Energy Institute (IP) 

61 New Cavendish Street 
London, WIM 8AR, United Kingdom 
Tel: 44 (0)20 7467 7100  
Fax: 44 (0)20 7255 1472 
http://www.energyinstpubs.org.uk/ 
 

4.  Deutsche International Norm (DIN) 

http://www.din.de 

 

DIN Publication: 

Summary of Contents for K12212

Page 1: ...Avenue Bohemia New York 11716 1796 USA Toll Free 1 800 878 9070 US only Tel 1 631 589 3800 Fax 1 631 589 3815 http www koehlerinstrument com e mail info koehlerinstrument com Petroleum Testing Analys...

Page 2: ......

Page 3: ...he applicable standards set forth in this certification Specifications ASTM D943 ASTM D2274 ASTM D2893 ASTM D4310 ASTM D6158 ACOS CD12 57 DIN 51586 DIN 51587 ISO 4263 ISO 12205 NF M 07 047 NF T 60 150...

Page 4: ...K12212 K12219 12 Unit Oxidation Bath Operation and Instruction Manual K12212 Manual 2...

Page 5: ...r Running Tests 8 4 3 Temperature Controller Operation 9 5 Operation 10 5 1 Bath 10 5 2 Power 11 5 3 Oxidation Cell Assembly 11 5 4 Flowmeter Calibration Procedure 11 5 5 Flowmeter Calibration Data 11...

Page 6: ...K12212 K12219 12 Unit Oxidation Bath Operation and Instruction Manual K12212 Manual 4 11 Warranty 16 12 Returned Goods Policy 17 Notes 18...

Page 7: ...nstrument service to better understand your requirements and provide you with the best solutions You can depend on Koehler for a full range of accurate and reliable instrumentation as well as support...

Page 8: ...s prior to use Equipment Modifications and Replacement Parts Any modification or alteration of this equipment from that of factory specifications is not recommended voids the manufacturer warranty pro...

Page 9: ...performing any maintenance and or cleaning Do NOT turn the power on unless the bath is filled with the proper medium otherwise damage may occur to the unit and the warranty will be void Air Supply Req...

Page 10: ...e bath medium for bath temperature uniformity 8 Oxidation Test Cell Assembly Oil Sample is placed within oxygen test tube and is contacted with oxygen in the presence of water and an iron copper catal...

Page 11: ...umber Description K122 0 18 Oxygen Delivery Tube K122 0 19 Oxidation Test Tube K122 0 20 Condenser 250 000 40C ASTM 40C Thermometer Range 72 to 126 C For ASTM D2893 Part Number Description K12212 D289...

Page 12: ...automatically store the value The lower green display will stop flashing If further adjustments are necessary press the Program Key again Resume regular operations by pressing the Exit Function key t...

Page 13: ...strument it is necessary to have an additional Calibrated and Certified Flowmeter capable of reading the air flow rate for your desired range 1 Connect the air source to the Calibrated and Certified F...

Page 14: ...r K12212 K12219 12 Unit Oxidation Bath is equipped with Over temperature Protection OTP circuitry which prevents the unit from exceeding unsafe operating temperatures If the unit cannot maintain the s...

Page 15: ...03 036 RTD Temperature Safety Limit 120V 275 103 037 RTD Temperature Safety Limit 230V 278 001 002 Slow Blow Fuse 1A 5x20 mm 278 040 001 Time Delay Fuse 40A 278 030 002 Time Delay Fuse 30A 600VAC 278...

Page 16: ...K12212 K12219 12 Unit Oxidation Bath Operation and Instruction Manual K12212 Manual 14 Wiring Diagrams 8 1 K12212 Unit Wiring...

Page 17: ...K12212 K12219 12 Unit Oxidation Bath Operation and Instruction Manual K12212 Manual 15 8 2 K12219 Unit Wiring...

Page 18: ...K12219 12 Unit Oxidation Bath should not require service Any service problem can be quickly resolved by contacting Koehler s technical service department either by letter phone fax or email In order...

Page 19: ...tem s to be returned and the reason for the return You will be issued a Returned Authorization RA number which must be prominently displayed on the shipping container when you return the material to o...

Page 20: ...K12212 K12219 12 Unit Oxidation Bath Operation and Instruction Manual K12212 Manual 18 Notes...

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