KAM Simple Precision LKF User Manual Download Page 8

8

KFMANUAL 0317

KAM CONTROLS, INC.

Place a funnel in stopper hole at the top of the Cathode Solution Cell 

(G)

 and pour entire 

contents of KAM

®

 Generator Solution C (5 ml) ampoule into the Cathode Solution Cell 

(G)

Remove funnel and place the glass Stopper 

(H)

 in place.

BASE ASSEMBLY

NOTE: Before assembling the base unit and  glassware, ensure that the unit has been turned off. 

9.

1.

2.

3.

4.

4. OPERATION continued

NOTE: Generator Solution C ampule is glass. To open, hold the ampule in a paper or cloth towel, 

and apply pressure to the top of the ampule just above the small dot. Top should cleanly snap off 

the base of the ampule. 

Titration Cell Sleeve

Swivel Clamp

Cathode Solution 

Cell Jack (black)

Detector Electrode 

Jack (red)

Turn the swivel clamp toward back of KF unit and place the entire Generator Solution Cell 

assembly into the Titration Cell Sleeve. Turn Swivel Clamp over the top of the cell and secure by 

hand tightening the screw on top of the clamp. Do not over tighten. 

Plug the free end of the Cathode Solution Cell  Wire into the black colored jack on the side 

panel of the base unit, and the free end of the Detector Electrode Wire into the red colored jack. 

If using a portable unit, remove the power cord from packing or storage compartment and plug 

into the power jack on the back of the base. Plug unit into power source and press power but-

ton.

The power button should glow blue. If you are using a portable unit, the light will blink when the 

battery is charging. The LCD display should show the Main Menu. 

Titration Cell Assembly

Summary of Contents for Simple Precision LKF

Page 1: ...PKF Karl Fischer Moisture Analyzer TEL 1 713 784 0000 FAX 1 713 784 0001 Email Sales KAM com KAM CONTROLS INC 3939 Ann Arbor Drive Houston Texas 77063 USA User Manual KFMANUAL 0317 An ISO 9001 certif...

Page 2: ...dding reagent 7 Base assembly 8 Setting date and time 9 Reset reagent life 9 Sample size and titration mode 10 Initial titration 10 Running samples 11 moisture content determination Sample dilution 12...

Page 3: ...e maintenance program By analyzing lube oil on compressors turbines etc the Moisture Analyzer can detect cooling water leaks before they become severe enough to damage equipment Karl Fischer titrimetr...

Page 4: ...exceeds API MPMS 10 9 ASTM D4928 ISO 12937 and EI 386 Generator electrode config With diaphragm Titration speed 1000 g H2 O min max at high H2 O concentrations Power requirements Operates on either A...

Page 5: ...ion Cell Assembly Titration Cell Sleeve Power Cord Storage Silica Gel Storage Detector Electrode Wire Cathode Solution Cell Wire Swivel Clamp 3 COMPONENTS FRONT PANEL portable model shown REAR PANEL p...

Page 6: ...screen Battery Life Indicator blinks when charging USB Indicator BlueTooth Power Cord Charging portable units LCD Display main menu shown Screen Navigation Arrows ENTER Key Karl Fischer Moisture Anal...

Page 7: ...o not apply pressure to the Electrode Rather let it seat under its own weight Rotate it half a turn backward and forward to ensure the grease is spread evenly and a seal has been created Drop the cera...

Page 8: ...n Cell Jack black Detector Electrode Jack red Turn the swivel clamp toward back of KF unit and place the entire Generator Solution Cell assembly into the Titration Cell Sleeve Turn Swivel Clamp over t...

Page 9: ...set time navigate to time indicator and use the UP DOWN arrows to change the hour 24 hour clock and use the RIGHT LEFT arrows to move between fields Press ENTER to save values and return to Main Menu...

Page 10: ...5 After long periods without use the unit has been turned off and or each time the reagents have been replaced you must run an initial titration to remove any ambient moisture from the reagents and c...

Page 11: ...m the inside of the syringe The tip of the plunger should exactly align with the sample volume marking Press NEW SAMPLE key on Keypad The display will read Inject Sample and a thirty second countdown...

Page 12: ...h sample log Data for any individual sample can be retrieved by using the UP DOWN arrows to navigate to the desired sample number and pressing ENTER The display will show the date time water percentag...

Page 13: ...ill appear Type in the desired name for the output file in the format Filename xls and hit save Example August titrations xls A window will open with all the sample files listed Select all the KFF fil...

Page 14: ...G WITHTHE OPTIONAL BLUETOOTH PRINTER 1 2 3 4 5 MENU Reagent Life Date Time Saved Samples Language Calibration Version Info English 78 Aug15 98 BT Mode 09 21 BT Mode Modem Printer Scanning for Printer...

Page 15: ...ueTooth icon will appear at the top of the screen This indicates the devices have been paired successfully To print from the MAIN MENU use the navigation arrows to scroll down to Saved Samples and pre...

Page 16: ...nother record to the printer while a record is still printing NOTE if at any time the KF unit is turned off you must turn off the printer then follow the steps on page 14 of this manual to reconnect t...

Page 17: ...on the side of the printer two times in quick succession The printer will shut down Wait until the blue light on the printer stops blinking and turns off Then press the power button once more The pri...

Page 18: ...om the cell Dispose of fluids according to SDS sheet s Empty contents of Generator Solution Cell by pouring into a suitable container or aspiration Dispose of fluids according to the SDS sheet Thoroug...

Page 19: ...KF Karl Fischer Moisture Analyzer due to the potential for the other types of grease to absorb moisture and interfere with titration if it is silicon based KAM CONTROLS is not responsible for problems...

Page 20: ...night discard the nitric acid in the cell and rinse the inside and outside of the cell with running tap water until the yellow color disappears Place distilled water in the cell and place it in a 400...

Page 21: ...Calibration Verification Check Solution 1 1 ml and 10 l Gastight Syringes 14 and 19 gauge Needles package of rubber Septums 100 Funnels 2 Special Grease 1 and Silica Gel 1 REAGENTS and CONSUMABLES GL...

Page 22: ...SAMPLE INJECTION PORT P 09044 STIR BAR P 09050 DRYING TUBE P 09029 RUBBER SEPTUM pack of 100 P 09015 SPECIAL GREASE 25 g tube P 370420 REPLACEMENT RECHARGEABLE BATTERY for model 09031 P 370400 POWER...

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