CONTENTS
4. ADJUSTMENT OF MEASUREMENT CONDITIONS AND
4.1
SETTING PULSE WIDTH IN SINGLE PULSE
MEASUREMENT..................................................................................4-1
4.2
SETTING WAITING TIME IN SINGLE PULSE
MEASUREMENT..................................................................................4-2
4.3
SETTING CONTACT TIME IN CP METHOD ....................................4-3
4.4
SETTING WAITING TIME IN CP METHOD .....................................4-4
4.5
SETTING SAMPLING POINT (X_POINTS) .......................................4-5
4.6
HOW TO USE FORWARD LINEAR PREDICTION ...........................4-6
4.7
HOW TO USE BACKWARD LINEAR PREDICTION........................4-7
5.1
OUTLINE OF MULTINUCLEAR MEASUREMENT..........................5-1
5.2
METHOD OF MEASURING RARE SPIN NUCLEUS OF SPIN
1/2 ...........................................................................................................5-2
5.3
METHOD OF MEASURING
1
H/
19
F......................................................5-2
5.4
METHOD OF MEASURING NUCLEUS OF SPIN 1 ..........................5-3
5.5
METHOD OF MEASURING NUCLEUS OF HALF-INTEGER
SPIN........................................................................................................5-3
6.1
OUTLINE OF RELAXATION-TIME MEASUREMENT.....................6-1
6.2
RELAXATION TIME MEASUREMENT BY DIRECT
MEASUREMENT..................................................................................6-2
6.3
RELAXATION TIME MEASUREMENT OF
13
C BY TORCHIA
METHOD ...............................................................................................6-4
6.4
MEASUREMENT OF T
1
ρ
(T
1
IN THE ROTATING FRAME) .............6-5
6.5
RELAXATION TIME MEASUREMENT OF
1
H BY INDIRECT
OBSERVATION USING CP METHOD ................................................6-6
7.1
OUTLINE OF MQMAS METHOD.......................................................7-1
7.2
PRINCIPLE ............................................................................................7-3
7.3
ADJUSTMENT ......................................................................................7-5
7.3.1
Adjustment of Power .......................................................................7-5
7.3.2
Adjustment of Parameters ...............................................................7-6
7.4
MEASUREMENT..................................................................................7-8
7.5
PROCESSING........................................................................................7-9
7.6
APPENDIX ..........................................................................................7-12
7.6.1
Shearing process............................................................................7-12
7.6.2
Scaling Processing.........................................................................7-13
C-2
NMECAXS_V50-SLD-2
