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IKA ElektraSyn 2.0, Manual, Page: 12 / 21

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IKA ElektraSyn 2.0 Manual Download Page 12

 Start-up 

13

Start-up

/// Your ElectraSyn package

Unpack the device carefully. 

Any damage should immediately be  

reported to the carrier (mail, rail or freight forwarding company).

PREPARE STATION

SCOPE OF DELIVERY

Place single vial adapter on plate.

Note: The front of the vial adapter needs to  

be in line with the edge of the glass plate

Turn and engage (click)

Single vial holder

ElectraSyn 2.0 base unit

Power plug

IKA stir plate

Set of electrodes and single vial

1

Summary of Contents for ElektraSyn 2.0

Page 1: ...ElektraSyn 2 0...

Page 2: ...corresponds to the regula tions 2014 35 EU 2006 42 EC 2014 30 EU and 2011 65 EU and conforms with the standards or standardized documents EN 61010 1 EN 61010 2 051 EN 61326 1 EN 60529 EN ISO 12100 A...

Page 3: ...ion of warning symbols 8 General information 9 Device design 9 Permissible medium contaminants side reactions 10 Experimental procedures 10 Accessories 11 Power supply Switching off 12 Protecting your...

Page 4: ...erence Electrode RE 17 Working Electrode WE 18 Counter Electrode CE 18 CV setup 19 WARRANTY Regulations 22 SETTING UP A REACTION Basic guide 16 SMART ASSIST Take the guesswork out of Electrochemistry...

Page 5: ...hose values start stop C Menu button D Cyclic Voltammetry button E Back button F Graph button G Lock button Explication of symbols H Display I Power socket J Contact thermometer jack K Micro USB inter...

Page 6: ...rge 07 Polarity indicator 08 Actual temperature in connection with an external PT1000 sensor Display 09 Operation mode constant voltage constant current 10 USB connection with PC 11 All operation elem...

Page 7: ...ious injury Indicates practices which if not avoided can result in equipment damage Indicates a potentially hazardous situation which if not avoided can result in death serious injury Indicates a pote...

Page 8: ...and safety and accident prevention regulations Device design Danger Do not operate the device in explosive atmosphere and with hazardous substances Set up the device in a spacious area on an even stab...

Page 9: ...in other ways e g through light irradiation The stir plate can heat up due to the action of the magnets at high motor speeds Please consider any possible contaminations and unwanted chemical reaction...

Page 10: ...a depth of at least 20 mm when connected Accessories must be securely attached to the device and must not come off by themselves The center of gravity of the assembly must lie within the surface on wh...

Page 11: ...n Proper usage Basics Usage The potentiostat IKA ElectraSyn 2 0 has been designed for electrochemical reactions and mixing Unpack the device carefully Any damage to the exterior packaging should immed...

Page 12: ...er mail rail or freight forwarding company PREPARE STATION SCOPE OF DELIVERY Place single vial adapter on plate Note The front of the vial adapter needs to be in line with the edge of the glass plate...

Page 13: ...14 Start up Attach lid to vial PREPARE VIAL Put IKA FLON into vial Insert electrodes into lid Place vial on plate connection PLUG 2 3...

Page 14: ...the reaction until the set charge has passed based on mmol of substrate and equivalents of electrons F mol Timer will run the reaction for set amount of time Run continuous will run the reaction until...

Page 15: ...ctrode For example selecting power level medium will allow the ElectraSyn 2 0 to determine the current needed for a starting potential of 4 V The current determined will then be used to run a constant...

Page 16: ...tion on KCl on the frit If needed non aqueous electrolyte such as acetonitrile solution of AgNO3 could also be applied After the electrode has been lled it should be left inside a solution cont aining...

Page 17: ...above 1200 grit This electrode should be placed in the WE section of the cap There is also an indication of W and C at the top of a cap Counter Electrode CE The counter electrode consists of a platinu...

Page 18: ...5 Attach reference electrode into ElectraSyn vial lid 6 Attach working electrode and counter electrode to ElectraSyn vial lid note W and C on top of vial lid correspond to position working electrode a...

Page 19: ...ph screen will be displayed and a blue line will move across the top of the screen indicating the ElectraSyn 2 0 is collenting data When nished the CV curve will be displayed 5 When CV is complete the...

Page 20: ...acy speed 10 rpm Stirring quantity max per stirring position H2O 100 ml Length of stirring bar 20 mm Display TFT USB port yes RS 232 interface no Analogue output no Protection class to DIN EN 60529 IP...

Page 21: ...You can also send your device directly to IKA including the invoice and explaining your claim Please note that you will be responsible for the shipping costs The warranty does not cover worn out part...

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