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Hanna Instruments pH 300 Instruction Manual Download Page 54

107

106

HI 5412
Glass-body, single Calomel reference half-cell
electrode, refillable with 4mm  plug with 1m (3.3')
cable. Use: general purpose with constant tem-
perature range.

ORP  electrodes:

HI 3131B / HI 3111S
Glass-body, refillable, combination platinum
ORP electrode. Use: titration.

HI 3230B / HI 3210S
Plastic-body (Ultem

®

), gel-filled, combination

platinum ORP electrode. Use: general purpose.

HI 4430B / HI 4410S
Plastic-body (Ultem

®

), gel-filled, combination

gold ORP electrode. Use: general purpose.

120 mm

4.7"

12 mm

0.5"

HI 5412

150 mm

5.9"

12 mm

0.5"

"S" VERSION

HI 3131

120 mm

4.7"

12 mm

0.5"

HI 3230

"S" VERSION

Ultem

®

 is registered Trademark of "General Electrics Co."

120 mm

4.7"

12 mm

0.5"

HI 4430

"S" VERSION

FC 911B
Plastic-body (Kynar

®

), double junction, refill-

able with built-in amplifier, combination pH
electrode. Use: very high humidity.

HI 1413B / HI 1410S
Glass-body, single junction, flat tip, Viscolene,
combination pH electrode. Use: surface mea-
surement.

Half-cell  electrodes:

HI 2110B
Glass-body, single half-cell pH electrode. Use:
general purpose.

HI5311
Glass-body, Ag/AgCl  reference half-cell  elec-
trode, double junction, refillable with 4mm  plug
with 1m (3.3') cable. Use: general purpose with
wide temperature range.

110 mm

4.3"

12 mm

0.5"

FC 911

110 mm

4.3"

12 mm

0.5"

HI 1413

120 mm

4.7"

12 mm

0.5"

9.5mm DIA

0.37"

HI 2110

Kynar

®

 is registered Trademark of "Pennwalt Corp."

120 mm

4.7"

12 mm

0.5"

HI 5311

Summary of Contents for pH 300

Page 1: ...nch top pH mV ISE C Meters ON OFF pH METER TIME PAPER PRINT RANGE CAL PGM CFM ENTER pH302 m s 1 2 3 Rel mV mV C ppm ppm pH pH DATE TIME INTV CAL LOG MEM CFM WRONG BUF h t t p w w w h a n n a i n s t c...

Page 2: ...to make the calibration procedure easy to follow Calibration is not allowed until the electrode has stabilized to ensure accu rate measurements Through the RS 232 serial port you can transfer sample m...

Page 3: ...n values and to confirm baud rate and command prefix during communication setting mode MR to recall the stored value MS to hold and memorize the measured value The last reading will be frozen on the d...

Page 4: ...pH 0 01 ISE 0 1 mV ORP 1 mV C 0 1 Accuracy pH 0 01 20 C 68 F ISE 0 2 mV ORP 1mV C 0 5 Typical EMC pH 0 01 Deviation ISE 0 6 mV ORP 1 mV C 0 5 pH Calibration Automatic 1 or 2 points with 3memorizedbuff...

Page 5: ...proved Environment 0 to 50 C 32 to 122 F 95 RH Dimensions 280x200x75mm 11x7 9x3 Shipping Weight 1 3 kg 2 9 lb SPECIFICATIONS pH 301 Keyboard on the Left CAL to start the calibration mode for pH mV and...

Page 6: ...M to select a program PRINT to obtain a printout prints time date sample number and pH or mV val ues RANGE to select the measurement range pH or mV or to display the calibration buffer or the temperat...

Page 7: ...0 1 Accuracy pH 0 01 20 C 68 F ISE 0 2 mV ORP 1mV C 0 5 Typical EMC pH 0 01 Deviation ISE 0 3 mV ORP 1 mV C 0 5 pH Calibration Automatic 1 or 2 points with 3memorizedbuffers 4 01 7 01 10 01 Temperatur...

Page 8: ...quit from the calibration mode the offset and the slope of the instrument would be set to 0 mV and 100 respectively ON OFF C pH C pH CAL OPERATIONAL GUIDE ELECTRODE AND PROBE CONNECTIONS For combinat...

Page 9: ...when fully charged The battery is automatically charged any time the meter is plugged in either turned on or off If you need to unplug the instrument press OFF before disconnecting the meter from the...

Page 10: ...me The hour and the minutes will be displayed on the primary LCD the logging interval on the secondary one RANGE TIME INTV C C CAL DATE DATE TIME s TIME INTV Press CAL to exit the date setting mode Pr...

Page 11: ...ture In order for the meter to measure the pH accurately temperature must be taken into consideration A perfect equilibrium between the pH elec trode and the sample is reached in approxi mately 15 min...

Page 12: ...will display the last pH calibration data C C DATE CAL 1 mV pH CAL 2 mV pH CAL pH CAL DATA as close to the electrode as possible and wait for 1 2 minutes If you know the temperature of the sample to...

Page 13: ...ss than 400 mV tenths of mV are displayed for values greater than 400 mV the decimal digit disappears 3 mV pH CAL Rel mV C mV RANGE 4 cm 1 Press UP or DOWN to get this information in the following seq...

Page 14: ...s UP or DOWN to get this information in the fol lowing sequence Rel mV C C ppm Rel mV CAL DATA ION C C Note that the change in scale from 0 1 mV to 1 mV as resolution is automatic For all models appea...

Page 15: ...H MEM a Date of the last ION calibration month day and year b Time when the last ION calibration was completed hour and minutes c Offset calibration value expressed in mV and displayed on the primary...

Page 16: ...Pour small quantities of pH7 01 HI7007 HI8007 and pH4 01 HI7004 HI8004 and or pH10 01 HI7010 HI8010 solution into individual beakers If possible use plastic beakers to minimize any EMC interferences F...

Page 17: ...you are going to measure acid samples or pH 7 01 and pH 10 01 for alka line measurements or for pH301 only per form a 3 point calibration for the entire range PROCEDURE Press RANGE for pH300 and pH302...

Page 18: ...ond buffer solution pH 4 01 or pH10 01 for pH301 only the second buffer can also be pH 1 68 or pH 9 18 and shake briefly Note the electrode should be submerged ap proximately 4 cm 1 into the solu tion...

Page 19: ...fset and the 1st slope of the meter calibrated Note the meter will automatically skip the buffer that was used for the first calibra tion to avoid erroneous calibration DATE CAL Calibration com pleted...

Page 20: ...peraturedur ingcalibration CFM CFM WRONG WRONG BUF RANGE Note during calibration the secondary LCD dis plays the selected buffervalue Bypress ing RANGE the tem perature value can be also displayed Thi...

Page 21: ...or 10 01 If the buffer temperature is at 20 C the dis play will show pH 4 00 7 03 10 06 If the buffer temperature is at 50 C the dis play will show pH 4 06 6 98 9 82 1 67 1 67 1 67 1 67 1 68 1 68 1 6...

Page 22: ...BUF C C CFM For greatest accuracy it is recommended that the instrument is calibrated frequently The standard calibration program of the meter however is prepared for 2 maximum buff ers The selectabl...

Page 23: ...CAL and the calibra tion process is ended with only the offset of the meter calibrated For best accuracy however it is recommended that a two point calibration is performed Note during calibration th...

Page 24: ...ted for the mV and is ready for measurements The cali bration data are stored in the EEPROM The ORP electrodes are interchangeable and no mV calibration is needed when the ORP electrode is replaced If...

Page 25: ...connection cable connect it to the BNC electrode socket Turn the pH302 on by pressing ON plus CFM simultaneously mV CAL CFM CFM mV CAL CFM CFM ON CFM PROCEDURE FOR pH 301 Connect the meter to the sim...

Page 26: ...imulator to 0 0 mV As soon as the reading is stable after about 10 seconds the CFM indicator will start blinking Press CFM to confirm the value The primary LCD will display 500 0 mV Set the simulator...

Page 27: ...e and is ready for measure ments The temperature probes are interchangeable and no temperature calibration is needed when the temperature probe is replaced If for any reason the temperature measure me...

Page 28: ...soon as the read ing is stable the CFM indicator will start blinking C CAL CFM 0 C 32 F C CFM 50 C 122 F C C CAL CFM CAL ON The secondary LCD will display 0 0 C with the CAL indi cator As soon as the...

Page 29: ...een 1 15 30 sec onds or 1 5 30 60 120 180 minutes Select the appropriate measurement mode by pressing the pH or mV or ION key Press LOG and then CAL to enter the log ging mode Once in the logging mode...

Page 30: ...om page 16 CFM BUF CFM ON LOG Press LOG and the primary LCD will show the current lot number and the secondary LCD will display the current page number Press LOG again to display the current sample nu...

Page 31: ...exceeded the program stops by printing the endpoint hour and minute The printout interval can be se lected from 1 minute to 24 hours This pro gram can also be stopped by selecting any other PGM functi...

Page 32: ...PROGRAM 1 1 set sample no 2 set time 3 set date Sample number 200 Program 7 To select a different printing language 6 languages are available see page 78 Program 8 To print the ion concentration in M...

Page 33: ...ple no 2 set time 3 set date Sample number 200 Time 14 00 Date 2 04 0 PGM 2 4 P1 will be displayed on the secondary LCD To set the time press 2 followed by EN TER P1 2 will be displayed on the sec ond...

Page 34: ...1st buf fer 2 enter 2nd buf fer 1st buffer 6 92 2 ENTER PROGRAM 2 pH 302 This program lets you calibrate with buffer values other than 4 01 7 01 and 10 01 pH which are pre programmed into memory To e...

Page 35: ...minute and 24 hours To enter the program press PGM and 4 The printout defines functions 1 2 and 3 1 is a start time 2 is the time interval 3 is the finish time PROGRAM 3 DATE 2 04 TIME 14 04 OFFSET m...

Page 36: ...PROGRAM 4 1 enter start time 2 enter time int erval 3 enter end time start time 10 20 time interval 00 05 2 ENTER To set the start time choice 1 press 1 followed by ENTER P4 1 will be dis played on t...

Page 37: ...m press PGM plus 5 DATE 2 04 TIME 10 20 SAMPLE 202 C 20 3 pH 6 38 DATE 2 04 TIME 10 25 SAMPLE 203 C 20 4 pH 6 39 DATE 2 04 TIME 10 30 SAMPLE 204 C 20 3 pH 6 38 LOG PGM 0 5 PGM To set the finishing tim...

Page 38: ...nter end pH mV value Start time 10 30 Time Interval 1 30 The printout defines functions 1 2 and 3 1 is a start time 2 is the time interval 3 is the interrupt value of pH mV To set the start time choic...

Page 39: ...arm DATE 2 04 TIME 10 30 SAMPLE 210 C 20 3 pH 4 50 DATE 2 04 TIME 12 00 SAMPLE 211 C 20 4 pH 4 01 DATE 2 04 TIME 12 25 SAMPLE 212 C 20 3 pH 3 50 LOG PGM 0 6 PGM To set the end pH mV value choice 3 pre...

Page 40: ...limit 2 set upper limit 3 clear alarm lower limit 6 50 upper limit 7 50 3 To set the lower limit choice 1 press 1 followed by ENTER P6 1 will be dis played on the secondary LCD with 0 on the primary o...

Page 41: ...E 10 20 ECHANTILLON 215 C 20 0 pH 6 52 PRINT 8 PGM PROGRAM 8 3 88 pH 0 132 mM H 9 PGM To definitely exit the program press PGM plus 0 PROGRAM 7 pH 302 This program allows the user to select a differen...

Page 42: ...escape character baud rate 4800 STRINGII code 25 PGM 2 ENTER The printout defines functions 1 and 2 1 is the baud rate 2 to set the STRINGII code of Escape char acter To set the baud rate choice 1 pre...

Page 43: ...ration Thereadingdrifts Display shows Display shows Display shows Display shows WRONG BUF 1 and or WRONG Display shows WRONG BUF 2 and or WRONG Rel mV C pH INTERFACE WITH PC Data transmission from the...

Page 44: ...ze clogging and assure a quick response time the glass bulb and the junc tion should be kept moist and not allowed to dry out Replace the solution in the protective cap with a few drops of HI70300 or...

Page 45: ...ctrode Slow Response Excessive Drift Soak the tip in Hanna Solution HI7061 or HI8061 for 30 minutes rinse thoroughly in dis tilled water and then follow the Cleaning Procedure above electrodes Follow...

Page 46: ...NNA pH SENSITIVE GLASS The resistance of glass electrodes partially depends on the temperature The lower the temperature the higher the resistance It takes longer for the reading to stabilize if the r...

Page 47: ...be changed using HI92000 Hanna Soft ware CFM C C COMM C C COMM ADDITIONAL INFORMATION ABOUT INTERFACE WITH PC for technical personnel only If you are not using Hanna Instruments HI92000 application so...

Page 48: ...4 Buffer used when slope was done E g 0401 for 4 01 pH 5 Slope in mV E g 000592 for 59 2 mV 6 Temperature E g _01199 for 119 9 C 00099 for 9 9 C BAR Requests the meter to send the RS232 baud rate Sel...

Page 49: ...en the slope was done E g 012345 for 1234 5 mV 6 Temperature E g _00105 for 10 5 C 00099 for 9 9 C DA Requests the meter to send the date E g 022896 for 28th Feb 96 PRE Requests the meter to send the...

Page 50: ...Offset in mV E g _00504 for 50 4 mV 00504 for 50 4 mV 4 Buffer used when slope was done E g 0401 for 4 01 pH 5 Slope in mV E g 000592 for 59 2 mV 6 Temperature E g _01199 for 119 9 C 00099 for 9 9 C T...

Page 51: ...0 mL ELECTRODE STORAGE SOLUTIONS IN FDA APPROVED BOTTLE HI80300M Storage Solution 230 mL HI80300L Storage Solution 460 mL ELECTRODE CLEANING SOLUTIONS HI7061M General Cleaning Sol 230 mL DA Requests t...

Page 52: ...rganic Cleaning Sol 230 mL HI7074L Inorganic Cleaning Sol 460 mL HI7077M Oil Fat Cleaning Sol 230 mL HI7077L Oil Fat Cleaning Sol 460 mL ELECTRODE CLEANING SOLUTIONS IN FDA APPROVED BOTTLE HI8061M Gen...

Page 53: ...t Corp HI1330B HI1310S Glass body semimicro single junction refillable combinationpHelectrode Use laboratory HI1331B HI1311S Glass body semimicro single junction refill able combination pH electrode U...

Page 54: ...ION Ultem is registered Trademark of General Electrics Co 120 mm 4 7 12 mm 0 5 HI 4430 S VERSION FC911B Plastic body Kynar double junction refill able with built in amplifier combination pH electrode...

Page 55: ...1210S 33 Solvents HI 1043B HI1040S 34 Strongacid HI 1043B HI1040S 35 Submersionapplication HI 1130B HI1110S 36 Surfacemeasurements HI 1413B HI1410S 37 Swimmingpool H1130B HI 2114B HI2910B 38 Titration...

Page 56: ...mentsreservestherighttomodify thedesign constructionandappearanceofits products without advance notice CE DECLARATION OF CONFORMITY RecommendationsforUsers Before using these products make sure that t...

Page 57: ...112 MANpH300R1 07 96 PRINTED IN ITALY h t t p w w w h a n n a i n s t c o m...

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