Hanna Instruments HI 4521 Instruction Manual Download

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HI 4521 & HI 4522

pH/mV/ISE/Temperature/

Conductivity/Resistivity/TDS/Salinity

Bench Meters

Instruction Manual

99 Washington Street
Melrose, MA 02176

Phone

781-665-

1400

Toll Free 1-800-517-8431

Visit us at www.T

estEquipmentDepot.com

Summary of Contents for HI 4521

Page 1: ...22 pH mV ISE Temperature Conductivity Resistivity TDS Salinity Bench Meters Instruction Manual 99 Washington Street Melrose MA 02176 Phone 781 665 1400 Toll Free 1 800 517 8431 Visit us at www TestEqu...

Page 2: ...NS FOR USERS Before using these products make sure they are entirely suitable for the environment in which they are used Operation of these instruments in residential areas could cause unacceptable in...

Page 3: ...prescribed maintenance is not covered If service is required contact the dealer from whom you purchased the instrument If under warranty report the model number date of purchase serial number and the...

Page 4: ...EMENT 90 TDS MEASUREMENT 91 SALINITY CALIBRATION 92 SALINITY MEASUREMENT 92 TEMPERATURE CALIBRATION 94 LOGGING 95 PC INTERFACE 100 pH BUFFER TEMPERATURE DEPENDENCE 101 PROBE CONDITIONING MAINTENANCE 1...

Page 5: ...adapter HI 4521 01 and HI 4522 01 are supplied with 12 Vdc 115 Vac adapter Note Save all packing material until you are sure that the instrument works properly Any defective item must be returned in t...

Page 6: ...out temperature compensation HI 4522 only Pure water checking using the USP 645 standard Conductivity probe automatic recognition Automatic or custom standard conductivity calibration in up to four po...

Page 7: ...NAL DESCRIPTION FUNCTIONAL DESCRIPTION FUNCTIONAL DESCRIPTION FUNCTIONAL DESCRIPTION FUNCTIONAL DESCRIPTION 110 pH ELECTRODES All electrodes part numbers ending in B are supplied with a BNC connector...

Page 8: ...ND PROBE CLEANING SOLUTIONS HI 70000P Electrode Rinse Sachets 20 mL 25 pcs HI 7061L General Purpose Solution 500 mL bottle HI 7073L Protein Cleaning Solution 500 mL bottle HI 7074L Inorganic Cleaning...

Page 9: ...ottle 500 mL HI 6004 pH 4 010 Buffer Solution 500 mL bottle HI 8006L pH 6 86 Buffer Solution in FDA approved bottle 500 mL HI 6068 pH 6 862 Buffer Solution 500 mL bottle HI 8007L pH 7 01 Buffer Soluti...

Page 10: ...o t c a f 0 0 1 h t i w S D T l a u t c a n o i t u l o s e R m p p 1 0 0 0 m p p 1 0 0 m p p 1 0 t p p 1 0 0 0 t p p 1 0 0 t p p 1 0 y c a r u c c A m p p 1 0 0 g n i d a e r f o 1 107 TEMPERATURE C...

Page 11: ...S M E L B O R P N O I T U L O S e v i s s e c x e e s n o p s e r w o l S t f i r d e d o r t c e l e H p y t r i D n i p i t e d o r t c e l e e h t k a o S 0 3 r o f n o i t u l o s 1 6 0 7 I H n a...

Page 12: ...b o r p e h t t r e s n I s w o h s y a l p s i D s t n e m e r u s a e m g n i r u d f o t u o g n i d a e R e g n a r r e t e m e h t e t a r b i l a c e R s i e l p m a s e h t k c e h C e l b a r...

Page 13: ...rodes Follow the Preparation Procedure on page 103 before taking measurements Note NEVER STORE THE ELECTRODE IN DISTILLED OR DEIONIZED WATER PERIODIC MAINTENANCE Inspect the electrode and the cable Th...

Page 14: ...GLP displaying mode Press while in Measure mode The Choose Display Configuration message will be displayed in the Reminder messages area Press The instrument will display the detailed GLP data DISPLAY...

Page 15: ...ected axis Note While in zoom graph menu the key is not accessible Press to return to the main menu 102 MEASURE Rinse the conductivity probe with distilled water Immerse the tip bottom 4 cm 1 in the s...

Page 16: ...0 1 0 0 1 4 5 4 2 1 0 3 7 2 2 3 0 7 6 1 2 7 0 3 7 0 0 4 2 8 9 6 0 3 1 7 9 5 4 9 6 1 3 0 1 9 7 3 3 1 5 8 7 2 1 4 0 7 6 1 1 5 0 3 2 0 0 4 9 4 9 6 8 9 0 7 1 9 3 9 5 4 2 0 1 8 7 1 3 1 0 1 3 8 2 0 5 1 7 6...

Page 17: ...is pressed Wrong Key If this option is ON a long beep will be heard when an incorrect key is pressed SYSTEM SETUP SYSTEM SETUP SYSTEM SETUP SYSTEM SETUP SYSTEM SETUP 100 PC INTERFACE PC INTERFACE PC I...

Page 18: ...ional Info 1 Additional Info 2 for general purpose notations 99 highlighted lot The Please wait message will be dis played on the LCD for a short period The user customised report will be displayed on...

Page 19: ...as Direct AutoHold in order to use this logging mode To log data using this mode Press while in Measure mode to start the logging session The logged values are only the ones frozen on the LCD after wa...

Page 20: ...ing period and AutoHold indicators will be displayed on the LCD To store another frozen value press again To stop the logging session press LOGGING MODE 3 This logging mode can be used for any sample...

Page 21: ...p the logging session press The Log Save screen will display thelog lot ID the settable log interval sampling Press to adjust the log interval and or the log sampling or press to save the current log...

Page 22: ...The logging behaviour is dependent on the Logging Type and Reading Mode options from the parameter setup The Logging Data Configuration options from the appropriate unit setup must be set first in ord...

Page 23: ...by using and tohighlightthedesired characterandthenpress toadditto the text bar It is also possible to delete the last character by positioning the cursor on the Backspace character and pressing Press...

Page 24: ...93 PRACTICAL SALINITY SCALE UNESCO 1978 PRACTICAL SALINITY SCALE UNESCO 1978 PRACTICAL SALINITY SCALE UNESCO 1978 PRACTICAL SALINITY SCALE UNESCO 1978 PRACTICAL SALINITY SCALE UNESCO 1978 According t...

Page 25: ...for the pH buffers used for calibration are available Automatic the instrument automatically selects the closest buffer to the measured pH value from the edited buffer group Semiautomatic the instrume...

Page 26: ...Press and use or to highlight the 1st Cal Point option Press and use or to highlight the desired option Press to confirm your selection or press to cancel operation Edit Custom Buffers If you want to...

Page 27: ...rs at least one pH buffer has to be removed in order to add another buffer To set the Buffer Group Use or to select the Calibration option Press and use or to highlight the Edit Buffer Group option Pr...

Page 28: ...o highlight the Set Reminder Period option Press and use to select next previous entry to be edit Press and use or to set the desired value then press to save the modified value Press to return to the...

Page 29: ...a pure water using the United States Pharmacopeia standard USP 645 This USP standard consists of three stages one in line and two off line tests as following Stage 1 this is an in line test To perform...

Page 30: ...o select the signal stability criterion for the measured parameter pH mV ISE Fast this criterion will give faster results with less accuracy Medium this criterion will give medium speed results with m...

Page 31: ...probe in the second beaker Tap the probe repeatedly to remove any air bubbles that may be trapped inside the sleeve Enter in calibration mode by pressing Wait to stabilize When the automatic standard...

Page 32: ...replaced At least once a week Before USP measurements After testing aggressive chemicals When calibration reminder is activated Conductivity Cal Expired If the readings are far from the calibration p...

Page 33: ...ption Press to generate a new manual lot A pop up menu will be displayed asking for confirmation Press to confirm or press to escape without saving and return to the Log options 84 Clear Calibration A...

Page 34: ...ess and use or to highlight the Alarm Limits option Press and use to select next previous entry to be edit Press and use or to set the desired value then press to save the modified value Press to retu...

Page 35: ...the isopotential point has been modified recalibration must be performed for the pH channel To set the Isopotential Point Use or toselecttheIsopotentialPointoption Press and set the desired isopotenti...

Page 36: ...mV mV SETUP SETUP SETUP SETUP SETUP 81 TDS TDS TDS TDS TDS SETUP SETUP SETUP SETUP SETUP The TDS Setup menu allows the user to set the parameters related to the TDS measurement Accessing TDS Setup Pr...

Page 37: ...Hold reading mode the ion concentration can be frozen on the LCD after starting the AutoHold mode Known Addition In the Known Addition method a standard with a known concentration of the measured ion...

Page 38: ...emperature Compensation This option allows the user to enable disable the temperature compensation for the measurement of Ion concentration To set the Temperature Compensation Use or to select the Tem...

Page 39: ...p section Electrode Type This option allows the user to select the desired Ion Selective Electrode used for measurements from a list Ammonia Bromide Cadmium Calcium Carbon Dioxide Chloride Chlorine Cu...

Page 40: ...t saving or to return to the editing mode Otherwise the modified option is saved automatically TosettheappropriateIonmolarweight ing molunits use or and then press to save the current value or press t...

Page 41: ...ee pH Setup section Note The Alarm Limits Low and High are set in the selected concentration unit of the measured ion or chemical compound and are displayed in a scientific format value and value expo...

Page 42: ...ificant Digits Accessing this option the number of ISE significant digits can be set with one x two xx or three xxx significant digits To set the ISE Significant Digits Use or to select the ISE Signif...

Page 43: ...nt calibration by selecting five of the available buffers CALIBRATION PROCEDURE Calibration has a choice of 8 memorized buffers pH 1 68 3 00 4 01 6 86 7 01 9 18 10 01 12 45 and up to 5 custom buffers...

Page 44: ...w added calibration point will replace an old one if the difference between them is 0 2 pH If the existing stored calibration is full five calibration points a pop up menu will be displayed on the LCD...

Page 45: ...ck if you have selected the appropriate calibration buffer Wrong buffer temperature this message appears if the buffer temperature is out of the defined buffer temperature range Clean the electrode or...

Page 46: ...coefficient using or to increase decrease the value Press to save the current value or press to cancel operation Calibration Cell Constant The conductivity probe can be calibrated using the conductivi...

Page 47: ...probe approximately 4 cm 1 into the sample to be tested Allow time for the electrode to stabilize The measured pH value will be displayed on the LCD If pressing the AutoHold indicator will start blin...

Page 48: ...1 7 1 5 5 1 7 4 5 1 2 4 5 1 8 3 5 1 4 3 5 1 9 2 5 1 5 2 5 1 1 2 5 1 6 1 5 1 2 1 5 1 8 8 0 5 1 4 0 5 1 0 0 5 1 6 9 4 1 1 9 4 1 7 8 4 1 3 8 4 1 9 7 4 1 5 7 4 1 1 7 4 1 9 7 6 4 1 3 6 4 1 9 5 4 1 5 5 4 1...

Page 49: ...e will be displayed on the LCD If pressing the AutoHold indicator will start blinking on the LCD until the stability criterion is reached The mV value will be frozen on the LCD along with AutoHold ind...

Page 50: ...isting Relative mV or use or to adjust the Relative mV value and then press to save the current Relative mV Press at any time to return to Relative mV Measure mode Before performing a Rel mV calibrati...

Page 51: ...ustment Buffer to the calibration standards CALIBRATION PROCEDURE Up to five point calibration is possible using five memorized standard solutions 0 1 1 10 100 1000 ppm and 5 custom solutions The ISE...

Page 52: ...rate the instrument using Custom Standard entry type Press If the instrument was calibrated before and calibration was not cleared the old calibration can be cleared by pressing After 10 seconds will...

Page 53: ...asurements Otherwise will appear on the LCD When in MTC mode if pressing after enter ing ISE calibration and while a standard solution is selected a pop up menu will be displayed on the LCD in which t...

Page 54: ...s as a result of an erroneous slope condition Press to clear old calibration and restart calibration Difference between standards temperature is too high Press Accept to update the calibration or clea...

Page 55: ...tails Add ISAB to the sample solution Submerge the Ion Selective Electrode tip and the tempera ture probe approximately 4 cm 1 into the sample to be tested Allow time for the electrode to stabilize IS...

Page 56: ...trength The Nernst equation can be rewritten ION SELECTIVE ANALYSIS METHODS Direct Analysis Direct Analysis Direct Analysis Direct Analysis Direct Analysis This method is a simple procedure for measur...

Page 57: ...ective Electrode tip approximately 4 cm 1 into the sample to be tested Press to take the first mV reading When the reading is stable press to store the first mV reading The second step of the method w...

Page 58: ...ncentration will be recalculated Press to start another measurement Note Press at any time to stop the measurement and return to ISE Measure mode ANALYTE SUBTRACTION To measure the concentration of a...

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