Hanna Instruments HI 4101 Instruction Manual Download Page 18

18

XV.  

XV.  

XV.  

XV.  

XV.  Storage and Care of the HI 4101 sensor

Storage and Care of the HI 4101 sensor

Storage and Care of the HI 4101 sensor

Storage and Care of the HI 4101 sensor

Storage and Care of the HI 4101 sensor

The HI 4101 sensor can be stored assembled and ready to
use in HI 4001-45 Conditioning solution overnight or
between measurements. After overnight storage, gently pull
on the cable to compress the spring mechanism thus
permitting electrolyte to exchange from the bulk to the thin
film between the membrane and glass. Calibration is
required after doing this.
For longer term storage (over a week), disassemble the
sensor completely and rinse off the internal pH/reference
assembly, the outer body and the membrane cap. Discard
the white PTFE membrane. (Note: keep black membrane
cap). Cover the glass tip with the protective shipping cap
and store parts securely in the original shipping box.  When
reassembling the sensor follow section IX.

XVI. 

XVI. 

XVI. 

XVI. 

XVI. Conversion T

Conversion T

Conversion T

Conversion T

Conversion Tables

ables

ables

ables

ables

For NH

For NH

For NH

For NH

For NH

33333

Multiply by

Multiply by

Multiply by

Multiply by

Multiply by

Moles/L (M) NH

3

 to ppm NH

3

 (mg/L)

1.70 X 10

4

ppm NH

(mg/L) to M (Moles/L)

5.882 X 10

-5

For N-NH3 (ppm as nitrogen)

For N-NH3 (ppm as nitrogen)

For N-NH3 (ppm as nitrogen)

For N-NH3 (ppm as nitrogen)

For N-NH3 (ppm as nitrogen)

Multiply by

Multiply by

Multiply by

Multiply by

Multiply by

Moles/L (M) NH

3

 to ppm N-NH

3

 (mg/L) 1.40 X 10

4

Summary of Contents for HI 4101

Page 1: ...1 HI 4101 HI 4101 HI 4101 HI 4101 HI 4101 Ammonia Ion Selective Electrode Instruction Manual A M M O N IA HI 4101...

Page 2: ...2...

Page 3: ...monium ions are also measured by conver sion to ammonia gas upon ISA addition II II II II II Specifications Specifications Specifications Specifications Specifications Type NH3 gas sensing electrode w...

Page 4: ...gas in the sample and thin film are equal The change in pH is proportional to the concentra tion of dissolved gas in the sample solution The Nernst expression for an ammonia sensor is expressed in th...

Page 5: ...ethemembrane membranecap outerprobe body with antirotation key and the pH reference assembly which includes the outer electrode cap spring inner cap and pH reference electrode assembly Outer probe bod...

Page 6: ...A HI4001 00 Hanna 0 1 M standard HI4001 01 Hanna 100 ppm N standard HI4001 02 Hanna 1000 ppm N standard HI4001 03 Please Note These calibration standards are ppm as NH3 N See Section XVII for addition...

Page 7: ...atingor wetting thePTFEmembranewill effect the response Inspect sensor before using Re place PTFE membrane if damage is evident Rinse electrode with distilled or deionized water be tweensamplesanddabd...

Page 8: ...ionized water These pH solutions contain chloride ions and pH buffers that are used to verify the inner electrode pH internal is operational See Section XVII for replacement accessories and maintenanc...

Page 9: ...lution carry over Do not rub the glass Take a measurement in the second buffer and record mV Pay attention to minus sign if present Calculate the difference in mV between the two solutions Example of...

Page 10: ...le gently stretching membrane over opening and cap turing opposite membrane corner against threads Smoothexcessmembranematerialaroundthethreads 4 Screw outer membrane cap onto body thus capturing the...

Page 11: ...de spring and elec trode cap down cable and screw cap on outer body until fully engaged Do not invert electrode Do not overtighten 8 Install assembled electrode in gas sensor test vessel or in electro...

Page 12: ...has stabilized This value should be less than the previous noted more negative DeterminethedifferencebetweenthetwomVvalues An acceptable value for this slope is 54 4 mV at ambient temperatures between...

Page 13: ...bound nitrogen such as oil sludge waste or samples which may contain surfactants digest sample first using a total Kjeldahl nitrogen TKN procedure This involves oxidationwithhotsulfuricacidwhich conv...

Page 14: ...in the measurement range of the unknowns with ISA added are measured in mV mode on the meter These standards are plotted on semilog graph paper and their points are connected to form a straight line c...

Page 15: ...ed gas by covering and using promptly 3 FollowsectionVII GeneralGuidelinestooptimizetest set up 4 Duringcalibrationitisbesttostartwithlowerconcen trationsamplesfirst Waitforastablereadingbefore readin...

Page 16: ...erature of measurement should be determined and used if possible This will improve ac curacy Known addition is Method 4500 NH3 E from StandardMethodsfortheExaminationofWaterandWaste water 1 The volume...

Page 17: ...with an electrode 1 mL of ISA is added to the sample and the color change is noted The sample is covered and permitted to mix The mV is then recorded when the sensor has stabilized 2 5 mL VSTANDARD o...

Page 18: ...mpletely and rinse off the internal pH reference assembly the outer body and the membrane cap Discard the white PTFE membrane Note keep black membrane cap Cover the glass tip with the protective shipp...

Page 19: ...ppm N standard 500 mL HI4001 03 Hanna 1000 ppm N standard 500mL HI4001 30 Nitrate test kit Bulk pkg Please Note These calibration standards are ppm as NH3 N For Maintenance For Maintenance For Mainten...

Page 20: ...m date of purchase when used for their intended purpose and maintained according to instructions If they fail to work whenfirstusedcontactyourdealerimmediately Damagedue to accidents misuse misapplica...

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