Hach ISENH4181 User Manual Download Page 9

9. 

 Do steps 

3

through 

8

 to read the

value of the
remaining standard
solutions.

10. 

 Save the

calibration.

Section 6 Sample measurement

The procedure that follows is applicable to meters that can connect to Intellical ISE probes. Refer to
the applicable meter documentation for meter operation and probe-specific settings.

6.1 Sample measurement notes

Read the notes that follow before sample measurements.

• Rinse the probe with deionized water and dry with a lint-free cloth between measurements to

prevent contamination.

• If the stabilization time is long, try a different stir rate and make sure to condition the probe.
• Keep all of the solutions (standard solutions and samples) at the same temperature (± 2 °C

(± 3.6 °F)) for best results.

• If complete traceability is necessary, enter a sample ID and operator ID before measurement.

Refer to the meter manual for instructions.

• Stir the standards and samples at a slow and constant rate to prevent the formation of a vortex.
• The meter automatically saves the measurement data when the user manually reads each data

point and when the meter is set to read at regular intervals. The user must manually save each
data point when the meter is set to read continuously.

• Air bubbles below the sensor can cause a slow response or error in the measurement. Make sure

to remove air bubbles before and during measurements.

6.2 Sample measurement procedure

1. 

 Pour 25 mL of

fresh sample into a
50

mL beaker.

2. 

 Add one

Ammonium Ionic
Strength Adjustor
(ISA) Solution Pillow.

3. 

 Add a stir bar.

Put the beaker on an
electromagnetic
stirrer. Stir at a
moderate rate.

4. 

 Rinse the probe

with deionized water.
Dry the probe with a
lint-free cloth.

English

   

7

Summary of Contents for ISENH4181

Page 1: ...DOC022 53 80029 ISENH4181 05 2021 Edition 5 User Manual...

Page 2: ......

Page 3: ...n 5 5 1 Calibration notes 5 5 2 Calibration procedure 6 Section 6 Sample measurement 7 6 1 Sample measurement notes 7 6 2 Sample measurement procedure 7 6 3 Low level measurements 8 6 4 Interferences...

Page 4: ...Table of Contents 2...

Page 5: ...2 Specifications Specifications are subject to change without notice Specifications Details Probe type Digital combination probe with a non refillable reference junction and a built in temperature sen...

Page 6: ...r Certifications CE FCC ISED Section 3 Safety information 3 1 Intended use The Intellical probes are intended for use by individuals who measure water quality parameters in the laboratory The Intellic...

Page 7: ...probe before use To condition the probe soak the probe in approximately 25 mL of the lowest concentration standard solution used for calibration for 30 to 60 minutes Do not add the ISA to the standard...

Page 8: ...e 1 Go to the calibrate menu Select the probe if applicable The display shows the standard solutions to use for calibration 2 Add 25 mL of each standard solution to different beakers 3 Add one Ammoniu...

Page 9: ...lete traceability is necessary enter a sample ID and operator ID before measurement Refer to the meter manual for instructions Stir the standards and samples at a slow and constant rate to prevent the...

Page 10: ...ow apply The sample does not contain interferences The sample pH is within the range given in the specifications Omission of the ISA is accepted by the regulatory reporting agency if the measurement i...

Page 11: ...o the acceptance criteria 7 1 Verification procedure 1 Go to the verification menu The display shows the standard solution to use for verification Note Menu name for HQd meters Run check standard 2 Po...

Page 12: ...rd solution 8 2 Storage Keep the sensor protection cap on the probe during storage to prevent damage to the sensing element Note Make sure to condition the probe after long term storage Refer to Prepa...

Page 13: ...contamination Use the specified standard solution of good quality Too much time passed after the ISA was added Measure the sample or standard solutions immediately after the ISA is added 9 1 Slope ch...

Page 14: ...tandard addition A percent recovery of 100 5 is an indication that the sample measurements are accurate Percent recovery CM CE x 100 Where CM measured concentration of the sample after the addition of...

Page 15: ...scription Quantity Item no Beaker polypropylene 50 mL low form 1 108041 Disposable wipes 11 x 22 cm 280 pkg 2097000 Wash bottle polyethylene 500 mL 1 62011 Probe stand for standard Intellical probes 1...

Page 16: ...14 English...

Page 17: ......

Page 18: ...932 orders hach com www hach com HACH LANGE GMBH Willst tterstra e 11 D 40549 D sseldorf Germany Tel 49 0 2 11 52 88 320 Fax 49 0 2 11 52 88 210 info de hach com www de hach com HACH LANGE S rl 6 rout...

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