Hach Intellical PHC805 User Manual Download Page 16

Section 9 Troubleshooting

Keep the probe clean and in the recommended storage solution when not in use for the best
accuracy, stabilization time and life of the probe.

Problem

Possible cause

Solution

Decreased probe performance
causes slow stabilization and
prevents accurate calibrations or
measurements.

The glass sensor is dirty.

Clean and condition the probe.
Refer to 

Clean the probe

on page 11.

The reference junction is
clogged.

Clean and condition the probe.
Refer to 

Clean the probe

on page 11.

The filling solution has
contamination.

Replace the filling solution.
Refer to 

Replace the filling

solution

 on page 12.

The probe is not conditioned
to the sample sufficiently.

Condition the probe. Refer to 

Preparation for use

 on page 5.

The glass sensor has become
dry.

Soak the probe tip in buffer
solutions. Refer to 

Soak

procedure for dry probes

on page 12.

The calibration slope of the
probe has changed.

Increase the accepted slope
limit settings if possible, or
contact technical support.

Sample properties cause slow
stabilization or inaccurate
measurements.

The sample absorbs carbon
dioxide (CO

2

) from the air,

which causes the pH value to
slowly decrease in low ionic
strength (LIS) or high purity
samples.

Use the LIS chamber for
LIS/high purity samples to
prevent CO

2

 absorption.

The sample temperature is
low, or there is a large
temperature difference
between samples.

Increase the sample
temperature or adjust the
temperature of different
samples to be the same (within
2 °C (3.6 °F)).

Procedure problem causes slow
stabilization and prevents
accurate calibrations or
measurements.

The filling hole is closed.

Open the filling hole during
use.

Air bubbles are around or
below the probe tip.

Carefully tap or shake the
probe to remove air bubbles.

The electrical connection
through the reference junction
is not sufficient.

Shake the probe in the solution
from side to side to refresh the
reference junction.

The stir speed is too slow or
too fast.

Try a different stir speed.

An incorrect buffer solution
was used or the buffer
solution has contamination.

Use the specified buffer
solutions of good quality.

The protective tape was not
removed from the filling hole.

Remove the tape from the
filling hole. Refer to 

Preparation for use

 on page 5.

14

   

English

Summary of Contents for Intellical PHC805

Page 1: ...DOC022 53 80436 PHC805 05 2021 Edition 2 User Manual...

Page 2: ......

Page 3: ...7 5 2 Calibration procedure 7 Section 6 Sample measurement 8 6 1 Sample requirements 8 6 2 Sample measurement notes 9 6 3 Sample measurement procedure 9 Section 7 Verify the calibration 9 7 1 Verifica...

Page 4: ...Table of Contents 2...

Page 5: ...mples of low ionic strength For best accuracy do not use the probe to measure the pH of very alkaline samples Figure 1 Probe overview 1 Probe soaker bottle with storage solution 5 Probe soaker bottle...

Page 6: ...acturing defects but not improper use or wear Certifications CE FCC ISED Section 3 Safety information 3 1 Intended use The Intellical probes are intended for use by individuals who measure water quali...

Page 7: ...ion for use N O T I C E Make sure to remove the protective tape from the filling hole of new probes A probe with a blocked filling hole will not operate correctly New probes are filled with electrolyt...

Page 8: ...Figure 2 Remove the protective tape Figure 3 Probe position during use 1 Open filling hole 3 Level of calibration solution or sample 2 Level of electrolyte filling solution 6 English...

Page 9: ...more than one probe is connected to the meter if applicable Calibrate the probes and verify the calibration regularly for best results Use the meter to set calibration reminders The calibration data...

Page 10: ...e meter documentation for meter operation and probe specific settings 6 1 Sample requirements N O T I C E Make sure that the sample type is compatible with the probe or probe damage can occur Samples...

Page 11: ...mple 2 Open the filling hole 3 Rinse the probe with deionized water Dry the probe with a lint free cloth 4 Put the probe in the sample with the sensor and reference junction fully in the sample Do not...

Page 12: ...ionized water Dry the probe with a lint free cloth 5 Put the probe in the pH buffer solution with the sensor and reference junction fully in the solution Do not put the probe on the bottom or sides of...

Page 13: ...ater Dry the probe body with a lint free cloth 4 Soak the probe in pH 4 buffer for 20 minutes 5 Rinse the probe with deionized water Dry the probe body with a lint free cloth Table 1 Cleaning solution...

Page 14: ...eplace the filling solution 1 Tilt the probe and open the filling hole 2 Use a plastic transfer pipet to remove the contaminated solution from the filling hole Discard the solution 3 Rinse the inner p...

Page 15: ...s of low ionic strength For short term storage the probe can stay in the sample for a maximum of 2 hours if the sample pH is not high Close the filling hole and put the soaker bottle that contains the...

Page 16: ...ilization or inaccurate measurements The sample absorbs carbon dioxide CO2 from the air which causes the pH value to slowly decrease in low ionic strength LIS or high purity samples Use the LIS chambe...

Page 17: ...ckets 20 mL each 20 pkg 2770020 pH 7 00 buffer solution Singlet one use packets 20 mL each 20 pkg 2770120 pH 10 01 buffer solution Singlet one use packets 20 mL each 20 pkg 2770220 pH 4 01 and pH 7 00...

Page 18: ...escription Quantity Item no Beaker 30 mL plastic colorless 80 pkg SM5010 Beaker 30 mL plastic red 80 pkg SM5011 Beaker 30 mL plastic yellow 80 pkg SM5012 Beaker 30 mL plastic blue 80 pkg SM5013 Beaker...

Page 19: ......

Page 20: ...669 2932 orders hach com www hach com HACH LANGE GMBH Willst tterstra e 11 D 40549 D sseldorf Germany Tel 49 0 2 11 52 88 320 Fax 49 0 2 11 52 88 210 info de hach com www de hach com HACH LANGE S rl 6...

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