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StamoLys CA 71 SI

Trouble-shooting

Hauser

39

9.3

Process errors without messages

Error

Possible cause

Tests and / or corrective measures

Measured values 
always the same

Reagents 
contaminated or aged

Simple check: Add about 20 ml of standard solution with about 1 ml of reagent in a vessel. If it 
does not change colour after max. 10 min, replace the reagents .

No sample, no 
reagents

Make sure sample and reagents are supplied, check level monitor and clean if necessary

System blocked

Flush with 12.5% bleaching lye (monthly maintenance)

Measured values 
inaccurate

Incorrect 
concentration of 
standard 

Check the concentration in the laboratory. Adjust the standard accordingly 
("PARAMETER ENTRY", "Calibration solution") or replace the standard.

Reagents 
contaminated or aged

Simple check: Add about 20 ml of standard solution with about 1 ml of reagent in a vessel. If it 
does not change colour after max. 10 min, replace the reagents.

Reagent blank value 
too high

After replacing the reagents, carry out an offset calibration and then a calibration 
(CONFIGURATION, "Offset calibration")

Wrong dimension

Check the setting in the CONFIGURATION menu, "Measuring unit".

Wrong optical cell

Check the setting in the CONFIGURATION menu, "Photometer"

Sample suction time 
too short

Increase the suction time (CONFIGURATION, "Delay to sample")

Matrix effects
(substances that 
interfere with the 
photometric methods)

Detect interfering substances (see Technical Information, "Measuring principle"), 
possibly use sample conditioning

Standard is dosed to 
the sample

Check the valves and valve settings. Replace valve hoses if necessary.

Filter life too long

Take counter sample at analyzer inlet and check the concentration in the laboratory. If the 
analyzer measured values have no deviations, clean ultrafiltration modules or backflush filters 
more frequently.

System block or 
contaminated

Flush with 12.5% bleaching lye (monthly maintenance)

Dosing

Replace pump hoses.

Optical cell dirty

Flush with 12.5% bleaching lye first and then with 5% hydrochloric acid

Counter sample in the 
laboratory delivers 
deviating measured 
values

Sample ageing

Shorten time between sampling and analysis.

Measured value 
transfer errored

Wrong size of analog 
output

Check the setting (CONFIGURATION, "Analog output 1"  " 2").

Incorrect measuring 
range

Adjust measuring range (PARAMETER ENTRY, "Measuring range")

Background noise

Check line for interference from strong sources of induction.

Analyzer will not 
switch on

No power

Check the electrical connection and ensure power supply.

Fuse

Replace fuse F1 (time-lag 0.5 A)

Analyzer is running 
but display reading is 
garbled or off

Initialisation failed

Switch the analyzer off and after approx. 30 seconds back on.

Pumps fail to run

Leak

See "Spillage error" error message

Leak sensor 
bypassed

Interrupt contact between two leak sensors (pins 67-66)

Fuse

Check all fuses and replace if necessary.

Pump defective

E+H-Service

Measurement does 
not start

Leak on photometer

E+H-Service

Summary of Contents for Stamolys CA71CL

Page 1: ...Quality made by Endress Hauser ISO 9001 BA 364C 07 en 07 03 51512332 Valid of Software version 5 2 StamoLys CA 71 SI Silicate Analyzer Operating Instructions...

Page 2: ......

Page 3: ...eration 20 5 4 Calibration 28 6 Commissioning 30 6 1 Function check 30 6 2 Switch on 30 7 Maintenance 32 7 1 Maintenance schedule 32 7 2 Replacing reagents 33 7 3 Replacing pump hoses 34 7 4 Replacing...

Page 4: ...cular the analyzer is intended for steam and condensate analysis reversed osmosis demineralisers Any other use than the one described here compromises the safety of persons and the entire measuring sy...

Page 5: ...n it cleaned to the Endress Hauser sales centre responsible Please use the original packaging if possible Please enclose the completed Dangerous Goods sheet copy the second last page of these Operatin...

Page 6: ...Sample transfer from two measuring points two channel version Power supply 0 Power supply 230 V AC 50 Hz 1 Power supply 115 V AC 60 Hz Collecting vessel for up to 3 analyzers A Without collecting ves...

Page 7: ...output 4 edge covers a quality certificate Operating Instructions english Note Reagents please order separately with analyzer version CA 71 XX XXXXXX1 With versions CA 71 XX XXXXXX2 and CA 71 XX XXXXX...

Page 8: ...eck that the scope of delivery is complete and agrees with your order and the shipping documents The packaging material used to store or to transport the product must provide shock protection and humi...

Page 9: ...11 08 00 xx 001 eps Fig 4 Collecting vessel at analyzer optionally 1 Ventilation 2 Sample inlet from sampling 3 Collecting vessel 4 Electrical connections 5 Analyzer sample inlet C07 CA71xxx 06 08 02...

Page 10: ...cation mount the right adjusting pin or no adjusting pin Fig 6 and Fig 7 position 2 2 Pull the marked pipe position 3 downwards due to your application 1 2 or 3 analyzers E H Collecting vessel at CA 7...

Page 11: ...valve hoses V1 Valve 1 V2 Valve 2 1 To the pump 2 Y piece connecting hose to valve 1 behind it 3 Hose valve 2 front standard 4 Hose valve 2 back cleaning agent 5 Hose valve 1 front sample 6 Secure th...

Page 12: ...Sample Reagent 1 Reagent 2 Reagent 3 Standard solution Cleaner P SI1 SI2 SI3 S R Permeate can contain air bubbles CAT 430 or is free of bubbles customer supplied ultrafiltration Distance between the a...

Page 13: ...s short as possible sampling line between T piece and the second analyzer Fig 11 item 5 shorter than 1 5 m Cross section of sampling line ID 3 2 4 mm one sample receiver each without level measurement...

Page 14: ...onnel must have read and understood the instructions in this manual and must adhere to them Ensure that there is no voltage at the power cable before beginning the connection work 4 1 1 Quick wiring g...

Page 15: ...not ready To start measurement the voltage must stay at 0 V for at least 5 seconds Function Designation Terminal one channel Terminal two channels Mains L 3 3 N 2 2 PE 1 1 Alarm value 1 channel 1 COM...

Page 16: ...l version place the cable cores of all cables data cables to analog output 1 and to analog output 2 through the interference suppressor 4 2 2 One channel version C07 CA71xxx 03 08 00 xx 001 eps Fig 13...

Page 17: ...ult Retrieves error message using operation menu Channel or measurement end1 1 Alternative selection Displays active channel Displays Measurement finished 5 s Analog output l 1 channel 1 0 or 4 mA mea...

Page 18: ...g commands can be sent from the PC in order to read out data D Data memory Measured values C Data memory Calibration factors S Setup parameter entry configuration F Frequency current Connection Termin...

Page 19: ...e check the terminal assignment for analogue output 1 or 2 Device status and specifications Note Is the analyzer or cable externally undamaged Visual inspection Electrical connection Note Does the sup...

Page 20: ...rial interface RS 232 4 Operating keys and control LEDs 5 3 Local operation The operating keys and the integrated indicator LEDs have the following functions RS 232 ENDRESS HAUSER STAMOLYS CA 71 M CE...

Page 21: ...as not yet expired Note Measuring flashes when the analyzer is ready for the next measurement but has not yet received the enable signal from the sample collector or the sample conditioning unit Selec...

Page 22: ...oncentration of the standard see PARAMETER ENTRY calibration solution The deviation results from factors such as reagent ageing ageing of constructive components etc The calibration factor compensates...

Page 23: ...only Setting for whether contact for alarm value 1 channel 2 works as NO current or NC current contact Alarm value AV 2 2 Two channel version only Setting for whether contact for alarm value 2 channel...

Page 24: ...teresis 2 of alarm value Alarm value AV 2 1 SI A 1 200 g l 200 g l SI B 100 5000 g l 5000 g l Concentration threshold value limit relay 2 channel 1 differential hysteresis 2 of alarm value Alarm value...

Page 25: ...n interval of 48 72 h Calibration solution SI A 1 200 g l 500 g l SI B 100 5000 g l 500 g l Concentration of the calibration standard Select a standard whose concentration is in the upper third of the...

Page 26: ...y to enter the menu Option Display Info Pumps and valves Virtual switching board Various valve and pump combinations can be selected The setting options are Valve 1 P sample or S standard Pump 1 and p...

Page 27: ...n ASCII format via the serial interface For this the receiving end PC must be configured like this 9600 N 8 1 To send data the receiving end PC must send the ASCII character 81 Shift D Clear data This...

Page 28: ...sub menu 5 4 2 Interferences Measuring range Concentration mg l Frequency Hz Silicate lower measuring range SI A 1 200 g l 0 000 0 020 0 040 0 060 0 080 0 100 0 120 0 140 0 160 0 200 0 251 515 831 10...

Page 29: ...e which lies in the past 6 Press F to accept the value and then press Htwice to return to the main menu 7 Press Fagain This takes you back to measuring mode The calibration is now carried out automati...

Page 30: ...nfigured and calibrated the measuring cycle starts automatically Entering parameters is no longer necessary To perform initial start up or to readjust the device parameters proceed as follows 1 Plug i...

Page 31: ...R or S with V and then switch the P1 sample pump on Leave the pump running until you can tell that there is cleaning agent at the T connector Switch P1 back off 7 Now switch the valves to passage for...

Page 32: ...ekly Check and note calibration factor for service purposes Move valve hoses into their position and spray with silicone extends the service life CONFIGURATION every 2 weeks Check concentration of the...

Page 33: ...ee Trouble shooting instructions the reagents are too old the reagents have been spoilt by incorrect storage conditions or environmental influences Reagents check a Check the standard solution concent...

Page 34: ...m the connecting nipples on the pump s 3 Remove the reagent hoses from the reagent canisters in order to prevent contamination of the reagents 4 Loosen the hose cassette Now you can remove the hoses 5...

Page 35: ...left of the mixer 4 Remove the old mixer from the clip and insert the new one 5 Connect the new mixer to the hoses again 6 Attach the photometer housing and screw it down 7 After installation refill...

Page 36: ...el SS 1 4301 AISI 304 with a lint free cloth and Glittol RG 10 51 GFR housing with a damp cloth or with tenside based alkaline cleaning agent 7 8 Placing out of service You must place the analyzer out...

Page 37: ...O2 Si order no CAY642 V10C10AAE Note Please note the disposal instructions in the safety data sheets of the reagents 8 3 Hose cleaner Cleaning agent alkaline 100 ml order no CAY746 V01AAE Cleaning age...

Page 38: ...ngly PARAMETER ENTRY Calibration solution or replace the standard Reagents contaminated or aged Simple check Add about 20 ml of standard solution with about 1 ml of reagent in a beaker If it does not...

Page 39: ...methods Detect interfering substances see Technical Information Measuring principle possibly use sample conditioning Standard is dosed to the sample Check the valves and valve settings Replace valve...

Page 40: ...date Interval not expired or 0 h Change parameters Leak on Photometer Device or discharge blocked Remove blockage E H Service Blockage deposits in device Water hardness Lime deposits can by flushing w...

Page 41: ...w with sample collector 51504114 122 Hose made of C Flex 6 4 mm 51504115 123 Hose made of C Flex 1 5 mm 51512535 130 Hose adapter 1 6 mm x 1 6 mm 51506495 131 Hose adapter T 1 6 mm x 1 6 mm x 1 6 mm 5...

Page 42: ...arm Contacts 2 limit contacts per channel 1 system alarm contact optionally end of measurement with two channel version display of channel no available Load max 500 Serial interface RS 232 C Load capa...

Page 43: ...e time selectable from 20 to 300 s standard 80 s Rinse again time 30 s Filling time 15 s Maintenance interval 6 month typical Servicing requirement 15 minutes per week typical Ambient temperature 5 40...

Page 44: ...sample Deutsch English Fran ais Italiano Nederlands Suomi Magyar Polski Error messages Pumps and valves Frequency Mixture Measured values Output Clear data Measuring range start Alarm value 1 Calibra...

Page 45: ...ys CA 71 SI Appendix Endress Hauser 45 Analog output Alarm value 1 Alarm value 2 Error contact act Date time Frequency offset Standard solution Flushing interval Flushing time 1st Flushing Calibrate o...

Page 46: ...s Suomi Magyar Polski Error messages Pumps and valves Frequency Mixture Measured values Output Clear data Measuring range start1 Calibration Measuring Flushing Waiting PARAMETER ENTRY AUTO MEASURING L...

Page 47: ...m value 1 2 Calibration solution 1st Flushing act Date time Frequency offset Calibrate offset Error contact Alarm value 2 2 Alarm value 2 1 Analog output 2 Flushing interval Flushing time n Channel 1...

Page 48: ...ctive 1 l SI1 SI2 SI3 each CAY641 V10AAE Cleaning agent 1 l CAY642 V10C05AAE Standard solution 0 5 mg l SiO2 Si CAY642 V10C10AAE Standard solution 1 0 mg l SiO2 Si Chemicals for Ultra filtration Quant...

Page 49: ...se ID 6 4 mm 51504115 123 1 m C Flex hose ID 1 5 mm 51512535 130 10 Hose adapter 1 6 mm x 1 6 mm 51506495 131 10 Hose adapter T 1 6 mm x 1 6 mm x 1 6 mm 51506490 132 10 Hose adapter 3 2 mm x 3 2 mm 51...

Page 50: ...output 0 20 mA 4 20 mA AV 1 normally closed normally open AV 2 normally closed normally open Fault signal normally closed normally open Frequency offset Hz Ground line demineralised water without reag...

Page 51: ...gain Filling time Reaction time U min K floating mean N Points C1 mg l g l F 1 Hz C2 mg l g l F 2 Hz C3 mg l g l F 3 Hz C4 mg l g l F 4 Hz C5 mg l g l F 5 Hz C6 mg l g l F 6 Hz C7 mg l g l F 7 Hz C8 m...

Page 52: ...ith pressurised water disposable syringe Remove hose holder unit from the pump Done KW 1 KW 3 KW 5 KW 7 KW 9 KW 11 KW 13 KW 15 KW 17 KW 19 KW 21 KW 23 Date Done KW 25 KW 27 KW 29 KW 31 KW 33 KW 35 KW...

Page 53: ...y symbols 5 Incoming acceptance 8 Input 42 Installation 4 8 11 Examples 12 Interference suppressor 16 Interferences 28 L LANGUAGE 26 M Main menu 21 Maintenance 32 Schedule 32 Mechanical construction 4...

Page 54: ...eening 16 Serial interface 18 SERVICE 26 Signal connection 16 Spare parts 40 Standard solution 37 Storage 8 Switching contacts 17 Switch on 30 Symbols 5 T Technical data 42 43 Terminal assignment 15 T...

Page 55: ...health o biologically hazardous o inflammable o safe Please mark the appropriate warning hints 5HDVRQ IRU UHWXUQ BBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBBB BBBBBBBBBB...

Page 56: ...ta D C Colsein Ltda Tel 01 2 36 76 59 Fax 01 6 10 78 68 Costa Rica San Jose Euro Tec S A Tel 2 20 28 08 Fax 2 96 15 42 Ecuador Quito Insetec Cia Ltda Tel 02 2 26 91 48 Fax 02 2 46 18 33 El Salvador Sa...

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