Ecom ECD2600 User Manual Download Page 1

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ECD2800

ECD2600

ECOM spol. s r.o., Trebonicka 239, 252 19 Chrastany u Prahy, Czech Republic

tel: +420 221 511 310, fax: +420 242 498 212, [email protected], http://www.ecomsro.com/

IČO: 411

192, DIČ: CZ411

92 192

User’s Guide

ECD2800

ECD2600

UV-VIS

DETECTOR

Summary of Contents for ECD2600

Page 1: ...M spol s r o Trebonicka 239 252 19 Chrastany u Prahy Czech Republic tel 420 221 511 310 fax 420 242 498 212 info ecomsro cz http www ecomsro com IČO 411 92 192 DIČ CZ411 92 192 User s Guide ECD2800 ECD2600 UV VIS DETECTOR ...

Page 2: ...Formánek Second issue 02 11 09 2017 Kateřina Kněžourková Jaroslav Formánek Third issue 03 16 01 2018 Kateřina Kněžourková Jaroslav Formánek Update chapter 15 16 17 03 01 06 2018 Michaela Čamborová Jaroslav Formánek New photo on first page 03 6 11 2019 Dominika Pavlová Jaroslav Formánek Address change in chapter 13 19 and in the footer of the first page 04 8 03 2021 Dominika Pavlová Jaroslav Formán...

Page 3: ...ion Cables 12 4 4 Start of the Unit 12 4 5 Basic Control by Keyboard 13 4 6 Description of Symbols on the Screen 14 5 CONTROL FROM PC 14 6 WORKING WITH MENU 14 6 1 Parameters 15 6 1 1 Wavelength 15 6 1 2 Time Constant 15 6 1 3 Sample Rate 16 6 1 4 Thresholds 16 6 2 Preferences 17 6 2 1 Lamp 17 6 2 2 Cell Temp 17 6 2 3 Display 17 6 2 4 Sound 17 6 2 5 Cooling 18 6 2 6 Opti Filter 19 6 2 7 Leakage 19...

Page 4: ... 31 8 RS232 32 9 REPLACEMENT OF LINE FUSE 33 10 TROUBLESHOOTING 33 11 MAINTENANCE 34 11 1 Cleaning and Decontamination 34 11 2 Control of Tubing and Cell Connection 34 11 3 Lamp Control 34 11 4 Operational Qualification 34 12 SPARE PARTS 35 13 WARRANTY AND POST WARRANTY REPAIRS 36 14 CELLS 36 14 1 Order of Cell Components 37 14 2 Control of Cell Purity and Absorbing Mobile Phase 37 14 3 Replacemen...

Page 5: ...ECD2800 ECD2600 5 47 17 APPENDIX 2 ECD2600 EX ECD2800 EX WITH OPTICAL CONNECTORS 43 18 APPENDIX 3 ES DECLARATION OF CONFORMITY 46 ...

Page 6: ...ed Fersions ECD2800 UV VIS Detector Cat ADA0000X ECD2600 UV VIS Detector Cat ADB0000X ECD2800 CE UV VIS Detector Cat ADACE00X ECD2600 CE UV VIS Detector Cat ADBCE00X ECD2800 EX UV VIS Detector Cat ADAEX00X ECD2600 EX UV VIS Detector Cat ADBEX00X ECD2600 is not equipped with tungsten lamp as a secondary light source 1 3 Accessories BASIC ACCESSORIES P N Qty Picture Description 23984000 1 Tube fuse ...

Page 7: ...et ECD2600 2800 00000121 1 PEEK One Piece Handtight Nut 1 16 10 32 ADA40000 1 Test cell TC01 18329000 1 Screwdriver Torx T10 99040300 1 Open End Wrench 7 5 5 mm 00016000 1 Door 2000 DOC00001 1 User s guide DOC00002 1 Production protocol Spare parts and selectable accessories see 12 Spare parts Cell specified in purchase order is inserted in the detector ...

Page 8: ...ver look in the cell area Always put in at least test cell Exchange of deuterium lamp must be carried out with disconnected power cord Caution Never dismount unit cover There is nothing needing customer service or maintenance 2 1 Safety Symbols on Unit UV light is dangerous for your eyes If the flow cell is installed in unit then UV light is perfectly shielded In case of any manipulation with flow...

Page 9: ...es 9 Display 10 Status LED lights LAMP green indicates light sources deuterium lamp and tungsten lamp It blinks during lamp turning on off and lights when a lamp is turned on RMT yellow indicates status of unit remote control It lights when the unit is communicating through interface ETHERNET or RS232 ERR red indicates error status of the unit It lights if an error is indicated and blinks if a fat...

Page 10: ... item confirm the new set value of the parameter invoking the QUICK DIAGNOSTICS screen ESC Return one step without saving changes Directional key The value of the setting parameters are increased decreased with the up down arrows and the wavelength value is increased decreased directly on the main screen REAR VIEW No Description 1 Combined power socket with main switch and main fuse 2 Connector Et...

Page 11: ...cal parameters operating environment conditions 4 1 Cell Connection Unscrew black dummy screws Connect the inlet of the cell below marked as IN to the column using capillary and PEEK screw Connect hydrodynamic resistor to the cell outlet OUT above to restrain bubbles forming in the cell Check the tightness of cell during mobile phase flow Caution Never look inside opened cell compartment if the la...

Page 12: ...ed otherwise the hinges may get damaged 4 3 Connection to Power Supply and Connection of Communication Cables Plug the power supply cord into the instrument socket on the rear panel Connect PC via Ethernet or using RS232 If you are connecting whole system connect in the same manner also other units 4 4 Start of the Unit Use a switch on the rear panel of the detector for connecting to mains voltage...

Page 13: ...LAMP PREEHEATING This mode is followed by calibration of wavelengths in mode OPTICAL CALIBRATION using maximum of zero order and spectral line of hydrogen at 656 and 486 nanometers Status of this process is signalized on the screen After successful calibration the main screen displays absorbance measurement MEASURE ABSORBACE ABS Now you can set wavelength by pressing key WL Keys with arrows left a...

Page 14: ...ter Symbol of successfully executed wavelength calibration empty box means that calibration has not been performed Unsuccessful wavelength calibration initial calibration constants are used Unsuccessful Autozero process Leakage sensor is activated Values marked with this symbol may be changed in menu 5 CONTROL FROM PC During unit control from PC communication proceeds through serial line RS232 or ...

Page 15: ...enu Preferences Signal Autozero After WL Change 6 1 2 Time Constant Time constant represents level of signal filtering and is counted for level 63 5 Preset value is used for both digital and analogue output Slower longer time constant improves overall noise of the detector output at the price of decreasing response speed Low values decrease response speed response delay time lag and change the sha...

Page 16: ...default 2 1 2 20 1 0 6 50 0 4 0 2 100 0 2 0 1 for 20 points per peak coefficient 1 7 was used for conversion of width and half width Example narrowest expected peak half width in analysis is 11 s and therefore minimal recommended sampling rate is 2 sps samples per second For standard chromatographic analysis is usually suitable default value of sampling rate 10 sps samples per second But it is nec...

Page 17: ...ped using key ESC 6 2 1 3 Auto Turn On Mode The unit can be set in a mode that immediately after unit start the light sources are automatically turned on In mode OFF the lamps are not turned on after unit start in mode ON the lamps are started automatically Default value is OFF 6 2 2 Cell Temp This mode is not used so far 6 2 3 Display 6 2 3 1 Brightness The display brightness can be set in eight ...

Page 18: ...nt Lower rotation speed of fans decreases the noise sound level in laboratory but increases working temperature of illuminator The lower the illuminator temperature is the better is the stability and working parameters of the unit Recommended range of working temperature is 30 50 C Diagnostics of cooling status is done in Menu Diagnostic Cooling where are displayed actual measured values of coolin...

Page 19: ...ngths in range of 361 580 nm Yellow filter YELLOW is used for wavelengths over 581 nm At this setting is not inserted any filter for test scans Recommended and default setting NONE None filter is inserted All light goes through WHITE White filter is inserted It absorbs wavelengths under 300 nm YELLOW Yellow filter is inserted It absorbs wavelengths under 480 nm Standardly is set automatic mode Oth...

Page 20: ...one on spectral line 486 nm and if it is not correct detector displays a warning At the end of calibration is performed autozero and eventual deuterium lamp turnoff If the use of tungsten light is set in detector menu Menu Preferences Lamps Lamps use than even in spite of that deuterium lamp is turned on during optical unit calibration and turned off afterwards 6 4 IO Config 6 4 1 Ethernet In menu...

Page 21: ...nother network It is necessary to set up on the unit and also on PC using suitable connecting parameters e g ECD2000 IP 192 168 91 20 MASK 255 255 255 0 and PC IP 192 168 91 1 MASK 255 255 255 0 Caution When using static IP address in corporate network always contact network administrator to avoid network collisions Default setting is automatic parameters setting using DHCP which enables easier pr...

Page 22: ...atible with TTL HC HCT Overvoltage category up to 24 V Opened at level H Active at level L 6 DIN1 DIGITAL INPUT 1 Digital input 1 Compatible with TTL HC HCT Overvoltage category up to 24 V Opened at level H Active at level L 7 ACOB DIGITAL OUTPUT SWITCH Semiconductor switch contact A and B Operating voltage max 60 Vdc 42 Vac Operating current max 240 mA Switch impedance ON max 2 5 ohm Residual cur...

Page 23: ... it has the same function as Digital Input I but it may be used by controlling SW 6 4 3 4 Output Switch DIGITAL OUTPUT SWITCH may be used as follows threshold values A and B can be set in Menu Parameters Thresholds SETTING OF ACTIONS ON DIGITAL OUTPUT Setting Description OFF None action is executed Output is disconnected Default value REMOTE RMT Switch over of the unit to remote control mode conne...

Page 24: ...ns closed input low level Regarding digital output is displayed OFF for open switch and ON for closed switch 6 4 4 Analog Output Analogue output of detector is placed on rear panel and labeled as ANALOG OUTPUT For connecting equipment to analogue output is intended cable from the accessories equipped with 3 pin terminal block ANALOGUE OUTPUT SPECIFICATION Pin Abbr Description On cable 1 AGND Analo...

Page 25: ... and TIME total operating time 6 5 2 Boards Here can be selected board we need information about 6 5 2 1 Main Board BN board name HW board version FW firmware version UN board identification number 6 5 2 2 Display Board BN board name HW board version FW firmware version UN board identification number 6 5 2 3 Power Board BN board name HW board version FW firmware version 6 5 2 4 XPORT Module Ethern...

Page 26: ...ors If a serious problem occurs display shows symbol E with a number of errors in brackets Meaning of these errors is described in this menu which you can enter fast by pressing key ENTER 6 6 2 Warnings If a problem occurs which does not obstruct further operation display shows symbol W with a number which means number of warnings Meaning of these warmings is described in this menu which you can e...

Page 27: ... A VBL W voltage W OFF 0 00 V W voltage W ON 11 00 V 10 50 V 11 80 V IBL W current W OFF 0 000 A W current W ON 0 812 A 0 780 A 0 840 A VFA SMALL FAN voltage both lamps OFF 0 00 V SMALL FAN voltage any lamp ON 18 80 V 18 00 V 19 60 V IFA SMALL FAN current both lamps OFF 0 000 A SMALL FAN current any lamp ON 0 025 A 0 020 A 0 030 A 6 6 4 Cooling Shows temperature of illuminator TEMP rotation speed ...

Page 28: ...h grating MOTOR W and filters MOTOR F At the same time is performed a test of their optical position sensors grating OPTOSWITCH W a filters OPTOSWITCH W serve for finding default position Functionality correctness of individual elements is marked as OK In case of an error message please contact service engineer and describe test results 6 7 Service Service menu is available in two levels which are...

Page 29: ...ecause fingerprints will irretrievably damage the lamp when it is turned on afterwards The position of lamp is exactly determined in the unit no further adjusting is necessary After lamp exchange are the steps for assembly the same as for dismantling only in reverse order Turn on the unit and ignite the lamp if no error occurs turn the lamp off and follow with calibration of new lamp according to ...

Page 30: ... intensity on the sensors or for cell purity diagnostics and is displayed on the absorbance measuring screen For example on wavelength 254 nm will be displayed R52 S53 If S value is significantly lower it denotes impurities in the cell or absorbing mobile phase GRAPH OF LIGHT INTENSITY WITH NEW LAMP 0 20 40 60 80 100 120 190 290 390 490 590 690 790 Wavelength nm Intensity D2 REF D2 SAM D2 W REF D2...

Page 31: ...at first exchange both lamps and then perform calibration process as described in previous chapter If the tungsten lamp is exchanged separately it is only necessary to set operating hours to zero no calibration is needed After entering Menu Service Parts replacement Tungsten Lamp W and confirming new lamp operating hours are set to zero Data about old lamp are archived in the unit memory 6 7 1 3 C...

Page 32: ...ed by pressing key LAMP Wavelength setting SET WAVELENGTH SWL Mode of wavelength setting In this menu are not available any settings and commands and it is not possible to interrupt it Automatic zeroing AUTOZERO AZR In this mode the detector is preparing analogue circuits of the unit for absorbance measuring and it zeroes output signal None settings and commands are available and it is not possibl...

Page 33: ...er unit switch on none LED diode lights up neither display on front panel Line fuse failure Check main fuse in rear side of the unit see 9 Electronic failure Contact service Higher noise and drift Leaking cell dirty cell gas bubbles nontransparent mobile phase old defective lamp flow and temperature fluctuations Perform Lamp test see 6 6 8 1 and Cell test see 14 2 Check cell connection Check mobil...

Page 34: ... the safety instructions for this liquid Before manipulating with the cell turn off the lamp Never touch the cell windows or lens with bare fingers or with sharp or hard tools 11 2 Control of Tubing and Cell Connection Control all cell connections tubing and cell windows if they are not leaking before starting process All leakages must be fixed Check the cell windows for any impurities 11 3 Lamp C...

Page 35: ... lamp with cable and connector only for version 800 ADA40000 Test cell TC01 ADA70000 Analytical cell AC05 l 5 mm 1 16 UNF10 32 ADA60000 Analytical cell AC02 l 2 0 mm 1 16 UNF10 32 ADA50000 Analytical cell AC10 l 10 mm 1 16 UNF10 32 78000110 Quartz window for analytical cell 4 mm ADA53030 Cell lid seal for AC05 and AC10 ADA61030 Microcell AC02 lid seal ...

Page 36: ...il info ecomsro cz www ecomsro com 14 CELLS In the unit may be used the following analytical cells AC 02 optical path length 2 mm and volume 1 ul AC 05 optical path length 5 mm and volume 8 ul AC 10 optical path length 10 mm and volume 16 ul In order to restrict formation of bubbles a hydrodynamic resistor is supplied with the cell to be connected to the outlet capillary Decrease of the effect of ...

Page 37: ... of cell purity and absorbing mobile phase is performed at the wavelength used for measuring or at the wavelengths used in the program Caution Measure on a stabilized unit and measuring cell without bubbles A common problem are also air bubbles stuck inside the cell in the area of light transmission They cause worse measuring results The bubbles may be caused by gas released in the liquid Stuck bu...

Page 38: ...in the cell Check for perfect condition of gaskets and cleanness of sealing surfaces for debris of the window or any other impurities Damaged seals must be replaced After assembly tighten screws crosswise very carefully the windows may crack by excessive tightening therefore use solely horologic screwdriver which does not put on such a great momentum Then inspect the optical aperture by magnifying...

Page 39: ... configurable Wetted materials Depend on a cell fused silica PTFE stainless steel Vespel PEEK Communication RS232 Ethernet LAN Display keypad VFD 140x32 pixels 10 pushbuttons Power supply 100 240 V 50 60 Hz 110 VA Dimensions w x h x d 280 x 135 x 498 mm Weight 10 2 kg Operational environment conditions Indoor use only Altitude up to 2000 m Temperature 5 40 C Humidity maximum relative humidity 80 f...

Page 40: ...600 CE Cat No ADBCE00X and ECD2800 CE Cat No ADACE00X In this chapter is described installation of capillary and basic unit differences No Description 1 Front switch 2 Keyboard 3 Compartment for capillary 4 Drain from cell compartment 5 Leakage sensor 6 Drain channel with cone for connecting waste system 7 Door hinges 8 Slots for tubing and capillaries 9 Display 10 Status LED lights ...

Page 41: ...with bare hands Close the box move the screw back and tighten it Now the capillary is fixed at correct place Note The unit is adjusted with testing capillary and at spectral light maximum about 214 240 nm shall be 100 value of energy with new lamp Note This unit does not include test cell cell nor accessories of cell BELOW ARE STATED ONLY DIFFERENCES FROM BASIC TECHNICAL PARAMETERS OF THE UNIT Par...

Page 42: ...scription 00051478 1 Terminal block 3 pins green EKAB 040 1 LAN cable 1 m K0310000 1 Analog output 18329000 1 Screwdriver Torx T10 99040300 1 Open End Wrench 7 5 5 mm 00016000 1 Door 2000 DOC00001 1 User s guide DOC00002 1 Production protocol ...

Page 43: ...X00X and ECD2800 EX Cat No ADAEX00X These detector versions have differences from basic unit as described in this chapter No Description 1 Front switch 2 Keyboard 3a Output for optical cables light source 3b Input for optical cables light sensor 4 Drain from cell compartment 5 Leakage sensor 6 Drain channel with cone for connecting waste system 7 Door hinges 8 Slots for tubing and capillaries 9 Di...

Page 44: ...he SMA connector for output For input unplug both parts of connector and screw in the SMA connector Test cell ZK EX is used for easy diagnostics of detectors and lamp intensity measuring Connected test cell and working cell Note External cell and fiber optic cables have to be ordered separately according to customer needs Note The sample signal level is adjusted at 100 using two 1 m long fiber opt...

Page 45: ...TATED ONLY DIFFERENCES FROM BASIC TECHNICAL PARAMETERS OF THE UNIT Parameter Value Noise Test cell 254 nm TC 2 s 10 Hz 15 10 6 AU Drift Test cell 254 nm 3 10 4 AU hr BASIC ACCESSORIES P N Qty Picture Description 23984000 1 Tube fuse T 2 5A 250V CSA EKAB 011 1 Mains cable 10A 250V 1 5 m 00051478 1 Terminal block 8 pins green EKAB 040 1 LAN cable 1 m K0310000 1 Analog output QA160000 1 Test cell ZK ...

Page 46: ...y u Prahy Co ID No 41192192 The following technical standards were applied when evaluating conformity EN 55011 ed 3 2010 A1 2011 group 1 class A EN 61000 3 2 ed 3 2006 A1 2010 A2 2010 EN 61000 3 2 2006 A1 2009 A2 2009 EN 61000 3 3 ed 2 2009 EN 61000 3 3 2008 EN 61326 1 ed 2 2013 class A EN 61326 1 2013 art 6 Table 1 EN 61010 1 ed 2 2011 EN 61010 1 October 2010 Evaluation of conformity was performe...

Page 47: ...ECD2800 ECD2600 47 47 ...

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