Daedalus RM, User Manual, Page: 3 / 40

1
TABLE OF CONTENTS
LIST OF FIGURES .................................................................................................... 2
WARNINGS / INFORMATION ................................................................................... 3
ITEMS INCLUDED WITH THE RM SYNTHESIZER .................................................. 4
ITEMS TO BE SUPPLIED BY THE END-USER ........................................................ 5
INSTRUMENT SITE CONSIDERATIONS ................................................................. 6
CONNECTION DETAILS ........................................................................................... 7
THEORY OF OPERATION ...................................................................................... 10
CONVENTIONS USED IN THIS MANUAL .............................................................. 14
VALVE DESCRIPTIONS ......................................................................................... 14
BACK PANEL CONNECTIONS ............................................................................... 16
FRONT PANEL CONTROL ..................................................................................... 17
PREPARING THE INSTRUMENT FOR USE .......................................................... 17
THE MIXING CHAMBER / ADDING REAGENTS .................................................... 19
SEALING THE MIXING CHAMBER ......................................................................... 21
PROTOCOL FOR MAKING SAMPLES ................................................................... 22
TRANSFERRING SAMPLES FROM THE MIXING CHAMBER TO THE NMR CELL
................................................................................................................................. 25
CLEANING THE MIXING CHAMBER ...................................................................... 26
RESETTING THE SYSTEM FOR THE NEXT SAMPLE .......................................... 28
TIPS ......................................................................................................................... 29
CALIBRATING THE SYSTEM ................................................................................. 31
REPLACING THE WINDOW SEALS ....................................................................... 32
SPECIFICATIONS ................................................................................................... 36
FURTHER INFORMATION ...................................................................................... 38