Innovators in
Microwave Chemistry
CEM Corporation
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PO Box 200
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Matthews, NC 28106
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(800) 726-3331
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(704) 821-7015
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www.cempeptides.com
4. Operating
Unit
a. Place the luer plug on the bottom of the reaction vessel and load with desired reactants
b. Place the reaction vessel into the holder and drop into the microwave cavity
c. Place the fiber-optic probe with thermowell cover directly into the reaction vessel
d. Press the Start button on the Discover and the loaded method will run.
e. To drain and wash the reaction vessel, remove it from the microwave and place in the well located in
front of the waste bottle immediately after removing the luer plug. Turn the vacuum pump power on and
the liquid reagents should drain into the 1L bottle.
f. Wash the resin in the reaction vessel with desired solvent.
g. Remove the reaction vessel from the vacuum manifold and re-attach the luer plug. The vessel is now
ready for reagents to be added.
Reaction Vessel Assembly
Reaction Vessel Filtration and Washing