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6 Operation

22

C-660 Operation Manual, Version F

Table 6-4: Parameter menu

Parameter menu

Description

back

Jumps back into 

Main menu

.

Rack type

The predefined rack types FC4 – FC60 and Syncore Racks R4 – R96 can be selected. 
Customized racks are saved under C01 - C10 and U11.

Order

The sequence according to which the individual fractions are filled into the tubes can be 
entered.

  This is the best choice for the racks FC12, 30 and 60 as this order corresponds 

to the rack numeration. The collector arm works within one rack by column 
from left to right and viceversa. Same time intervals between fraction change.

  The collector arm works within one rack line by line from left to right and vice 

versa. Same time intervals between fraction change.

 The collector arm works within one rack line by line only from left to right.

 The collector arm works within one rack by column only from left to right.

If customized racks are used whose collection starts in another corner, the pictogram does not 
reproduce the path precisely.

No. of racks

Number of racks on the drip tray of the Fraction Collector.

No. of tubes

Enter how many tubes are currently in the racks (see also the free positions in the Show mode)

Show 

Shows the position of the individual tubes in the rack in the display and simulates the  
progression of the collector arm.

Collecting

It is possible to set whether collection should take place in fixed  time intervals or according to 
volume (only in connection with a BUCHI pump).

Size

Determines total time or volume according to which the tubes are filled.

Delay

The time prior to the start of the collection function can be entered. During the delay time the 
flow goes into the waste.

Detector

Activates the peak collection function according to detector 1 or detector 2. Default: No 
detector.

Threshold

Defines the signal strength in % of the end-scale deflection at which the peak collection func-
tion is activated. A tube change occurs whenever this threshold is exceeded or is fallen short 
of.

Sensitivity

Defines the sensitivity of the peak defection. According to the noise of detector. Sensitivity 4 is 
the most sensitive and 1 the setting with the lowest sensitivity.

Change

Defines the criteria for a tube change:

  A tube change takes places after threshold is exceeded and upon detection 

of minima.

  A tube change takes places after threshold is exceeded and upon detection 

of minima, and also upon detection of maxima.

Mode

Collection occurs only during the detected peaks. The fractions between the 
peaks below the threshold are directed to the waste container, as well as 
substances not recorded by the detector.
Collection occurs during and between the peaks. All fractions are thus 
collected.

Summary of Contents for C-660

Page 1: ...Fraction Collector C 660 Operation Manual 096969 en...

Page 2: ...eserves the right to make changes to the manual as deemed necessary in the light of experience espe cially in respect to structure illustrations and technical detail This manual is copyright Informati...

Page 3: ...3 Installation 16 5 3 1 Power connection 16 5 3 2 Fitting and ferrule 16 5 3 3 Optional waste diverter valve 16 Read this manual carefully before installing and running your system and note the safet...

Page 4: ...height of the collector arm 24 6 3 4 Interface RS 232 25 6 3 5 Peak detection 25 7 Maintenance 28 7 1 Cleaning 28 8 Troubleshooting 29 8 1 Malfunctions and their remedy 29 8 2 Customer service 30 9 Sh...

Page 5: ...s 96961 96965 UV Monitor C 630 Operation Manual numbers 96950 96953 and 96966 UV Photometer C 635 Operation Manual numbers 96957 96960 and 96967 Cartridger C 670 Operation Manual numbers 96945 96949 1...

Page 6: ...s as a basis for training 2 2 Proper use The Fraction Collector C 660 has been conceived of and constructed as a laboratory instrument Its correct usage is the optimal and reliable collection of indiv...

Page 7: ...uilt in accordance with current state of the art technology however risks to users property and the environment can arise when the instrument is used care lessly or improperly The manufacturer has det...

Page 8: ...The operator shall inform the manufacturer without delay of any safety related incidents which might occur during the operation of the instrument Legal regulations such as local state and federal law...

Page 9: ...r detailed information on the listed products see www buchi com or contact your local dealer 3 1 1 Standard instrument Table 3 1 Standard instrument Product Order number Fraction Collector C 660 44900...

Page 10: ...French 96971 Italian 96972 3 1 3 Optional accessories Table 3 3 Optional accessories Product Order number Waste valve valve for the Fraction Collector Prevents dripping during the fraction change 511...

Page 11: ...0 250 mL tubes for rack FC 12 diameter of 39 mm height of 300 mm 44960 i 20 50 mL tubes for rack FC 30 diameter of 25 mm height of 185 mm 44961 j 100 20 mL tubes for rack FC 60 diameter of 16 mm heigh...

Page 12: ...25 W Frequency 50 60 Hz Installation category II Degree of protection IP20 Pollution degree 2 Environmental conditions Temperature Altitude Humidity for indoor use only 5 40 C up to 2000 m maximum re...

Page 13: ...signals Display Back lit LCD graphic display 28 64 pixels 58 29 mm Dialog languages en de fr it es jp Interfaces 2 RS 485 system bus 1 RS 232 process data output 1 Mini DIN waste valve 1 Mini DIN TTL...

Page 14: ...F switch f FC 60 rack with glass tubes g Drip tray Fig 4 1 Example of System 3 4 2 Function principle The fraction collector is characterized by the following features Up to 12 liters 48 250 mL or up...

Page 15: ...scertained that the instrument is not exposed to aggressive substances such as acids bases and solvents which can have a negative influence on the useful life WARNING The fraction collector is not exp...

Page 16: ...to firmly seal the tubing end with the ferrule Fig 5 2 Installing fitting and ferrule 5 3 3 Optional waste diverter valve If the flow rate of the pumps exceeds 10 mL min a waste diverter valve is rec...

Page 17: ...bing guide f so that it pokes out approximately 3 mm Connect the valve to the WASTE VALVE con nection i 9 Fig 5 3 Installating the waste diverter valve 2 3 4 1 8 5 6 7 9 10 Fig 5 4 Control arrangement...

Page 18: ...Control elements 1 2 3 4 5 a START NEXT button b STOP PAUSE button c Display d Selector switch turn and press knob e ON OFF Power switch Fig 6 1 Control elements of the fraction collector Table 6 1 Fu...

Page 19: ...llection status PAUSE Pressing the STOP Pause button once The program sequence is interrupted and the BUCHI pump modules are stopped no reset Other brand pumps will not be stopped The program sequence...

Page 20: ...in the stop mode You set the desired values by turning the selector switch Press the selector switch in order to confirm the new value After 10 seconds without confirmation the cursor jumps back to t...

Page 21: ...avigation Parameters Table 6 3 Main menu Main menu Description Fraction Displays the current fraction Time or volume It is possible to collect according to time and volume This setting is selected in...

Page 22: ...e rack in the display and simulates the progression of the collector arm Collecting It is possible to set whether collection should take place in fixed time intervals or according to volume only in co...

Page 23: ...programs P01 P10 are deleted Table 6 6 Rack definition menu Rack definition menu Description back Jumps back into the Parameter menu Rectangular rack Jumps into Rack Menu 1 Ractangular rack Irregular...

Page 24: ...erwise the previously defined empty C01 C10 racks C01 C10 can be deleted with a yes no query 6 3 3 Setting the height of the collector arm Setting the height The distance between the collector arm and...

Page 25: ...n in the Waste column in the Wait Pause and Error states While the arm is moving from one position to the next the new tube number and tube position are entered and the Waste column is not marked The...

Page 26: ...ially in the case of only slightly separated peaks this procedure allows the multiple extraction of a fraction with sufficient purity for the subsequent analysis A tube change takes place when crossin...

Page 27: ...n times have considerably flatter flanks and are usually somewhat more agitated such peaks require a more slug gish switching decision The following serves as a rule of thumb Use Range 3 for separatio...

Page 28: ...or to any maintenance work on the instrument switch off the power supply and remove all sources of flammable vapor ATTENTION Use only genuine consumables and spare parts for any maintenance and repair...

Page 29: ...it on again if Arm is jammed appears in the display thus enabling the collector arm to reposition itself Please contact the BUCHI customer service if this measure does not help 8 1 Malfunctions and t...

Page 30: ...ons or application prob lems please contact one of these offices The customer service offers the following Spare part delivery Repairs Technical advice Before calling us Our service personnel will be...

Page 31: ...nces Clean the instrument and all accessories thoroughly to remove possibly dangerous substances Do not clean dusty parts with compressed air Store the instrument and its accessories at a dry place in...

Page 32: ...timum system performance and reliability Prior written permission of the manufacturer should be obtained before any modifications are made to the spare parts used 1 3 4 2 Table 10 1 Spare parts Produc...

Page 33: ...ause harmful interference in which case the user will be required to correct the interference at his own expense Fran ais Cet appareil a t test et s est av r conforme aux limites pr vues pour les appa...

Page 34: ...11 Declarations and requirements 34 C 660 Operation Manual Version F 11 2 Declaration of conformity...

Page 35: ......

Page 36: ...www buchi com cn India BUCHI India Private Ltd IN Mumbai 400 055 T 91 22 667 75400 F 91 22 667 18986 india buchi com www buchi in Indonesia PT BUCHI Indonesia ID Tangerang 15321 T 62 21 537 62 16 F 6...

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