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Bruker minispec, User Manual

The Bruker minispec, a state-of-the-art scientific device, offers precise measurements in a compact size. To ensure users can maximize its potential, a comprehensive User Manual is available for download, absolutely free. Access this valuable resource at manualshive.com, guiding you through every step of operating this remarkable product.

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Copyright © by Bruker Corporation

All rights reserved. No part of this publication may be reproduced, stored in a retrieval
system, or transmitted, in any form, or by any means without the prior consent of the
publisher.  Product  names  used  are  trademarks  or  registered  trademarks  of  their  re-
spective holders.

This manual was written by

Bruker BioSpin AIC

© October 07, 2016 Bruker Corporation

Document Number: 10000031930

P/N: H148850

For further technical assistance for this product, please do not hesitate to contact your

nearest BRUKER dealer or contact us directly at:

Bruker Corporation

Am Silberstreifen

76287 Rheinstetten

Germany

Phone: + 49 721 5161 0

E-mail: [email protected]

Internet: www.bruker.com

Summary of Contents for minispec

Page 1: ...minispec Sample Automation XYZ Sample Changer User Manual Version 003 Innovation with Integrity AIC ...

Page 2: ...r registered trademarks of their re spective holders This manual was written by Bruker BioSpin AIC October 07 2016 Bruker Corporation Document Number 10000031930 P N H148850 For further technical assistance for this product please do not hesitate to contact your nearest BRUKER dealer or contact us directly at Bruker Corporation Am Silberstreifen 76287 Rheinstetten Germany Phone 49 721 5161 0 E mai...

Page 3: ... Design and Function 17 4 1 Sample Changer Components 17 4 2 Additional Equipment Required 19 4 3 Optional Accessories 20 4 4 Chemical Compatibility 20 5 Transport Packaging and Storage 21 6 Installation 23 6 1 Preparing for Installation 23 6 1 1 Choosing a Location 23 6 1 1 1 Space Requirements 24 6 1 1 2 Work Surface Requirements 24 6 1 1 3 Power Requirements 24 6 2 Installing the Temperature Un...

Page 4: ...ample Stage on the Base 51 9 1 4 Connecting the Data Cables 52 9 1 5 Connecting to a Power Source 52 9 2 Operating the Sample Stage 53 10 Maintenance 55 10 1 Cleaning the Sample Changer 55 10 1 1 Daily External Cleaning 55 10 1 2 Weekly Cleaning 56 10 2 Cleaning the Safety Barrier 56 10 3 Mounting the Z Drive Assembly 57 10 3 1 Tools Required 57 10 3 2 Using Tubing Tamers 60 10 3 3 Connecting the ...

Page 5: ...850_3_003 v 14 2 1 Power Requirements 70 14 2 2 Data Connectors Sample Changer 71 14 2 3 Data Connectors Temperature Units 71 14 3 Pneumatic connections 71 15 Contact 73 List of Figures 75 List of Tables 77 Index 79 ...

Page 6: ...Contents vi H148850_3_003 ...

Page 7: ...Bruker s policy to improve products as new techniques and components become available Bruker reserves the right to change specifications at any time Every effort has been made to avoid errors in text and Figure presentation in this publication In order to produce useful and appropriate documentation we welcome your comments on this publication Field Service Engineers are advised to check regularly...

Page 8: ...ce of not following the warning 1 This is the safety condition u This is the safety instruction NOTICE NOTICE indicates a property damage message This is the consequence of not following the notice 1 This is a safety condition u This is a safety instruction SAFETY INSTRUCTIONS SAFETY INSTRUCTIONS are used for control flow and shutdowns in the event of an error or emergency This is the consequence ...

Page 9: ...ce for this manual consists of analytical chemists and laboratory technicians To use this manual effectively you should have a basic knowledge of chemistry a basic knowledge of electronic sampling equipment at least a beginning level of computer experience and working knowledge of other equipment used with the device WARNING Chemical Injury Hazard Exposure to laboratory chemicals may result in ser...

Page 10: ...Introduction 10 H148850_3_003 ...

Page 11: ... requirements of the country where the device was purchased Power is supplied to the device through the included 24V power supply 3 1 2 Power Cord Safety Maintenance The operator should check the condition of the power signal supply cord The device should not be operated if the mains inlet is cracked or broken Any obvious damage to the case from a drop or fall should be checked by service personne...

Page 12: ...d service provider Protection provided by the device may be impaired if the device is used in a manner not specified by the manufacturer WARNING Shock Hazard from Liquids Liquid coming in contact with electrical components may result in a serious injury through shock u Do not allow any liquid to enter the device cabinet other than as intended through the specified tubing or come into contact with ...

Page 13: ...cessary precautions u Always use appropriate personal protective equipment including protective eyewear 3 1 5 Mechanical Hazards If you insert any part of your body between the moving parts of the device you could be injured The figure below shows the location of potential hazards Figure 3 1 Overview of the Mechanical Hazards Without Optional Safety Barrier Figure 3 2 Overview of the Mechanical Ha...

Page 14: ...Do not put hand under the gripper assembly Lifting Hazard Single person lift could cause injury Use assistance when moving or lifting 3 2 Electromagnetic Interference FEDERAL COMMUNICATIONS COMMISSION FCC NOTICE This equipment has been tested and found to comply with the limits for a Class A digital device pursuant to Part 15 of the FCC Rules These limits are designed to provide reasonable protect...

Page 15: ...paratus ICES 001 of the Department of Communications AVIS CANADIEN Cet appareil numérique respecte les limites de bruits radioélectriques applicables aux appareils numériques de Classe A prescrites dans la norme sur le matériel brouilleur Appareils Numériques NMB 001 édictée par le ministre des Communications 3 3 Explanation of Regulatory Marks The CE mark is a registered trademark of the European...

Page 16: ...Safety 16 H148850_3_003 ...

Page 17: ...e gripper mounting bracket The Z Drive motor assembly attaches onto the sample changer arm 3 Gripper Assembly The pneumatic gripper assembly moves vials between the temperature units and the instrument 4 Sample Changer Head The sample changer head contains electronics for the sample changer and supports the sample changer arm 5 Power Indicator Lamp The LED indicates that the sample changer is conn...

Page 18: ... sample changer arm 3 Gripper Assembly The pneumatic gripper assembly moves vials between the temperature units and the instrument 4 Sample Changer Head The sample changer head contains electronics for the sample changer and supports the sample changer arm 5 Power Indicator Lamp The LED indicates that the sample changer is connected to a power source and turned on 8 Base The temperature units and ...

Page 19: ... and is powered and controlled through a connector on the back of the sample changer 6 Gripper Tubing Fittings An internal pump generates air flow to power the pneumatic gripper head 7 E Stop Connector Connector for the emergency stop button The following standard components are also shipped with the sample changer Power Supply A desktop power supply powers the sample changer Communication Cable T...

Page 20: ...er objects coming in contact with the moving arm and gripper of the sample changer Balance Adapter Kit Allows a laboratory balance to be integrated on the rear of the sample stage 4 4 Chemical Compatibility Sample changer components are made of corrosion resistant stainless steel alloys or anodized aluminum The enclosure and base are made from a high strength aluminum alloy that is treated with a ...

Page 21: ... for any kinked tubing If the system is shipped or removed from storage during cold weather allow the packaged equipment to equilibrate to room temperature before opening and exposing to warm humid air It is usually sufficient to provide four to eight hours for this purpose NOTICE Material Damage from Condensation Condensation that forms on or inside the device may cause equipment damage u Allow t...

Page 22: ...Transport Packaging and Storage 22 H148850_3_003 ...

Page 23: ... power is left on motors may move unexpectedly and cause injury u Ensure the device power is off before proceeding with installation 6 1 Preparing for Installation Installing the sample changer requires preparation Before you install the sample changer you should evaluate the physical arrangement of the laboratory to choose a suitable location Once you choose a location you must carefully unpack t...

Page 24: ...of the power supply may result in a fire or shock hazard u Use only the provided power supply u The power supply must be plugged into an outlet which has a protective ground connection u Ensure that the power cord is disconnected before removing any covers The sample changer is intended to operate from DC power supplied through the provided power supply The power supply is provided power through a...

Page 25: ...sen the screws in the two mounting brackets and pull the clamp outward Figure 6 1 Mounting Bracket With the help of an assistant carefully lower the instrument so that the mounting bars on the bottom of the instrument rest in the mounting brackets Tighten the screws See the instrument manual for information on connecting and using the instrument 6 4 Connecting the E Stop Button The e stop button m...

Page 26: ...rument Use the two included screws to attach the bracket to the side of the base Figure 6 2 E Stop Shown on Left Side of the Base Open the button enclosure Insert the two mounting screws through the back of the button and through the holes in the bracket Figure 6 3 Location of Holes in the Bracket Figure 6 4 Location of Mounting Screws ...

Page 27: ...visible Replace the front of the button enclosure Connect the button to the back of the sample changer Figure 6 6 E stop Connected to the Sample Changer 6 4 2 With the Safety Barrier The e stop button is installed when the safety barrier is assembled See the Safety Barrier Assembly Quick Installation Guide Connect the button to the back of the sample changer as shown in Figure 6 6 27 ...

Page 28: ...ard configuration A virtual COM port is created when using the USB and therefore the connection looks like a standard RS 232 serial port to the host PC software The serial RS 232 protocol is also a supported configuration There are two RS 232 serial ports on the sample changer and a serial interface kit may optionally be shipped with the sample changer 6 7 Establishing a USB Communications Interfa...

Page 29: ... installation media Figure 6 7 Message Showing that a Driver was not Found Insert the installation media if necessary Select Install from a specific location and click Next Figure 6 8 Choosing to Install USB Driver Select Search removable media Figure 6 9 Choosing to Install USB Driver from a Removable Media ...

Page 30: ...while the computer searches the media Figure 6 10 Searching for the Driver When the driver is found select it and click Next Figure 6 11 Selecting the Driver The driver installation is complete Figure 6 12 Driver Installation is Complete ...

Page 31: ...1 port Connecting the adapter to the COM2 port on the sample changer will cause a malfunction The sample changer COM2 port is used for communication with the temperature units When interconnecting any computing devices keep the communications cables away from sources of electromagnetic or radio frequency RF interference such as electric motors transformers fluorescent light ballasts or RF energy s...

Page 32: ...h the ASX 7000 alignment utility Refer to the alignment guide or the online help within the alignment software for instructions 6 9 2 Testing the Gripper Once the sample changer has been aligned test it with empty sample vials Load the sample changer with empty sample vials at the positions you wish to test Turn the sample changer power switch on and verify that the LED power indicator is on Use t...

Page 33: ...rd Lifting without assistance may cause injury u Two people are required to lift the device u Lifting should be done with a person situated on either side of the device u Never attempt to lift or move the device when the temperature units and NMR instrument are installed 7 1 Preparing the Sample Changer The following steps must be carried out before assembling the safety barrier Step 1 Turn off po...

Page 34: ... the E stop cover by unscrewing the four screws that hold the cover on Step 4 Remove the E stop bracket from back of the E stop by removing the two screws with a 9 64 Allen wrench while holding the acorn nuts on the back Step 5 Unplug the E stop from the back of the autosampler ...

Page 35: ...using 10 32x 75 FHPH screws Bag G two on each side Make sure the recessed holes for the two screws are facing out Step 7 Remove the four screws holding the back panel of the instrument Step 8 Install the mounting bracket on the left side of the autosampler as viewed from the front using the two screws that were removed previously ...

Page 36: ...embly When positioning the acrylic walls begin with the back segment Step 1 While one person holds the acrylic wall steady secure with two 6 32x0 625 PHPH Bag A screws Ensure that the cables and tubing connected fit in the opening of the back panel and do not get pinched during assembly ...

Page 37: ...Safety Barrier Assembly Installation Optional H148850_3_003 37 Step 2 Fasten the braces to the back wall using 8 32x 375 PHPH Bag B screws three on each bracket Step 3 Next identify the right wall ...

Page 38: ...ng in the remaining 8 32x 1 5 PHPH Bag E screws without the aid of the second person Step 5 Once the base is secure attach the wall to the back panel by affixing it to the two braces using 8 32x 375 PHPH Bag B screws Three for each bracket If both of the heater chiller units are on the base of the unit it is best if you mount the E stop button to the left wall before assembling the wall Otherwise ...

Page 39: ...ier Assembly Installation Optional H148850_3_003 39 Step 6 Unscrew the four screws joining the yellow cap to the button base and remove the cap Step 7 Find the mounting holes on the outer side of the acrylic wall ...

Page 40: ... nuts bag C to mount the stop to the wall The bolts insert into the button s base and the acorn nuts on the bottom of the wall Use a 9 64 Allen wrench for the screws and a 1 4 wrench or nut driver to hold the acorn nut Step 9 Once the base is secure match the TOP s on the base and the cap of the button assembly ...

Page 41: ...er using the same procedure as described in step 4 Step 12 Join the wall to the top brace using 8 32x 375 PHPH Bag B screws three per bracket Step 13 Next secure the wall to the mounting bracket that was installed in the step Preparing the Sample Changer 35 using the four 8 32x 75 PHPH Bag D screws Step 14 Plug the E stop button into the connector on the back panel of the autosampler ...

Page 42: ...el while the second secures one side with three 10 32x0 375 Bag F screws Ensure that the key lock is on the top When finished with one side move to the next while person two is still holding the panel steady Use the other three 10 32x0 375 Bag F screws on the second side The safety barrier is now installed The NMR system is ready for full operation ...

Page 43: ...he temperature does not exceed 80 F 26 C the system is not exposed to condensing humidity and the system is not exposed to excessive flammable or corrosive materials Avoid rough handling of the sample changer If possible do not expose the sample changer to vibration or shock Protect the sample changer from long term exposure to condensation corrosive materials solvent vapor continual standing liqu...

Page 44: ...samples you are analyzing CAUTION Hazard from Mismatched Sample Vials Use of mismatched sample vials may result in malfunctions or sample spills Be sure your vials meet the given requirements 8 2 Starting the Sample Changer Once the samples are loaded you can start the sample changer and let it run until the sampling sequence is finished WARNING Pinch Hazard Keep fingers hair and loose clothing aw...

Page 45: ...he power cord either at the power supply or at the wall outlet 8 5 Using the Safety Barrier The optional safety barrier reduces the possibility of a person or other objects coming in contact with the moving arm and gripper of the sample changer The barrier is not a full enclosure Samples can still be accessed by reaching under the barrier The top is open Two sliding doors on the front of the enclo...

Page 46: ...le changer and unplug the power cord Use the key to turn the latch 2 Slide the handle toward the center 3 Figure 8 2 Safety Barrier Latch To close the safety barrier Slide the handle away from the center Use the key to close the latch The unit can now be plugged in and turned on ...

Page 47: ... to the temperature controller TC3 unit for heating or the nuclear magnetic resonance NMR unit for analysis Figure 9 1 Sample Stage 10 mm Version Shown A power supply and data cables are also provided Features Sample Changer Compatibility Use only with a BRUKER Sample Automation XYZ sample changer Chemical Compatibility Exposed surfaces are made of corrosion resistant stainless steel alloys or ano...

Page 48: ...e from Condensation Condensation that forms on or inside the device may cause equipment damage u Allow the device to dry thoroughly before connecting it to a power source and operating it Remove the packing checklist from the shipping container and check off items against it Leave accessories in the packing until you are ready to install them Keep the factory packaging for use in case the product ...

Page 49: ...le stage on its side The bottom of the sample stage contains a cutout allowing access to the address dial Figure 9 2 Opening on the Bottom of the Sample Stage Insert a wooden probe through the cut out and rotate the dial to C or 12 Figure 9 3 Address Dial ...

Page 50: ... stages are now configured for dual operations The 11 and 12 values will be used as the RS 485 address of the sample stage for all sample stage commands Figure 9 4 Dual Sample Stage Addresses 26 mm Figure 9 5 Dual Sample Stage Addresses 10 mm ...

Page 51: ...ure the device power is off before proceeding with installation Figure 9 6 Base of the Sample Changer Place the sample stage on the base of the autosampler slightly toward the front edge of the base Keep the bottom of the sample stage parallel to the base so that the corners don t gouge the finish on the base Slide the sample stage back until the pins engage the holes You should hear or feel a cli...

Page 52: ...stage 9 1 5 Connecting to a Power Source The sample stage is powered by the supplied external power supply Ensure that you position the sample stage so that the location where the power supply cord plugs into it is easily accessible is not blocked and it can be quickly disconnected if needed In case of hazard the system should be disconnected from the power source Figure 9 8 Power Supply Check the...

Page 53: ...utlet which has a protective ground connection u Ensure that the power cord is disconnected before removing any covers Figure 9 9 Power Connections for the Sample Stage 9 2 Operating the Sample Stage Power On To turn the sample stage on plug in the cord from the provided power supply into the connector on the back of the sample stage Power Off To turn the sample stage off unplug the power cord fro...

Page 54: ...Sample Stage 54 H148850_3_003 ...

Page 55: ...remove contaminants such as abrasives from the sample changer s moving parts It may also be necessary to chemically neutralize spills The following sections explain daily and weekly cleaning procedures WARNING Shock Hazard from Liquids Liquid coming in contact with electrical components may result in a serious injury through shock u Do not allow any liquid to enter the device cabinet other than as...

Page 56: ...sample changer arm tubing NOTICE Hazard from Improper Lubrication Oiling the lead screws will cause gumming galling and binding of the gripper assembly u Never lubricate the lead screws The lead screw nuts are compounded with a dry film lubricant Wipe the sample changer exterior and base until they are clean using a towel dampened with a lab grade cleaning agent followed by a towel dampened with c...

Page 57: ...tructions if you need to mount the Z drive after cleaning or maintenance Reverse the steps if you need to remove the Z drive 10 3 1 Tools Required You will need the following tools Phillips head screwdriver NOTICE Device Damage Hazard Plugging in or unplugging the device cable with the power on may cause serious damage to the device u Plug in the device cable before powering on the device u Do not...

Page 58: ...Maintenance 58 H148850_3_003 Slide the Z drive onto the y arm Figure 10 2 Sliding the Z Drive onto the Y Arm Secure the screw Figure 10 3 Attaching the Z Drive to the Carriage ...

Page 59: ...strain relief block to the sample changer Figure 10 4 Attaching the Z Drive Strain Relief Block Plug the cable into the 15 pin connection port on the rear of the sample changer and tighten the screws Figure 10 5 Connecting the Z Drive Cable ...

Page 60: ...g Tubing Tamers Attach the Tubing Tamer to the Z Drive Run any communications wires and sample tubing along the Z Drive cable through the tamers Figure 10 6 Connecting Tubing Tamer Figure 10 7 Tubing Tamer Properly Installed on Z Drive Cable ...

Page 61: ...nnect the tubing to the appropriate fittings on the back of the sample changer Figure 10 8 Gripper Tubing Connection on Back of Sample Changer Connect the tubing to the appropriate fittings on the gripper Figure 10 9 Gripper Tubing Connected to the Gripper on the Z Drive ...

Page 62: ...m the gripper to the auxiliary connector as shown Figure 10 10 Auxiliary Connector Route the tubes and wires through the tubing tamers Make sure that the tubes and wires are positioned so that they will not catch on anything when the sample changer moves Figure 10 11 Tubing After Installation ...

Page 63: ... supply and also between the power supply and the wall outlet If the cable is plugged in ensure that it is not damaged in any way Check that the LED on the power supply is illuminated If the LED is not illuminated check the wall outlet using a device approved for that purpose If the wall outlet is working and the voltage is acceptable unplug the external power supply from the sample changer but le...

Page 64: ...roubleshoot these problems 11 2 1 USB Cable Problems Check that the USB cable is plugged into the port on the sample changer Check the host computer to ensure that the USB cable is connected to the appropriate USB port Check that the USB cable is not damaged in any way Check the host computer to ensure that the USB drivers are installed for USB operation of the sample changer Load the proper USB d...

Page 65: ...details on the shipping address and also in most cases a Return Merchandise Authorization number RMA number that allows references to the repair case Always refer to this RMA number in case of questions 3 Send the defective part to the local Bruker office and include the following documents RMA sheet if RMA number was assigned Signed Equipment Clearance Form The Equipment Clearance Form will be se...

Page 66: ...Replacement of Parts 66 H148850_3_003 ...

Page 67: ...al information for laboratory and industrial customers within the EU European Union This laboratory product is developed and marketed for Business to Business B2B so does not fall under article 6 clause 3 of the German Act ElectroG To meet the demands of the European Directive 2012 19 EU WEEE 2 Waste of Electrical and Electronic Equipment and the national Equipment Safety Act electrical and electr...

Page 68: ...2012 19 EU WEEE 2 Bruker BioSpin offers to take back the equipment only for deliveries after 23 03 2006 after termination of use at the customer site upon request by the customer This request must be affirmed when the equipment is ordered from Bruker BioSpin Additional costs for dismantling and transport service will apply Only 100 pre decontaminated equipment can and will be accepted by Bruker Bi...

Page 69: ...ty 0 to 80 non condensing for temperatures up to 31 C decreasing linearly to 50 at 40 C Non Operating Relative Humidity 0 to 95 non condensing Pollution Degree Pollution degree 2 Normally no pollution or only dry non conductive pollution occurs The pollution has no influence Occasionally however a temporary conductivity caused by condensation may be expected Table 14 1 Environmental Characteristic...

Page 70: ... A Sample Changer Input DC Voltage and Current 24 V 3 33 A Installation Category CAT I Mains isolated Use only with the provided power supply Sample Stage Power Supply Input AC Voltage Frequency and Current 100 240 V 50 60 Hz 0 5 A Installation Category CAT I Mains isolated Output 24 V DC 0 625 A Sample Stage Input DC Voltage and Current 24 V 0 5 A Installation Category CAT I Mains isolated Use on...

Page 71: ...d signal connection for Z drive 24V max output Connect only to the supplied Z drive using the cable which is part of the Z drive AUXILIARY Controls the gripper Use only with the provided gripper or as instructed by the manufacturer max 24V Table 14 3 Data Connectors on the Sample Changer 14 2 3 Data Connectors Temperature Units COM 1 DB 9 RS 232 serial connection to a controller PC max 12V DC 8 mA...

Page 72: ...Technical Data 72 H148850_3_003 ...

Page 73: ...3181702 Bruker BioSpin Hotlines Contact our Bruker BioSpin service centers Bruker BioSpin provides dedicated hotlines and service centers so that our specialists can respond as quickly as possible to all your service requests applications questions software or technical needs Please select the service center or hotline you wish to contact from our list available at https www bruker com service inf...

Page 74: ...Contact 74 H148850_3_003 ...

Page 75: ...mple Changer 27 Figure 6 7 Message Showing that a Driver was not Found 29 Figure 6 8 Choosing to Install USB Driver 29 Figure 6 9 Choosing to Install USB Driver from a Removable Media 29 Figure 6 10 Searching for the Driver 30 Figure 6 11 Selecting the Driver 30 Figure 6 12 Driver Installation is Complete 30 Figure 8 1 E Stop Button 45 Figure 8 2 Safety Barrier Latch 46 Figure 9 1 Sample Stage 10 ...

Page 76: ...850_3_003 Figure 10 8 Gripper Tubing Connection on Back of Sample Changer 61 Figure 10 9 Gripper Tubing Connected to the Gripper on the Z Drive 61 Figure 10 10 Auxiliary Connector 62 Figure 10 11 Tubing After Installation 62 ...

Page 77: ...7 List of Tables Table 6 1 Physical Characteristics 24 Table 14 1 Environmental Characteristics 69 Table 14 2 Power Requirements 70 Table 14 3 Data Connectors on the Sample Changer 71 Table 14 4 Data Connectors Temperature Units 71 ...

Page 78: ...List of Tables 78 H148850_3_003 ...

Page 79: ...upply 63 LEDs 17 lifting instructions 21 23 33 M mains disconnect 11 O operator qualifications 9 P pollution degree 69 power connections 28 power on procedure 44 requirements 24 70 Power connections Sample Stage 52 power cord 11 Q qualifications operator 9 R regulatory notices 11 S safety barrier 20 safety information 11 Sample changer 17 Sample stage 19 20 Symbols and Conventions Safety 7 T TC3 T...

Page 80: ...Index 80 H148850_3_003 ...

Page 81: ...H148850_3_003 81 ...

Page 82: ...Bruker Corporation info bruker com www bruker com Order No H148850 ...

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