Bruker minispec TC3 User Manual Download Page 2 | Manualshive

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Copyright © by Bruker Corporation

All rights reserved. No part of this publication may be reproduced, stored in a retrieval
system, or transmitted, in any form, or by any means without the prior consent of the
publisher. Product names used are trademarks or registered trademarks of their re-
spective holders.

This manual was written by

Bruker BioSpin AIC

© December 14, 2016 Bruker Corporation

Document Number: 10000031931

P/N: H148851

For further technical assistance for this product, please do not hesitate to contact your

nearest BRUKER dealer or contact us directly at:

Bruker Corporation

Am Silberstreifen

76287 Rheinstetten

Germany

Phone: + 49 721 5161 0

E-mail: [email protected]

Internet: www.bruker.com

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Summary of Contents for minispec TC3

Page 1: ...minispec Temperature Unit TC3 User Manual Version 004 Innovation with Integrity AIC ...

Page 2: ...r registered trademarks of their re spective holders This manual was written by Bruker BioSpin AIC December 14 2016 Bruker Corporation Document Number 10000031931 P N H148851 For further technical assistance for this product please do not hesitate to contact your nearest BRUKER dealer or contact us directly at Bruker Corporation Am Silberstreifen 76287 Rheinstetten Germany Phone 49 721 5161 0 E ma...

Page 3: ...omagnetic Interference 13 3 3 Explanation of Regulatory Marks 13 4 Technical Data 15 4 1 Environmental Characteristics 15 4 2 Electrical Characteristics 15 4 3 Gas Connection 16 4 4 Thermal Characteristics 16 5 Transport Packaging and Storage 19 6 Installation 21 7 Operation 23 7 1 Power On 23 7 2 Power Off 23 7 3 Controlling the Temperature 23 7 4 Understanding the LEDs 23 7 4 1 Power Indicator 2...

Page 4: ...Contents iv H148851_4_004 9 2 Disposal Europe 35 9 3 Disposal USA and Other Countries 36 10 Contact 37 List of Figures 39 List of Tables 41 Index 43 ...

Page 5: ...Bruker s policy to improve products as new techniques and components become available Bruker reserves the right to change specifications at any time Every effort has been made to avoid errors in text and Figure presentation in this publication In order to produce useful and appropriate documentation we welcome your comments on this publication Field Service Engineers are advised to check regularly...

Page 6: ...ce of not following the warning 1 This is the safety condition u This is the safety instruction NOTICE NOTICE indicates a property damage message This is the consequence of not following the notice 1 This is a safety condition u This is a safety instruction SAFETY INSTRUCTIONS SAFETY INSTRUCTIONS are used for control flow and shutdowns in the event of an error or emergency This is the consequence ...

Page 7: ...ersions 10 mm SFC version The unit holds vials in three temperature controlled zones Each zone holds 60 vials with a maximum temperature of 100 C 10 mm polymers version The unit holds vials in one temperature controlled zone The zone holds 60 vials with a maximum temperature of 110 C 26 mm version The unit holds vials in two temperature controlled zones Each zone holds 12 vials with a default maxi...

Page 8: ...o 110 C Sample Changer Compatibility Use only with an ASX 7600 pick and place NMR sample changer Chemical Compatibility Exposed surfaces are made of corrosion resistant stainless steel alloys or anodized aluminum 2 3 Intended Use This equipment is designed for use in analytical laboratories performing chemical analysis of samples ...

Page 9: ...Power is supplied to the device through the included 24V power supply 3 1 2 Power Cord Safety Maintenance The operator should check the condition of the power signal supply cord The device should not be operated if the mains inlet is cracked or broken Any obvious damage to the case from a drop or fall should be checked by service personnel for loose or damaged parts Refer to the individual part li...

Page 10: ...ower cord is disconnected before removing any covers 3 1 4 Mechanical Hazards Figure 3 1 Bottom View with Filter Drawer Removed WARNING Laceration Hazard If the unit power is left on the spinning fan blade just above the filter may cause injury u Ensure the AC power is off before removing the filter WARNING Lifting Hazard Lifting without assistance may cause injury u Two people are required to lif...

Page 11: ...ovider Protection provided by the device may be impaired if the device is used in a manner not specified by the manufacturer WARNING Shock Hazard from Liquids Liquid coming in contact with electrical components may result in a serious injury through shock u Do not allow any liquid to enter the device cabinet other than as intended through the specified tubing or come into contact with any electric...

Page 12: ...ary precautions u Always use appropriate personal protective equipment including protective eyewear 3 1 7 Explanation of Warning Labels Warning symbol marked on device This symbol means Attention Refer to the manual Warning symbol marked on equipment This symbol means Hot surface Touching external surfaces of the instrument can cause burn injury Do not touch the instrument until it has cooled down...

Page 13: ...ifications made to this device that are not expressly approved by the manufacturer may void the user s authority to operate the equipment CABLES Connections to this device must be made with shielded cables with metallic RFI EMI connector hoods to maintain compliance with FCC Rules and Regulations CANADIAN NOTICE This digital apparatus does not exceed the Class A limits for radio noise emissions fr...

Page 14: ...Safety 14 H148851_4_004 ...

Page 15: ...ution degree 2 Normally no pollution or only dry non conductive pollution occurs The pollution has no influence Occasionally however a temporary conductivity caused by condensation may be expected Table 4 1 Environmental Characteristics For indoor use only Avoid sudden extreme temperature changes which could cause condensation on circuit boards in the device 4 2 Electrical Characteristics Power In...

Page 16: ...ore than 35 kPa 5 psi 0 35 bar A typical gas flow of 0 5 liter minute shall apply 4 4 Thermal Characteristics Temperature calibration and validation is performed at the factory Figure 4 1 Thermal Characteristics of a 3 Zone 10 mm SFC Version Zone Default Temperature Temperature Range 3 0 C 0 C to 66 C 2 65 C Ambient 5 C to 66 C 1 100 C Ambient 5 C to 100 C ...

Page 17: ...Technical Data H148851_4_004 17 Figure 4 2 Thermal Characteristics of a 1 Zone 10 mm Polymers Version Zone Default Range 1 Ambient 5 C to 110 C ...

Page 18: ...Technical Data 18 H148851_4_004 Figure 4 3 Thermal Characteristics of a 2 Zone 26 mm Version Zone Temperature Range 2 Ambient 5 C to 80 C 1 Ambient 5 C to 80 C ...

Page 19: ...m storage during cold weather allow the packaged equipment to equilibrate to room temperature before opening and exposing to warm humid air It is usually sufficient to provide four to eight hours for this purpose CAUTION Equipment Damage from Condensation If condensation forms on or inside the unit allow it to dry thoroughly before connecting it to a power source and operating it Failure to do so ...

Page 20: ...Transport Packaging and Storage 20 H148851_4_004 ...

Page 21: ...r Service or personnel authorized by Bruker Installation initial commissioning retrofitting repairs adjustments or dismantling of the device must only be carried out by Bruker Service or personnel authorized by Bruker Damage due to servicing that is not authorized by Bruker is not covered by your warranty ...

Page 22: ...Installation 22 H148851_4_004 ...

Page 23: ...puter sends commands to the sample changer which then passes the commands through to the power supply 7 4 Understanding the LEDs There are two kinds of LEDs on the temperature unit A power indicator Status indicators for each temperature control zone Figure 7 1 LEDs for 10 mm SFC version with 3 zones 7 4 1 Power Indicator Green Lighted green when power is connected 7 4 2 Zone Status Indicators Red...

Page 24: ...Operation 24 H148851_4_004 ...

Page 25: ... power supply just above the power cord connector Figure 8 1 Fuse Holder for the TC3 Disconnect the power cord Inspect all of the equipment which is plugged into the power supply for moisture or other conditions which might pose a hazard and cause the new fuse to blow Using your fingernails or a small flat blade screwdriver squeeze the ends of the fuse holder Pull the fuse holder out Replace the b...

Page 26: ...FC version of the TC3 includes a user replaceable air filter Contact Bruker for information on replacement filters WARNING Laceration Hazard If the unit power is left on the spinning fan blade just above the filter may cause injury u Ensure the AC power is off before removing the filter Turn the power switch off Pull the filter drawer open Figure 8 3 Opening the Filter Drawer ...

Page 27: ...e the exterior surfaces only using a towel dampened with a lab grade cleaning agent Repeat the previous step using a towel dampened with clear water Dry the device exterior using a dry towel WARNING Shock Hazard from Liquids Liquid coming in contact with electrical components may result in a serious injury through shock u Do not allow any liquid to enter the device cabinet other than as intended t...

Page 28: ...ause the temperature controller may contain sample liquids as well as condensed moisture Use a disposable filter so that all glass shards may be safely disposed of The vacuum attachment which is supplied in the optional kit fits a vacuum hose with an outer diameter of 1 1 4 inches Isopropyl alcohol Mild detergent Flashlight Personal protective equipment A brush micro cleaning attachment and pestle...

Page 29: ...amaged vials from the temperature controller Only the broken vial should remain WARNING Laceration Hazard Coming in contact with broken glass vials may result in a laceration injury u Be careful not to cut yourself on the broken vial If sharp edges are exposed use forceps or wear heavy gloves even when handling the undamaged vials u Follow your workplace safety rules Figure 8 6 Example of a Broken...

Page 30: ...Maintenance 30 H148851_4_004 Figure 8 7 Bottle Cylinder Brush Figure 8 8 Inserting the Brush into the Broken Vial Figure 8 9 Removing the Broken Vial with the Brush ...

Page 31: ...he rod pestle in the surrounding openings in the event any of the breakage spilled into them Note If the module is cooling set the temperature to 65 C to liquefy any fat which has accumulated at the bottom of the block Figure 8 10 Steel Rod Figure 8 11 Breaking the Remaining Glass into Fine Granules with the Steel Rod Use the shop vacuum with the attachment to extract the glass particles Also clea...

Page 32: ...t to Remove Glass Particles Once all the broken glass has been extracted jet some isopropyl alcohol into the temperature controller Use warm water and a mild detergent on the brush to clean any fat from the bottom of the heater chiller block Figure 8 14 Jetting Isopropyl Alcohol into the Heater Chiller Block ...

Page 33: ...nce H148851_4_004 33 Figure 8 15 Using Warm Water and Detergent on the Brush to Clean the Bottom Use a flashlight to check that all glass particles have been removed Use the brush to clean any overlooked debris ...

Page 34: ...Maintenance 34 H148851_4_004 ...

Page 35: ...ronmental protection regulations 9 2 Disposal Europe Environmental information for laboratory and industrial customers within the EU European Union This laboratory product is developed and marketed for Business to Business B2B so does not fall under article 6 clause 3 of the German Act ElectroG To meet the demands of the European Directive 2012 19 EU WEEE 2 Waste of Electrical and Electronic Equip...

Page 36: ...2012 19 EU WEEE 2 Bruker BioSpin offers to take back the equipment only for deliveries after 23 03 2006 after termination of use at the customer site upon request by the customer This request must be affirmed when the equipment is ordered from Bruker BioSpin Additional costs for dismantling and transport service will apply Only 100 pre decontaminated equipment can and will be accepted by Bruker Bi...

Page 37: ...3181702 Bruker BioSpin Hotlines Contact our Bruker BioSpin service centers Bruker BioSpin provides dedicated hotlines and service centers so that our specialists can respond as quickly as possible to all your service requests applications questions software or technical needs Please select the service center or hotline you wish to contact from our list available at https www bruker com service inf...

Page 38: ...Contact 38 H148851_4_004 ...

Page 39: ...ng the Filter Drawer 26 Figure 8 4 Removing and Installing the Filter 27 Figure 8 5 Brush Micro Cleaning Attachment for Shop Vacuum and Steel Rod 28 Figure 8 6 Example of a Broken Vial 29 Figure 8 7 Bottle Cylinder Brush 30 Figure 8 8 Inserting the Brush into the Broken Vial 30 Figure 8 9 Removing the Broken Vial with the Brush 30 Figure 8 10 Steel Rod 31 Figure 8 11 Breaking the Remaining Glass i...

Page 40: ...List of Figures 40 H148851_4_004 ...

Page 41: ...List of Tables H148851_4_004 41 List of Tables Table 4 1 Environmental Characteristics 15 Table 4 2 Electrical Characteristics 15 ...

Page 42: ...List of Tables 42 H148851_4_004 ...

Page 43: ...otice 13 Filter 26 Fuse 25 H humidity 11 15 19 I ICES 001 13 intended use 8 interference 13 L Lamps LEDs 23 LEDs 23 lifting instructions 10 19 M mains disconnect 9 P pollution degree 15 power cord 9 R Regulatory notices 9 S Safety information 9 Symbols and Conventions Safety 5 T Temperature Operating 15 Temperature range 16 Tubing kinks 19 ...

Page 44: ...Index 44 H148851_4_004 ...

Page 45: ...H148851_4_004 45 ...

Page 46: ...Bruker Corporation info bruker com www bruker com Order No H148851 ...

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