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M19-354

Page 5

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2019 AMETEK Brookfield Inc.  All rights reserved.

I. INTRODUCTION

Falling Ball Viscometer, Model KF40, complies with the German industry standard DIN 53015.  

The measuring principle, according to Höppler, is to determine the falling time of a ball in a 

cylindrical glass tube filled with liquid.  The working angle of the falling tube in the KF40 

are variable at 80°, 70°, 60° and 50°

 relative to horizontal.  The water jacket, surrounding the 

falling tube, when connected to a Brookfield circulating temperature bath provides for precise 

temperature control of the sample.  

The user calculates the dynamic viscosity of the sample by determining the falling time of the 

ball between the upper and lower ring marks displayed on the falling tube.  Using data on the 

ball constants, the density difference between the liquid sample and the ball, and the working 

angle constant, a mathematical equation is used to convert the time measurement to a viscosity 

value in centipoise.

Note: 

   The ball constants (forwards and backwards) and ball densities are listed on the test 

certificate accompanying the instrument.  You must provide the density value for the 

liquid that you are testing.

The six (6) balls with different diameters and densities enable the KF40 to measure a wide 

range of viscosities.  The ability to adjust the angle of inclination extends the measuring range 

for low viscosity liquids.

For non-Newtonian liquids, by subjecting the same sample to repetitive measurements with the 

KF40 at different angles, pseudoplastic or dilatant behavior may be determined as explained in 

Section IV.  Time dependent behavior (thixotropy and rheopexy) may also be noted.

The ease of operation and precise temperature control, using a Brookfield circulating temperature 

bath, allows for very reproducible measuring results.

  I.1  Components

Component 

Part No. 

Quantity

KF40 Falling Ball Viscometer 

KF40 

1

Set of (6) balls with gauge (FB68) in a carrying case (FB26) 

FB30C 

1

Supplied w/certificate stating diameter and mass of each ball

  -Ball 1 (glass) 

FB1 

-

  -Ball 2 (glass) 

FB2 

-

  -Ball 3 (nickel and iron) 

FB3 

-

  -Ball 4 (nickel and iron) 

FB4 

-

  -Ball 5 (steel) 

FB5 

-

  -Ball 6 (steel) 

FB6 

-

Ball Tweezers 

FB51 

1

Wire Cleaning Brush for Sample Tube 

FB53 

1

Brush to clean loose debris from Falling Balls 

FB52 

1

Summary of Contents for KF40

Page 1: ...ON 11 Commerce Boulevard Middleboro MA 02302 USA Tel 508 946 6200 or 800 628 8139 USA excluding MA Fax 508 946 6262 Internet http www brookfieldengineering com BROOKFIELD KF40 Falling Ball Viscometer...

Page 2: ......

Page 3: ...mple Tube 11 II 3 Temperature Control of the Sample 12 II 4 Measuring the Falling Time 12 III CALCULATIONS 14 III 1 Dynamic Viscosity 14 III 2 Kinematic Viscosity 15 IV DETERMINATION OF THE NON NEWTON...

Page 4: ......

Page 5: ...ll densities are listed on the test certificate accompanying the instrument You must provide the density value for the liquid that you are testing The six 6 balls with different diameters and densitie...

Page 6: ...7x104 mPa s cP Falling Time Lower Limit 60 s for Ball No 1 30 s for Ball Nos 2 3 4 5 and 6 Falling Time Upper limit 300 s Materials with viscosity 7x104 mPa s require running times of over 300 s Meas...

Page 7: ...ed in the DIN53015 standard To determine the accuracy of the viscometer for balls 1 4 5 and 6 please refer to the method specified in the DIN 53015 standard I 4 Description of the Equipment Refer to F...

Page 8: ...meter See Appendix B 6 Thethermometerscrew 11 andthermometerseal 13 withinsertedthermometerisscrewed into M10x1Thermometer attachment thread 12 in the upper plate The thermometer screw should be tight...

Page 9: ...Part No FB64 6 Glass Tube 15 94mm dia with s n oriented 17 Lower Locking Plug Part No FB66 towards the top of the instrument Part No FB76 18 Cap Part No FB63 7 Upper Plate 19 Viscometer seal A 16mm x...

Page 10: ...alls These components material glass Ni iron steel perbunane silicone stainless steel surfaces must not be damaged or subject to chemical action by the cleaning fluid The cleaning procedure is to be c...

Page 11: ...scometers is not permitted Otherwise the ball constants lose their validity When the falling time for the ball is less than the minimum time turbulence may occur II 2 Filling the Sample Tube To fill t...

Page 12: ...Working Fluids Tubing 5 to 20 C Water distilled glycol mixture mixed in accordance with the manufacturer s instructions for the temperature range Insulated Latex tubing secured with tube band clips 1...

Page 13: ...same height as the ring mark shows the ball periphery more distinctly With dark liquids you can better observe the ball in the sample tube by looking from behind the instrument Possible variations in...

Page 14: ...g F working angle constant Angle of inclination a applied to the level Working angle constant F 80 DIN 1 0 70 0 952 60 0 879 50 0 778 The density and ball constant are each stated in the test certific...

Page 15: ...ights reserved III 2 Kinematic Viscosity The conversion of the dynamic viscosity into the kinematic viscosity is accomplished using the following equation Equation 2 2 Kinematic viscosity mm2 s Dynami...

Page 16: ...ity Pseudoplasticity and Dilatancy Using the KF40 Falling Ball Viscometer at different angles may serve to determine pseudoplastic or dilatant behavior for non Newtonian liquids If the sample is non N...

Page 17: ...ve that the ends of the sample tube project evenly from the upper and lower plates 7 Re calibrate all the ball constants according to Appendix B A 2 Exchanging the Water Bath Jacket Caution Glass Comp...

Page 18: ...o the method in DIN 53015 at 20 C 05 C A suitably calibrated thermometer can be obtained from your local authorized dealer on request Ball 6 is not recommended for use in performing a calibration chec...

Page 19: ...ing MA MID sales ametek com Available Online Brookfield has a growing number of published articles that can be downloaded directly from the Brookfield website These articles can be found on our main s...

Page 20: ...vice in the United States return to AMETEK Brookfield 11 Commerce Boulevard Middleboro MA 02346 U S A Telephone 508 946 6200 Fax 508 923 5009 www brookfieldengineering com For repair or service outsid...

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