7-32
PN 4237215AA (October 2011)
WARNING
Use proper safety equipment when handling liquid nitrogen, including, but not
limited to, safety glasses and low temperature thermal gloves.
WARNING
Always temper new dewars by adding a small quantity of liquid nitrogen and swirling
the liquid in the dewar before filling. This reduces the risk of implosion and injury.
IMPORTANT
Do not load the dewar onto the dewar rack until instructed to do so by a message on
the touch screen. Doing so will condense nitrogen on the sample, causing low
surface area results.
Figure 7.20 Adding Liquid Nitrogen to Dewar
Summary of Contents for SA 3100
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Page 17: ...PN 4237215AA October 2011 1 1 Screens Analysis Outgas Profiles Analysis ...
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Page 25: ...PN 4237215AA October 2011 3 3 Figure 3 1 Shipping lnsert ...
Page 28: ...3 6 PN 4237215AA October 2011 Figure 3 4 Connecting Vacuum Line to the Vacuum Pump ...
Page 29: ...PN 4237215AA October 2011 3 7 ...
Page 30: ...3 8 PN 4237215AA October 2011 Figure 3 6 Placing Vacuum Pump into Pump Shelf ...
Page 33: ...PN 4237215AA October 2011 3 11 IMPORTANT The cylinder pressure must be at least 100 psig ...
Page 34: ...3 12 PN 4237215AA October 2011 Figure 3 8 Gas Line Connections to the Analyzer ...
Page 35: ...PN 4237215AA October 2011 3 13 IMPORTANT The cylinder pressure must be at least 100 psig ...
Page 37: ...PN 4237215AA October 2011 3 15 Figure 3 1 0 Seating the O ring ...
Page 39: ...PN 4237215AA October 2011 3 17 Figure 3 1 2 Saturation Tube Installation 7 Analysis ...
Page 40: ...3 18 PN 4237215AA October 2011 Figure 3 1 3 Analyzer Power up Figure 3 1 4 Analysis Screen ...
Page 41: ...PN 4237215AA October 2011 3 19 Analysis Setup and Print Analysis ...
Page 43: ...PN 4237215AA October 2011 4 1 J ...
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Page 45: ...PN 4237215AA October 2011 4 3 Figure 4 1 SA 31 00 Analyzer Front View ...
Page 46: ...4 4 PN 4237215AA October 2011 Figure 4 2 SA 3100 Analyzer Back View ...
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Page 48: ...4 6 PN 4237215AA October 2011 Figure 4 3 Analysis Screen Analysis ...
Page 50: ...4 8 PN 4237215AA October 2011 Analysis Analysis Analysis Analysis ...
Page 51: ...PN 4237215AA October 2011 4 9 Outgas Figure 4 6 Outgas Screen Outgas Outgas Analysis Analysis ...
Page 52: ...4 10 PN 4237215AA October 2011 Profile Figure 4 7 Profile Screen Sample Information ...
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Page 54: ...5 2 PN 4237215AA October 2011 Figure 5 1 Sample Tube Assembly ...
Page 55: ...PN 4237215AA October 2011 5 3 Figure 5 2 Weighing the Sample Tube Assembly ...
Page 58: ...5 6 PN 4237215AA October 2011 Profiles Figure 5 6 Sample lnformation Screen ...
Page 60: ...5 8 PN 4237215AA October 2011 Outgas Outgas Outgas Outgas 1 Outgas ...
Page 67: ...PN 4237215AA October 2011 5 15 Figure 5 14 lnstalling Dewar Lid ...
Page 69: ...PN 4237215AA October 2011 5 17 Figure 5 1 5 Specific Surface Area Result Screen ...
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Page 79: ...PN 4237215AA October 2011 6 Figure 6 1 ldealized V T Plots ...
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Page 87: ...PN 4237215AA October 2011 7 5 Printer Setup and Print Analysis Profile New Profile ...
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Page 98: ...7 16 PN 4237215AA October 2011 Calculations Calculation Calculation Calculations Calculation ...
Page 100: ...7 18 PN 4237215AA October 2011 ...
Page 101: ...PN 4237215AA October 2011 7 19 Figure 7 1 1 Sample Tube Assembly ...
Page 103: ...PN 4237215AA October 2011 7 21 Figure 7 1 3 Adding Sample to the Sample Tube ...
Page 104: ...7 22 PN 4237215AA October 2011 Sample Information Outgassed Samples Sample Information ...
Page 109: ...PN 4237215AA October 2011 7 27 Outgas ...
Page 113: ...PN 4237215AA October 2011 7 31 Figure 7 19 Connecting the Sample Tube to the Analysis Port ...
Page 115: ...PN 4237215AA October 2011 7 33 Figure 7 21 Loading the Dewar into Dewar Rack ...
Page 119: ...PN 4237215AA October 2011 7 37 Screen Outputs Analysis Outgas Setup and Print ...
Page 120: ...7 38 PN 4237215AA October 2011 Setup Advanced Setup Advanced Setup ...
Page 121: ...PN 4237215AA October 2011 7 39 Setup and Print ...
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Page 126: ...PN 4237215AA October 2011 Figure 8 2 Seating the O ring ...
Page 128: ...PN 4237215AA October 2011 Figure 8 4 Draining Vacuum Pump Oil ...
Page 130: ...PN 4237215AA October 2011 Figure 8 5 Rinsing the Fan Filter ...
Page 131: ...PN 4237215AA October 2011 Figure 8 6 Oil Mist Filter Installation ...
Page 134: ...PN 4237215AA October 2011 Setup and Print Analysis ...
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Page 139: ...PN 4237215AA October 2011 A 1 ...
Page 140: ...A 2 PN 4237215AA October 2011 Figure A l SA VIEW Program Window ...
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Page 144: ...A 6 PN 4237215AA October 2011 Sample Information ...
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Page 147: ...PN 4237215AA October 2011 A 9 Figure A 4 Overlayed Results Dialog Box ...
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Page 149: ...PN 4237215AA October 2011 A 11 Figure A 5 Print Preview Screen ...
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Page 152: ...A 14 PN 4237215AA October 2011 Figure A 6 SA VIEW Program Copyright Dialog Box ...
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Page 157: ...PN 4237215AA October 2011 INDEX 1 A B C D ...
Page 158: ...PN 4237215AA October 2011 E F G H I K L M N ...
Page 159: ...PN 4237215AA October 2011 O P R ...
Page 160: ...PN 4237215AA October 2011 S T U ...
Page 161: ...PN 4237215AA October 2011 V W ...
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Page 163: ...PN 4237215AA October 2011 REFERENCES 1 ...
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