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ATAGO 3534, Instruction Manual

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3534-E06 

 
 
 
 
 
 
 

In-line Dimethylformamide Monitor 

CM-800

-DMF 

 
 
 

Instruction Manual 

Cat.No.3534 

 
 
 
 

Summary of Contents for 3534

Page 1: ...3534 E06 In line Dimethylformamide Monitor CM 800 DMF Instruction Manual Cat No 3534 ...

Page 2: ......

Page 3: ...et unit optional 16 7 Connecting the Power Cable or AC Adapter AD 32 AD 33 or AD 34 Optional 17 1 When the instrument is used alone 17 2 When the AC adapter AD 32 AD 33 or AD 34 Optional is used 18 8 External Output 19 1 Recorder output 19 2 RS 232C output 20 9 Power Supply 24 1 When the instrument is used alone 24 2 When the AC adapter AD 32 AD 33 or AD 34 optional is used 24 10 Measuring DMF sol...

Page 4: ...ollowing pages Explanation of indications WARNING If this indication is neglected and the instrument is handled incorrectly serious injury or death may result CAUTION If this indication is neglected and the instrument is handled incorrectly injury and or property damage may result Explanation of symbols This symbol denotes an item of which to be warned or cautioned The contents of warning are desc...

Page 5: ... ATAGO Distributor for an inspection Do not attempt to repair modify or disassemble the instrument yourself Improper servicing may result in fire electrical shock or burns If the instrument is dropped or is subjected to a strong shock have it inspected by an Authorized ATAGO Service Center Fire or malfunction may result if the instrument is used CAUTION Do not apply water or sample to any part of ...

Page 6: ... 32 AD 33 or AD 34 optional is used disconnect the power cable plug from the AC 100 240V outlet When transporting the instrument pack it in the original box When transporting by aircraft disconnect the power DC24V cable or the DC output cable of the AC adapter AD 32 AD 33 or AD 34 optional from the power input terminal of the instrument Carefully read this instruction manual and fully understand t...

Page 7: ...ck or burn For repair service of the power cable and plug contact an Authorized ATAGO Service Center Do not cut a plug to extend the power cable of the AD 32 AD 33 or AD 34 CAUTION Do not insert or pull out the connector and plug with wet hands When disconnecting the power cable of the AC adapter AD 32 AD 33 or AD 34 optional from the AC 100 240V outlet remove by pulling on the plug only Pulling t...

Page 8: ... power DC24V prior to connecting cables to the individual units If the AC adapter AD 32 AD 33 or AD 34 optional is used pull out the power cable plug from the AC100 240V outlet before connecting Connecting the cables while the power is on may result in electrical shock ...

Page 9: ... the temperature is extremely low Do not leave the instrument in a damp place Do not place or drop heavy objects on the instrument Use this instrument under the condition where humidity is 80 at 31 or lower falling linearly to 50 at 40 Main supply voltage fluctuation should not to exceed 10 the nominal voltage Installation categories Overvoltage Categories ｌｌ The pollution degree is 2 according to...

Page 10: ... the Refractive Index of the medium χ The Refractive Index varies with the wavelength of light and temperature and is represented as follows For example Refractive Index of water at 20 under the D line is 1 33299 Generally expressed as nD 1 33299 m The Refractive Index is based upon the supposition that the Refractive Index in a vacuum is 1 and is called the absolute Refractive Index Generally how...

Page 11: ... The AD 33 is an adapter that converts AC 110V to DC24V for supplying power to the instrument The AD 34 is an adapter that converts AC 220 240V to DC24V for supplying power to the instrument Sample inlet unit IDF ISO clamp union ferrule IDF ISO screw union screw JIS Flange small diameter series compression fitting and hose connector are available Refer to page 34 18 Consumable Parts and Optional I...

Page 12: ...d be connected to a power supply of AC 100 240V 50 60 Hz The instrument should be installed in a location with an ambient temperature of 5 to 40 Because the instrument incorporates highly precise components DO NOT install in locations exposed to direct sunlight or near a heating source or in an environment that is dusty or exposed to corrosive gasses The instrument should be installed in a locatio...

Page 13: ... the electric circuit from overheating Mounting screw locations Used to mount the instrument to the stand Operation display Comprised of the operation keys and display C 2 Operation Display page 12 Power DC24V input terminal Terminal to connect the power cable for DC24V input or the DC output cable of the AC adapter AD 32 AD 33 or AD 34 optional RS 232C output terminal Terminal to connect to a com...

Page 14: ...alue 4 Recorder output upper limit value 5 This setting mode is not applicable to this unit Fig 4 3 Up and down keys Increase or decrease the value in each setting mode The down key also switches the display of each setting mode The temperature is displayed when press the down key while measuring a sample 3 AC Adapter AD 32 AD 33 or AD 34 Optional Power cable Connects to the AC 100 240V outlet DC ...

Page 15: ...ws supplied with the stand to mount the instrument and AD 32 AD 33 or AD 34 on the stand or panel plate The depth of the screw locations is 10mm M6 Instrument Fig 5 1 AD 32 AD 33 or AD 34 Fig 5 2 Example of screw configuration Fig 5 3 The instrument or AD 32 AD 33 or AD 34 Washer M6 Spring washer M6 Hexagonal head bolt M6 10 m Hexagonal head bolts spring washers and washers are included as standar...

Page 16: ...re beginning Electrical shock may occur if the unit is mounted with the power connected CAUTION Ensure that the prism is clean and free of any damage and or scratches Completely remove any sample before installing the instrument to piping or equipment 1 Installation of the instrument with the sample inlet unit optional Compression Fitting Hose connector Straight type L type Fig 6 1 ...

Page 17: ...ism surface may become contaminated with solids dirt and or grease If this happens the prism surface must be cleaned by hand C 16 Cleaning the Prism page 32 The sample inlet unit should be installed in such a manner that it can be easily removed to allow access to the prism for cleaning N Suspending the instrument 2 4kg when using the sample inlet unit to connect to the piping is dangerous Use of ...

Page 18: ...Installation of the instrument without the sample inlet unit optional Please note the following when installing the instrument to piping or equipment without using a sample inlet unit optional The size of the prism stage of the instrument is a 3S ferrule The ferrule connection is recommended for installation Install the instrument so that the prism surface is at a right angle to the ground Connect...

Page 19: ... DC24V input cable connector provided to the power DC24V input terminal located at the bottom of the instrument Connect the opening of the input terminal with the connector pin and insert the connector Then fasten the connector by turning the connector ring clockwise To disconnect the power cable fully turn the connector ring counterclockwise and remove the connector Connect the power DC24V input ...

Page 20: ...connector pin and insert the connector Then turn the connector ring clockwise to fasten the connector To disconnect the DC output cable fully turn the connector ring counterclockwise and remove the connector m At this stage keep the plug disconnected from the AC 100 240V outlet m When AD 32 AD 33 or AD 34 is used the power DC24V input cable provided with the instrument is not used Fig 7 3 12 3 AD ...

Page 21: ...o 20mA signal open circuit voltage is approx 24V of the DMF and temperature 15 5 to 160 5 The DMF range to be output through the 4 to 20mA signal is set as described in Chapter 15 Setting the Recorder Output See page 30 To utilize the 4 to 20mA signal connect the Recorder Output Cable optional to the Recorder Output terminal on the main unit Recorder output cable and code table Fig 8 1 Pin No Code...

Page 22: ...the instrument and the PC should be separated by no more than 15 meters RS 232C output cable and code tables Fig 8 2 Fig 8 2 Pin No Code color 1 Black 2 Black White 3 Red 4 Shield Pin No Code color Signal name 2 Black TXD 3 Black White RXD 5 Red S GND 7 8 Fold Approx 2cm Waterproof connector plug 1 to 15m Clamp filter D sub connector 1 2 3 4 Cable ...

Page 23: ...a Tarm is used as an example Download Tera Term from a website such as the one below http ttssh2 sourceforge jp index html en 1 Start Tera Term Select serial on the New connection dialogbox Select the port number Click OK Check the port number Control Panel System and Security Device Manager Port 2 Click Setup and then Serial port ...

Page 24: ...ings are conformed to the instrument settings Enter the port number selected in step 1 Click OK 4 Click Setup and then Terminal port 5 Enter the settings as shown below and Click OK Make sure that the Local echo is checked ...

Page 25: ...ple Display DMF 06 30 6 30 25 00 25 0 LL LL 2 01 or less HH HH 40 51 or higher EE EE Error Temperature The temperature output range is 15 5 to 160 5 in the case of and is 004 1 to 320 9 in the case of F Example F Output Data Temperature Output Data Temperature LLL L 15 6 or less LLL L 4 F or less 023 5 23 5 050 0 50 F 120 0 120 0 250 0 250 F HHH H 160 6 or higher HHH H 321 F or higher ...

Page 26: ...3 or AD 34 to an outlet be sure to connect the ground pin m The instrument has no power switch When power is supplied to the instrument the measurement value display illuminates and the DMF measurement commences 1 When the instrument is used alone Confirm that the power DC24V input cable is properly connected to the instrument and the DC24V power supply When the DC24V power is supplied the instrum...

Page 27: ...struction manual When power is supplied to the instrument the DMF measurement starts m The instrument has no power switch The DMF value will be displayed when sample flows onto the prism surface If there is no sample on the prism surface only air the error message LL L will be displayed The instrument constantly detects the temperature of the prism When the sample temperature is within the range o...

Page 28: ...ay the real time measurements in DMF Hold down the key for one second Once t appears press the key C will appear C F F Use the key to select a scale Press the key to confirm the selection and t will appear Each time the key is pressed the menu item displayed switches in the order of 0 1 2 3 4 5 and DMF Select DMF N The factory default is ...

Page 29: ...lect DMF Measurement interval c There are 5 options of intervals at which the unit takes measurements The factory default is the shortest interval c 1 wherein measurements are taken every approx one second The other options indicate longer intervals c 2 is twice as slow as c 1 c 3 three times as slow and so forth The measurement interval setting is reflected on the data transmission rate Mode S le...

Page 30: ...ap water or to the true value for the reference sample by using the and or keys Fig 13 2 Pressing the sets the adjustment and the display returns to 1 Fig 13 1 Each time the is pressed the menu item displayed switches in the order of 2 3 4 5 and DMF Select DMF N If 30 seconds pass when in steps through above the display returns to the continuous DMF display To reset the reference point to original...

Page 31: ...About temperature correction for the instrument The instrument is programmed with a temperature coefficient that is specific to DMF concentration within the measurement temperature range of 5 to 40 The instrument detects the temperature of the prism and the DMF indication values are automatically corrected based upon the preset temperature correction values When the sample temperature is within th...

Page 32: ...0 Setting procedure Connect the power according to the procedure described on page 24 section 9 Power Supply The current DMF is displayed on the screen If there is no sample on the prism surface LL L will be displayed Press the key for one second t is displayed Press the key again and the display will change to 0 Press the key again to display 3 Fig 15 1 Press the key The current lower limit value...

Page 33: ...ssed the menu item displayed switches in the order of 5 and DMF Select DMF N If 30 seconds pass when in steps through above the display returns to the continuous display of the DMF m Recorder Output when an error message is displayed Please take note of the recorder output signal when an error message is displayed on the instrument unit Error Message Recorder Output LL L 4mA HH H 20mA EE E 20mA Co...

Page 34: ...d unplug from the outlet before cleaning Detach the clamp band that connects the main unit to the sample inlet unit piping or tank Clean the prism surface carefully with a soft tissue soaked with warm water or ethyl alcohol If the sample solution contains oil or grease use ethyl alcohol to ensure the prism surface does not develop a film Development of a film on the prism could cause erroneous mea...

Page 35: ...range DMF 0 0 to 40 0 Confirm that the error code HH H is replaced by the known DMF HH H The prism surface is dirty Run a sample with a DMF that is known to be within the indication range DMF 0 0 to 40 0 If HH H continues to be displayed the prism surface may need to be cleaned Clean the prism carefully as described on page 32 A sample with a DMF that significantly exceeds the upper limit value of...

Page 36: ...e AC 220 240V to the DC24V and supplies the power to the instrument Hose connector RE 67501 Outside diameter of the Hose connector 12mm φ Compression Fitting RE 67503 Compression fitting 10mmφ RE 67511 1S RE 67512 1 5S Straight type IDF ISO clamp union ferrule RE 67521 2S Straight type IDF ISO screw union screw RE 67523 2S RE 67515 25A Straight type JIS Flange RE 67525 40A RE 67611 1S Sample inlet...

Page 37: ...0mA Dimethylformamide concentration up to 40 5 can be set in 1 increments Temperature 15 5 to 160 5 4 to 20mA RS 232C output Source LED D line approximation Temperature sensor Thin film platinum sensor Materials in contact with the solution Prism Artificial sapphire Prism stage SUS316L Resistible pressure on the prism unit 0 98MPa 10kgf cm2 International Protection Class IP67 Power supply 100 to 2...

Page 38: ...36 20 Dimensions Instrument weight 2 4kg AD 32 AD 33 AD 34 Side Back detecting unit Front display unit Side Back Front ...

Page 39: ... not covered under the warranty All instruments received for repair are subject to a possible inspection fee If the unit is inspected and found to be either in good working order or is not covered by the warranty the customer will be responsible for any inspection fees repair costs including labor parts and materials use and shipping charges Replacement Part Information Please note that ATAGO cann...

Page 40: ...rvice Center nearest you The Authorized Service Center in your area will contact you within 1 to 2 business days North America Europe Canada U S A Mexico Netherlands Italy Germany France Spain U K Belgium Poland Greece Russia Belarus Ukraine Serbia Croatia Romania Central America Middle East Africa Asia Oceania Costa Rica El Salvador Guatemala Panama South America Argentina Bolivia Brazil Colombia...

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Page 42: ...37 2110 customerservice atago usa com TEL 91 22 28544915 40713232 customerservice atago india com TEL 66 21948727 9 66 21171549 customerservice atago thailand com TEL 55 16 3916 6000 customerservice atago brasil com TEL 39 02 36557267 customerservice atago italia com TEL 86 20 38108256 info atago china com TEL 7 812 777 96 96 info atago russia com TEL 234 707 558 1552 atagonigeria atago net TEL 7 ...

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