Agilent Technologies PHD-4 Instructions Download Page 2

 

 

 

 

The PHD-4 capillary leak consists of the following main parts (see figure 2): 
1) Capillary leak; 
2) Rechargeable Helium reservoir; 
3) Pressure gauge (from 0 to 11 bar/160 psi); 
4) Helium recharging valve (connections: Gc 1/4). 
5) Calibration curves 
6) Calibration chamber 
7) O-ring

 
 

3. OPERATION 

The calibration is done according to the following 
steps: 

1)  First of all, move the PHD-4 and probe away 

from Helium sources; 

2) 

Set the unit to Fixed Zero operation; 

3) 

Check the zero level; 

4)  Press simultaneously  the SENS and MODE 

pushbuttons for more than 2 seconds; 

5)  Insert the PHD-4 probe in the calibration 

chamber (see figure 3); the display show: 

- - >   C a l i b r a t i o n  

  P 

 W 

I T 

  * 

and after a few seconds the display will be as show: 

  . . . . . . . . .      

 0 

   

 

 

   <  -     C  A  L     -  >      

 

 

 
 

6)  Read on the capillary leak gauge the actual 

Helium pressure in the bottle; 

 

7) Using the pressure/concentration curve 

(attached to the Helium bottle neck), determine 
the actual concentration value in ppm; 

N.B.:  Use the pressure/concentration curve plotted 

for  your PHD-4 typology. 

8)  Pressing SENS (down button) or MODE (up 

button) pushbuttons, correct PHD-4 reading as 
necessary; 

9)  Press the SENS and MODE pushbutton 

simultaneously to exit the calibration routine and 
memorize the new setting. 

For any other information about the Calibration 
procedure refer to the

 PHD-4 instruction manual, 

Section IV, §4-2

 

NOTE 

The PHD-4 capillary leak is shipped with the 
reservoir filled with helium at low pressure. To 
operate it, a helium refilling should be performed, 
according to paragraph 4. 

 

 

 

Figure 2

 

87-900-073-01(B)  

PHD-4 capillary leak 

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