Measurement
29
Measurement
Information
:
To measure the sample volume, usually overflow measuring
beakers or measuring cylinders are used.
Chose the volume according to the measured value expected.
Too large measuring ranges will lead to inaccurate results. To
estimate the measured value you can reckon with approx. 80%
of the CBS value.
•
Sample preparation and filling of the measuring bottles
compare following
instruction: DIN 38409 part 52: "Measurement of the oxygen consumption" as
well as WTW applicationsreports see chapter "Sample preparation and
measurement"
.
•
Rinse
measuring bottle with
sample
. Empty thoroughly.
•
Exactly measure
the required oxygen-saturated (thoroughly homogenized)
quantity of the sample
according to information.
•
Put the
magnetic stirring rod
into the bottle.
•
Insert a
rubber quiver
in the neck of the bottle.
•
Put
2 sodium hydroxide tablets
into the rubber quiver with a tweezers
.
(Caution: The tablets must never come into the sample!)
•
Screw OxiTop
directly on sample bottle
(tightly close).
Start measurement:
Press S and M simutaneously.
(
2 seconds) untill the display
shows 00.
Display: Stored values are deleted.
•
Keep the measuring bottle with the OxiTop put on
for 5 days at 20°C
(e.g. in an
incubator). After the meas. temperature has been reached (after 1 hour at the
earliest, after 3 hours at the latest;
AutoTemp function
), the OxiTop
automatically starts the measurement of the oxygen consumption .
•
During the 5 days the sample is continuously stirred. The OxiTop
automatically
stores one value every 24 hours
for 5 days. To have the current value shown
press the M key.
Display current measured value:
Press M until measured value is displayed (1 second).
•
R
eadout of the stored values
after the 5 days have passed.
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