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Thermo Scientific

Dionex IC Pure system |

93

Maintenance

|

Chapter 13

Autoclaving the 0.2

μ

m final filter

Note

The lifetime of the sterile filter can be prolonged by sterilizing it. Proceed as follows to

autoclave the sterile filter.

Step

Action

Figure

1

Rotate the used sterile filter in a clockwise direc-
tion to remove it.

2

Use an autoclave to sterilize the sterile filter in a
steam autoclave at 121 °C for 30 minutes. You can
repeat the sterilization process for the sterile filter
up to 5 times.
When sterilization is completed, screw the sterile
filter back into the 1/4“ thread on the sampling tap
(see “Replacing the 0.2 µm final filter” on
page 92).

1/4“ thread

0.2 µm final filter

Note

If you wish to remove purified water and the flow

rate is too low, this is an indication that the sterile filter
is clogged. In this case, read the description in section
“Troubleshooting” on page 99, or replace the sterile
filter with a new one.

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Содержание dionex ic pure water

Страница 1: ...Thermo Scientific Dionex IC Pure Water Purification System Operating Instruction Manual 50133369 Revision C June 2016 ...

Страница 2: ...document are subject to change without notice All technical information in this document is for reference purposes only System configurations and specifications in this document supersede all previous information received by the purchaser This document is not part of any sales contract between Thermo Fisher Scientific Inc and a purchaser This document shall in no way govern or modify any Terms and...

Страница 3: ...n the intended use Thermo Fisher Scientific Inc provides this document to its customers with a product purchase to use in the product operation This document is copyright protected Any reproduction of the whole or any part of this document is strictly prohibited except with the written authorization of Thermo Fisher Scientific Inc The contents of this document are subject to change without notice ...

Страница 4: ...d party spares without Thermo Electron LED GmbH approval void the limited warranty Inspections and maintenance are performed at the specified intervals An installation verification test is performed on commissioning the system for the first time and repeated after each preventative maintenance and repair activity The warranty is valid from the date of delivery of the system to the customer The abo...

Страница 5: ...lt in death or serious injuries Note Is used for applicational hints and useful information Risk of electric shock Electrical work on the system is only to be carried out by qualified personnel Protective conductor connection Connect the power supply to an electrical socket with a protective connection Indicates a situation in which protective gloves or clothing must be worn Indicates a situation ...

Страница 6: ...g number Standards and directives The Dionex IC Pure system complies with the following standards and directives Low Voltage Directive 2014 35 EU EMC Directive 2014 30 EU ASTM D1193 6 RoHs 2011 65 EU Additionally the ultrapure water system is in compliance with many other international standards regulations and directives not listed here Should you have any questions regarding compliance with nati...

Страница 7: ...ting the external 20 L tank with level control optional 30 Illustration of drain 33 Mounting of the Power pack voltage supply 34 Connecting the control cable from the IC Pure system to a Dionex Integrion and Dionex ICS 2100 Dionex ICS 4000 Dionex ICS 5000 Dionex ICS 5000 or Dionex ICS 3000 system 36 Connecting water tubings from IC Pure system to an ion chromatograph Dionex Integrion and Dionex IC...

Страница 8: ...nd level control Optional 56 Chapter 10 Initial start up 57 Putting the system into operation 58 Dispensing water from the Dispensing valve 59 Venting the 0 2 μm final filter 59 Chapter 11 Operating elements 61 Description of control display 62 Control menu flow diagram 63 Chapter 12 System control 65 General 65 Operating Modes 65 Interval mode 65 NONSTOP mode 66 UV lamp 67 OFF mode 67 User menu 6...

Страница 9: ...8 Changing the ultrapure cartridge 78 Replacing the pretreament cartridge optional 80 Disinfection 82 Changing the ultrafilter 86 UV reactor assembly 89 Replacing the UV lamp 89 Replacing the 0 2 μm final filter 92 Autoclaving the 0 2 μm final filter 93 Recalibration of the tank sensor for an additional tank indicator 94 Draining the internal 5 L and external 20 L tank 95 Chapter 14 Waste disposal...

Страница 10: ......

Страница 11: ...Thermo Scientific Dionex IC Pure system 1 Transport and packaging Content Examination on receipt on page 2 Complaints on page 2 Packing for return shipment on page 2 ...

Страница 12: ...ainst the packing list Complaints Should damage have occurred to the goods during transport Immediately contact your delivery transport agency Save the complete packaging including the cardboard box for a possible inspection of them and or return shipment of the system Packing for return shipment If possible use the original box and packaging material When these are no longer available then CAUTIO...

Страница 13: ...is 6 days from the time of receipt of the goods The right to claim for damages ceases when this time has elapsed Note Only a trained person should take the system out of operation Prior to sending back an operated device empty the water dry the system and take out the ultrapure cartridges Plug and wrap the emptied ultrapure cartridges with a bubble wrap Return the cartridges together with the Dion...

Страница 14: ... Transport and packaging 4 Dionex IC Pure system Thermo Scientific Chapter 1 ...

Страница 15: ...ulations When an external tank with level control is used the feedwater pressure must be at least 10 kPa 1 45 psi and a maximum of 400 kPa 58 psi An additional pressure reducer must be installed should it be higher A low pressure check valve is recommended to prevent back flow of feedwater from the water system A grounded 100 240 VAC 50 60 Hz socket must be available see Electrical connections for...

Страница 16: ... on which the unit is to be installed or mounted must have an adequate load carrying capacity check the capacity and stability of the wall The dry weight of the unit is given under Dimensions and weight of Dionex IC Pure system 50132810 with ultrapure cartridge 09 1006 on page 14 When the internal tank is filled the unit has a weight during operation of approx 32 kg 70 55 lb The surface on which t...

Страница 17: ...ately rinse it with ample fresh water The unit or system components may heat up as a result of a defect It is recommended to always wear appropriate safety gloves to prevent skin damage or burns Wear safety gloves when changing the UV lamp to prevent that your skin comes in contact with the UV lamp glass Wear safety goggles when working with chlorine granulate or with disinfectant solutions If you...

Страница 18: ... Safety precautions 8 Dionex IC Pure system Thermo Scientific Chapter 2 ...

Страница 19: ...owing items are included with the Dionex IC Pure system 1 x Dionex IC Pure system Item No 50132810 1 x Filter set for Dionex IC Pure system Item No 09 1006 including 1 x Assembly kit Item No 50133371 consisting of 13 1 2 11 19 14 20 4 5 3 22 12 6 8 7 21 10 18 15 9 17 16 ...

Страница 20: ...30 12 Analyzer cable Dionex IC Pure system 50139329 13 Feedwater connecting kit 3 4 tubing thread o d 8 mm 0 31 in tubing 25 0075 14 plumbing reducer o d 8mm 0 31 in to 1 8 to Dionex IC Pure system 50143822 15 Connecting tubing o d 8 mm 0 31 in Dionex IC Pure system to 20 L tank 50146269 16 Connecting tubing concentrate o d 8 mm 0 31 in Dionex IC Pure system 50146270 17 Connecting tubing Drain o d...

Страница 21: ...al and biotechnological work with the safety levels L1 L2 and L3 Medical and microbiological laboratories according to DIN EN 12128 Laboratories in the central area of clinics and hospitals To allow working with a gradient pump system in aforementioned areas if the gradient pump is connected on the Dionex IC Pure system Unintended use The system must not be operated outside of the specifications a...

Страница 22: ... Intended use of the device 12 IC Pure Thermo Scientific Chapter 4 ...

Страница 23: ...25 C 1200 µS cm 0 0008 M cm 1 µS cm or 1 M cm Free chlorine max 0 1 ppb µg L Max 0 05 ppb µg L Manganese con tent max 0 05 ppm mg L not applicable Iron content max 0 05 ppm mg L not applicable pH range 4 11 4 11 TOC value 2000 ppb µg L max 50 ppb µg L Bacteria count 100 CFU mL 100 CFU mL Turbidity 1 0 NTU 1 0 NTU Carbon dioxide CO2 max 30 ppm mg L max 30 ppm mg L Silicate max 30 ppm mg L max 3 ppm...

Страница 24: ...e with pretreatment cartridge at manually operated POU 0 2 L min 0 2 L min Dimensions and weight of Dionex IC Pure system 50132810 with ultrapure cartridge 09 1006 Height 550 mm 21 65 in Width 306 mm 12 05 in Depth 385 mm 15 16 in Base area 277 x 372 mm 10 91 x 14 65 in Weight including ultrapure cartridge 26 kg 57 2 lb Weight with full tank 32 kg 70 55 lb Dimensions and weight of external 20 L ta...

Страница 25: ...ity 0 16 cm 1 Conductivity TOC 0 01 cm 1 Ultra pure water conductivity 0 01 cm 1 306 385 550 485 490 190 Water connections Dionex IC Pure system Feedwater tubing 8 mm 0 31 in o d Rinse water tubing 8 mm 0 31 in o d Connection to pump IC 30 psi 8 mm 0 31 in o d on 1 8 coupling Connection to pump IC 3 psi 8 mm 0 31 in o d on 1 8 coupling ...

Страница 26: ...h contact water Adjustable pressure retaining valve NBR Acrylnitril Butadien Rubber Pump head Nylon with glass fibre UV lamp High purity synthetic quartz UV Housing Stainless steel Ultrapure cartridge PP Polypropylene UF Housing PC Polycarbonate Rinsing solenoid valve PA Polyamide Dispensing valve PET Polyethyleneterephthalate Conductivity measuring cell POM Polyoxymethylen Stainless steel Distrib...

Страница 27: ...sing min 2 C max 60 C 90 relative humidity non condensing Line voltage variation Not more than 10 of the line volt age not applicable Transient over voltages As usually occur in the supply net work overvoltage category II acc to IEC 60364 4 443 Note The rated level of transient overvoltage is the withstand impulse voltage acc to overvoltage category II of IEC 60364 4 443 not applicable Ventilation...

Страница 28: ... Technical specifications 18 Dionex IC Pure system Thermo Scientific Chapter 5 ...

Страница 29: ...14 An atmospherically floor drain with an outer diameter of 63 mm or 2 48 inch DN 50 tube shall be provided The installation area must have a drain at floor level with at least a nominal outer diameter of 63 mm or 2 48 inch DN 50 pipe Should no such drain be available it is recommended to install a water watcher only for European specification Otherwise the manufacturer will not accept liability f...

Страница 30: ...er from the water system A grounded 100 240 VAC 50 60 Hz socket must be available see Electrical connections for Dionex IC Pure system and external 20 L tank on page 16 Ample working space must be provided around the unit for easy replacement of parts and for ease of operation see Accessibility to Dionex IC Pure system and external 20 L tank on page 16 Easy access for operation and control of the ...

Страница 31: ...C Pure system to a Dionex Integrion and Dionex ICS 2100 Dionex ICS 4000 Dionex ICS 5000 Dionex ICS 5000 or Dionex ICS 3000 system Connecting water tubings from IC Pure system to an ion chromatograph Dionex Integrion and Dionex ICS 2100 Dionex ICS 4000 Dionex ICS 5000 Dionex ICS 5000 or Dionex ICS 3000 system Sample Chromeleon CDS Software settings for Dionex ICS 2100 Dionex ICS 4000 system Sample ...

Страница 32: ...tting connector for sterile filter 4 Electrical connectors A 4 pin for ion chromatogram B 5 pin for tube jumper C 6 pin for level switch for external tank 5 Voltage supply connector for 24V DC 6 Quick coupling connector for to pump and to suppressor o d 8 mm 0 31 in tube 7 8 6 4 5 1 2 3 A B C A B C A B C IC Pure System without front cover front side view Electrical and Water connections IC Pure ri...

Страница 33: ...ector 6 pin for level switch for external tank 10 Fitting for o d 8 mm 0 31 in tube for A Inlet feedwater and B Tank overflow 11 Quick coupling connector for outlet o d 8 mm 0 31 in tube water supply from 20 L external tank to IC Pure system 12 1 4 thread connection for sterile vent filter 12 11 10 9 A B Note If you are using a external 20 L tank without level switch the connections A and B are fo...

Страница 34: ...pplied with the wall mounting brackets are only suitable for attaching the wall mounting brackets to a concrete wall or a solid masonry wall Step Action Figure 1 Use the wall mounting brackets to mark the anchoring points with a pen on the wall at the location where the holes are to be drilled for the wall mounting bracket Use an 8 mm 0 31 in drill bit to drill the holes See figure below 2 Insert ...

Страница 35: ...IC Pure system optional 2 Remove the cover from the ultrapure cartridge by pressing the snapper and pull the cover off toward the front 3 a Locate the ultrapure cartridge b Place the ultrapure cartridge in the rear section of the unit insert the two quick connectors into the ultrapure cartridge When you hear an audible click you can be sure that the quick action fasteners have been inserted correc...

Страница 36: ...ain 5 Connect short jumper cable into 5 pin tube jumper and 6 pin level switch external tank on right side of IC Pure system 6 Unscrew the cover for the internal 5 L feedwater tank and fill the tank with pretreated water or with potable water when you are using a pretreatment cartridge Step Action Figure Note If using IC Pure system with internal 5 L tank follow steps 5 7 If using IC pure system w...

Страница 37: ...t of 5 L tank calibrate the additional tank indicator new 8 Screw the sterile filter supplied with the unit into the 1 4 thread of the sampling tap Step Action Figure Note This additional tank indicator has already been calibrated at the factory If recalibration is required refer to Recalibration of the tank sensor for an additional tank indicator Note The additional tank indicator on the unit wil...

Страница 38: ...f the connections prevents any incorrect switched installation Note Keep the tube jumper in a safe place for later use e g in the disinfection procedure Tube jumper Quick connectors a Concentrate Note The external 20 L tank 50146376 will not be use the additional tank indicator on the IC Pure system directly After filling the tank manually and connecting the control cable to the IC Pure system the...

Страница 39: ...d 8 mm 0 31 in tube to the left connection of the 20 L tank d Attach the tube from the IN nozzle on the unit to one of the two connections on the external 20 L tank e Attach the o d 8 mm 0 31 in tube into the right connection of the external 20 L tank for tank overflow and route the tube with a downward slope to the drain Note If you are not using a pretreatment cartridge skip to step d Note Eithe...

Страница 40: ... tank The concentrate back flow from the Dionex IC Pure system into the external 20 L tank multiplies the ion content of water in the external 20 L tank a c Level switch cable Additional tank indicator Tank Unit Note The external 20 L tank with level control allows the automatic filling of the external tank The external 20 L tank with level control must be connected to a pressurized source The fee...

Страница 41: ... onto the feedwater tap c Attach the other end of the o d 8 mm 0 31in tubing to the left feedwater connection on the side of the external 20 L tank with level control Wet the end of the tubing with water before inserting 3 a Wet end of the tube with water and insert the o d 8 mm 0 31 in tube into the right connection of the external 20 L tank with level control for tank overflow Feedwaterconnectio...

Страница 42: ...s switch on the additional tank indicator on the unit and check the filling level Step Action Figure Note An illustration of the drain is given under Illustration of drain Concentrate connection on the unit o d 8 mm 0 31 in tube Note The power supply for the external 20 L tank with level control is delivered from the control wire of the Dionex IC Pure system Note This additional tank indicator has...

Страница 43: ...route it to an atmospherically vented drain The tubes that run from the Dionex IC Pure system to the drain must be routed with a downward slope and without any kinks or restrictions to ensure proper drainage If a standard drain siphon is in place the ends of the tubes must be located at least 20 mm 0 75 in above the drain Attach the tubes in such a manner that they remain in their position Minimum...

Страница 44: ...on to ensure that the plug and the power cable do not get wet Mount the power pack with dry hands Risk of an electrical shock Step Action Figure 1 Remove the protective foil on the back of the universal holder and from the universal adapter and attach the universal holder to the center of the back of the main adapter 2 Attach universal adapter to a smooth wall surface with supplied screws or with ...

Страница 45: ...ystem Next plug the power supply to a grounded 100 240 VAC 50 60 Hz power outlet 5 Switch the unit on and enter the serial number of the ultrapure cartridge in the control menu Changing the ultrapure cartridge The unit is ready for use now Step Action Figure CAUTION Do not bring the power pack in contact with water Risk of an electrical shock Note The removable power cable must always face downwar...

Страница 46: ...em and the ion chromatograph IC system are switched off Section Action Steps 1 Connecting the control cable from the IC Pure system to a Dionex Integrion and Dionex ICS 2100 Dionex ICS 4000 Dionex ICS 5000 Dionex ICS 5000 or Dionex ICS 3000 system 1 2 and 8 15 2 Set up of IC Pure system to single Dionex ion chromatograph 3 7 3 Set up an additional ion chromatograph to the IC Pure system as shown o...

Страница 47: ...case you must then make the settings for the Thermo ScientificTM DionexTM ChromeleonTM Chromatography Data System CDS Software Relay_2 refer to step 8 page 39 b The bottom dual pump DP Pump1 that you have selected for the Dionex ICS 5000 Dionex ICS 5000 or Dionex ICS 3000 system screw the two conductors of the connecting cable into Pins 14 and 15 of the connector and connect this to the back of th...

Страница 48: ...tegrion and Dionex ICS 2100 Dionex ICS 4000 Dionex ICS 5000 Dionex ICS 5000 or Dionex ICS 3000 system see Schematic illustration with connected suppressor Step Action Figure Connecting water tubings from IC Pure system to an ion chromatograph Dionex Integrion and Dionex ICS 2100 Dionex ICS 4000 Dionex ICS 5000 Dionex ICS 5000 or Dionex ICS 3000 system Note If hooking up more than one ion chromatog...

Страница 49: ...askbar To open the Service Manager window click or right click the Chromeleon Tray Icon 9 If the Chromeleon Tray Icon is not present you can start the Service Manager by selecting Start All Programs Thermo Chromeleon 7 Services Manager Closing the Service Manager window minimizes it to the Chromeleon Tray Icon 10 In the Chromeleon CDS Server Configuration open the corresponding configuration setti...

Страница 50: ...uration Panel 14 Place a check mark in the box for Flow Zero See Sample Chromeleon CDS Software settings for Dionex ICS 2100 Dionex ICS 4000 system See Sample Chromeleon CDS Software settings for Dionex ICS 5000 Dionex ICS 5000 and Dionex ICS 3000 system 15 Save your settings and exit the configuration settings The Dionex Integrion and Dionex ICS 2100 Dionex ICS 4000 Dionex ICS 5000 Dionex ICS 500...

Страница 51: ...Thermo Scientific Dionex IC Pure system 41 Installation Chapter 7 Sample Chromeleon CDS Software settings for Dionex ICS 2100 Dionex ICS 4000 system Dionex ICS 4000 system ...

Страница 52: ...5000 or Dionex ICS 3000 system in the feed line to the first IC system Both IC systems will then continue to be controlled using the Chromeleon CDS software The IC system that is connected to the control line at the unit serves as the master The second IC system does not have to be connected to the Dionex IC Pure system If the IC system connected to the Dionex IC Pure system is switched off neithe...

Страница 53: ...re Step Action Figure Note Again ensure that the cutting ring and the taper coupling are installed correctly see Connecting the control cable from the IC Pure system to a Dionex Integrion and Dionex ICS 2100 Dionex ICS 4000 Dionex ICS 5000 Dionex ICS 5000 or Dionex ICS 3000 system Step 4 1 8 tube T piece Note The system must be switched off The feedwater supply must be closed Check that the IC Sys...

Страница 54: ...tion fasteners have been inserted correctly 5 Take the precision metering valve and plug in the 1 8 tube coming from the Dionex IC Pure system into the left side from the precision metering valve 6 Proceed the same way as describe in step 5 with the 1 8 tube into the right connection side of the precision metering valve This tube is connecting to the Regen In connection of the suppressor from the ...

Страница 55: ...he flow rate should be determined with the suppressor connected to the suppressor supply line of the Dionex IC Pure system and with the suppressor turned off The flow will be lower once the suppressor is switched on and should be checked again 1 Record the weight of an empty container 2 Insert the waste line from the suppressor into the container and weigh the contents after a known time interval ...

Страница 56: ...00 system Eluent in EGC Vent OverͲ flow Suppressor line REGEN IN 1 4 2 3 1 Waste Precision metering valve 1 Connection panel Dionex IC Pure system To pump 3 psi Eluent in 4 2 3 To suppressor 30 psi Drain Tank overflow Note 1 Tubing from CD cell out should be routed to waste Pressure restrictor coils are required to be install at the CD cell outlet 1 ...

Страница 57: ... Precision metering valve Tee Suppressor line REGEN IN 1 2 3 Connection panel Dionex IC Pure system To pump 3 psi To suppressor 30 psi Drain Suppressor line REGEN IN Precision metering valve 4 3 Tank overflow Note 1 Tubing from CD cell out should be routed to waste Pressure restrictor coils are required to be install at the CD cell outlet 1 ...

Страница 58: ...SͲ4000 system Eluent line Overflow 1 2 3 4 Waste 1 2 3 Connection panel Dionex IC Pure system To pump 3 psi To suppressor 30 psi Drain Suppressor line REGEN IN Precision metering valve 4 3 Tank overflow metering valve 1 Note 1 Tubing from CD cell out should be routed to waste 1 Dionex ICS 4000 system ...

Страница 59: ...4 Precision metering valve l Tee Waste 1 2 3 Suppressor line REGEN IN 1 Eluent line 1 Precision metering valve Suppressor line REGEN IN 1 2 Connection panel Dionex IC Pure system To pump 3 psi To suppressor 30 psi 1 4 3 Drain Tank overflow 1 Note 1 Tubing from CD cell out should be routed to waste 1 ...

Страница 60: ...Pure system Eluent Eluent in in Overflow Overflow 1 4 2 3 To pump 3 psi To suppressor 30 psi Drain Tank overflow Waste Waste 2 3 4 1 Precision metering valve 1 Suppressor line REGEN IN Note 1 Tubing from CD cell out should be routed to waste Pressure restrictor coils are required to be install at the CD cell outlet 1 ...

Страница 61: ...low line 1 Waste Suppressor REGEN IN Tee 1 4 2 3 Eluent line Tee 1 Connection panel Dionex IC Pure system To pump 3 psi ision ering valve 4 2 3 To suppressor 30 psi Drain Tank overflow 1 Preci mete Suppressor line REGEN IN 1 Note 1 Tubing from CD cell out should be routed to waste Pressure restrictor coils are required to be install at the CD cell outlet 1 ...

Страница 62: ... Installation 52 Dionex IC Pure system Thermo Scientific Chapter 7 ...

Страница 63: ...ex IC Pure system 53 Flow chart Dionex IC Pure system with pretreatment and 20 L tank Drain Dionex IC Pure system with 5 L tank Ultrapure water ASTM Type I Pure water ASTM Type II Tap water Ultrapure water ASTM Type I Drain ...

Страница 64: ... F6 Pretreatment cartridge with activated carbon optional V8 Check valve 1bar LIS100 Float switch V9 Raw water solenoid valve LIS 101 Float switch optional S2 Sterile overflow LIS 102 Float switch optional S1 Sterile overflow optional LIS 103 Float switch optional P1 Pressure pump UV1 UV lamp QIA 300 Feedwater conductivity measuring cell QIA 301 TIA500 Ultrapure water conductivity measuring cell T...

Страница 65: ...to be fed with potable tap water The concentrate waste water must be routed to drain Potable water must first be filled manually into the internal 5 L or external 20 L tank for operation of the unit After the water is pumped through the pretreatment cartridge it is then recirculated throughout the unit to the UV bulb ultrapure cartridge and an ultrafilter The purity of the water s conductivity res...

Страница 66: ...ltaneously Dionex IC Pure system with external 20 L tank and level control Optional The external 20 L tank with level control allows potable tap water to feed directly If the level in the 20 L tank should fall to the minimum level the tank is refilled automatically After the water is pumped through the pretreatment cartridge it is then recirculated throughout the unit to the UV bulb ultrapure cart...

Страница 67: ...mo Scientific Dionex IC Pure system 57 Initial start up Content Putting the system into operation on page 58 Dispensing water from the Dispensing valve on page 59 Venting the 0 2 µm final filter on page 59 ...

Страница 68: ...e Note If an IC System is connected to the unit and switched on Analyser will appear on the control display of the Dionex IC Pure system The Nonstop and Interval mode are then no longer available The user menu can continue to be used however Note To vent air from the system switch the system 3 times successively to Rinsing in the menu and discard approx 5 L of water each time with the manual dispe...

Страница 69: ...knob Turn the knob clockwise to slow down or stop water flow CAUTION Do not over tighten knob once flow stops doing so could damage dispensing valve Knob Counter clock wise to dispense water Step Action Figure 1 The first time you dispense pure water at the main dispenser through the 0 2 µm final filter open the white knurled screw 2 Do not close the knurled screw until pure water runs out of the ...

Страница 70: ... Initial start up 60 Dionex IC Pure system Thermo Scientific Chapter 10 ...

Страница 71: ...Thermo Scientific IC Pure 61 Operating elements Contents Description of control display on page 62 Control menu flow diagram on page 63 ...

Страница 72: ... for sampling for increasing the numeric values in the menu On Off switch UV button enables manual operation of the UV lamp The desired value can be changed in the Mode menu The Menu button provides access to the following system parameters Feedwater limiting value Ultra pure water limiting value UV Lamp operating time Cartridge number and maintenance interval Rinsing Disinfection Display of error...

Страница 73: ...s Enter UV Menu UV Time 3000 h UV Menu UV Intensity Off UV Time ultrapure cartridge New UV lamp Press enter _ 450 days OEM Menu Language English Feedwater 3 55 M cm Limit value feed 2 0 µS cm Error display Standby Off Lim val pure w 2 0 µS cm UV Time 00005 h UV Intensity Serial no ultrapure cartridge Press enter 00000 00 Rinse Press enter Disinfection Press enter Error Log Press enter Code Press e...

Страница 74: ... Operating elements 64 IC Pure Thermo Scientific Chapter ...

Страница 75: ... an Dionex Integrion and Dionex ICS 2100 Dionex ICS 4000 Dionex ICS 5000 Dionex ICS 5000 or Dionex ICS 3000 system TOC is only displayed when the unit is in Nonstop and Analyser mode Conductivity Resistivity is displayed in every mode UV is shown on the display when the UV light in on TC is showed if temperature compensation is on In the event of an error the fourth line of display will display mo...

Страница 76: ... regardless of the active operating mode The display shows NONSTOP mode The control system switches the unit to the Nonstop mode when the NONSTOP button is pressed The Nonstop mode is the only mode in which pure water can be taken from the tap The Nonstop mode ends automatically at programmed intervals e g after 2 hours or when you press the INTERVAL button The unit then continues to operate in th...

Страница 77: ...e Menu button to scroll to the next menu item Each further press on the Menu button moves you further from one menu prompt to the next Settings can be changed with the arrow keys To change numbers use the Arrow buttons to go from 0 9 and the UV button to move to next digit When you confirm a value by pressing on the Enter button you are taken to the next menu prompt Settings can only be made when ...

Страница 78: ... will be displayed in both Interval and Nonstop modes When the error display is switched off the error is only displayed in Nonstop mode The Lim val pure w message is displayed when the limiting value is exceeded Ultrapure water measuring range 0 1 M cm Limiting value setting range 0 055 5 0 µS cm Basic setting 0 2 µS cm 10 M cm Basic setting error suppression On With settings above 5 0 µS cm the ...

Страница 79: ...is rinses or flushes the unit to drain During the rinse the pump and solenoid valve V4 are activated for a programmed period of time as set in the OEM menu see Set the interval rinse time on page 74 Note You can find more information in chapter Replacing the UV lamp on page 89 Note You can find more information in chapter Changing the ultrapure cartridge on page 79 Step Action Figure 1 Press the M...

Страница 80: ...apsed the rinsing solenoid valve opens until the disinfection procedure has finished The message New Filterset must be fitted is then displayed When this is fitted a confirmation press on the Enter button returns the system to the last operating mode The remaining disinfection time is counted down and displayed during the disinfection procedure Step Action Figure 1 Press the Menu key six times The...

Страница 81: ...able is entered and confirmed with Enter The unlocking is only active for a 5 minute period Press the Menu key nine times The display shows Step Action Figure 1 Press the Menu key seven times The display shows 2 Confirm error history by put ting the Enter button Now you can see two last saved errors with date and time The error code can be requested at the local service organization Note You can a...

Страница 82: ...Press enter On confirming this by pressing the Enter button the first menu point is called to be worked on To simplify making changes a press on the UV button allows the position that is to be changed in a number to be selected so that the Arrow buttons can be used to replace it with any digit from 0 9 A press on the Menu button takes you to the next menu prompt After system control has been unloc...

Страница 83: ...ing time Rinse time is the amount of time the V4 Solenoid valve is opened to flush water to drain This is helpful to purge air or impurities from the system Basic setting 30 sec Setting range 10 60 sec After entering the OEM menu press the Menu button two times The display shows Change the disinfection time The disinfection time can be set in this menu Disinfection time is the length of time requi...

Страница 84: ...shows Set the interval rinse time In this menu the rinse interval time can be set When the system operates in the Interval mode the system will rinse water to drain for 0 5 seconds every 30 minutes Basic setting 0 5 sec Setting range 0 1 2 sec After entering the OEM menu press the Menu button five times The display shows Set the real time clock The real time clock can be set in this menu Basic set...

Страница 85: ...0 5 12 hours After entering the OEM menu press the Menu button seven times The display shows Language selection Basic setting English Setting range Deutsch English French After entering the OEM menu press the Menu button eight times The display shows Select units conductivity resistance Basic setting Resistance M cm Setting range Resistance M cm Conductivity µS cm After entering the OEM menu press...

Страница 86: ...number of the unit can be viewed However the serial number of the system is an unalterable factory setting After accessing the OEM menu press the Menu button eleven times The display shows Note Turning the temperature compensation off will cause the displayed purity readings to change according to the water temperature Note The system is factory adjusted in the system control In this section it is...

Страница 87: ... operating instructions The operating instructions must be kept in an easily accessible location for anyone who is using or servicing the unit Calibration of the conductivity sensor may only be performed by a service technician authorized by the manufacturer Content Maintenance Intervals on page 78 Changing the ultrapure cartridge on page 79 Replacing the pretreament cartridge optional on page 80 ...

Страница 88: ...on electrical equipment are only to be carried out by qualified electricians Unplug the system from the main power outlet for all maintenance work on the system Material Flow chart no Item No Interval Other problems Ultrapure cartridge F1 09 1006 up to 12 months Or when the pure water limit value is exceeded whichever occurs first Bacteria growth may occur in the resin when the unit has been in us...

Страница 89: ...and outlet of the ultrapure cartridge and remove the used cartridge 4 We recommend performing a disinfection when an existing ultra pure cartridge is replaced 5 Place the ultrapure cartridge in the rear section of the unit and insert the two quick connectors into the ultrapure cartridge When you hear an audible click you can be sure that the quick action fasteners have been inserted correctly 6 Pu...

Страница 90: ...irm your entry by pressing Enter The new serial number for the ultrapure cartridge is then stored You can only use a ultrapure cartridge serial number one time 8 Step Action Figure Note For this action you must have a Level 1 code Refer to section Entering a Code number on page 71 to read where to find this code and how to enter it a b c Note Discharge the first 5 L Note The pretreatment cartridge...

Страница 91: ...e was first installed or with the yellow plugs that came with replacement cartridge in step 4 below 4 Locate the new pretreatment cartridge and insert the car tridge into the unit 5 Insert the quick connectors into the connecting points on the new pretreatment cartridge When you hear an audible click you can be sure that the quick connectors have been inserted correctly 6 Put the cover back in pla...

Страница 92: ...ICS 2100 Dionex ICS 4000 Dionex ICS 5000 Dionex ICS 5000 or Dionex ICS 3000 system from the Dionex IC Pure system Disconnect the tubes for the IC system from the connections at the Dionex IC Pure system Note To ensure effective disinfection of your unit fill the internal 5 L or external 20 L tank 80 with water You can read off the level of both tanks using the additional tank indicator on the unit...

Страница 93: ...h quick connectors for the ultrapure cartridge When you hear an audible click you can be sure that the quick connectors have been inserted correctly b Of the three pretreatment connections on the unit fit the right and center on in the tube jumper When you hear an audible click here you can be sure that the quick action fasteners have been inserted correctly Note If you are using an optional pretr...

Страница 94: ...he dis play and then press Enter a In the user menu press the Menu button to scroll to Disinfection Press Enter b The display shows Disinfection cartridge Press Enter to confirm that Disinfection cartridge or Disinfection adapter has been installed c The disinfection process is then started Step Action Figure Note There is no cause of worry should you notice a chlorine smell during the entire disi...

Страница 95: ...h the 20 L tank and then reattach the supply line for the 20 L tank to the connection on the Dionex IC Pure system e Switch the Dionex IC Pure system off and refill the tank completely with feedwater f Switch the unit back on and dispense around 10 L of water from the external tank at the sampling tap Step Action Figure Note To drain the content of the 5 L tank the Dionex IC Pure system must be in...

Страница 96: ...e cartridge tube jumper by pressing on the quick connectors at the connections for the pretreatment cartridge and then install a new pretreatment cartridge see Replacing the pretreament cartridge optional on page 80 7 Switch the system on Step Action Figure Tube jumper Quick connectors b Adapter for disinfection Quick connectors a Note You will need the following tools for replacing the ultra filt...

Страница 97: ... out e Pull the ultra filter out of the mounting bracket f Hold the tube still attached to it with one hand while rotating the ultra filter in a counter clockwise direction with the other hand until the Luerlock is loosened and you can pull the ultra filter out of the unit g Mark the position of the fittings before removing them Use the open end wrench size 17 mm 0 67 in to unscrew the top and bot...

Страница 98: ... and bottom connection for the ultrafilter and screw the fittings securely into place e Insert the ultrafilter back into the mounting bracket f Screw the UV assembly back into place see Step 2c 4 Replace the cover on the unit open the supply of the feedwater once the unit has been connected to the 20 L tank filling station and switch the unit on Dispense 5 L of water and activate three rinses for ...

Страница 99: ... Item No 21 5048 O ring Item No 21 5030 Immersion tube UV lamp casing Item No 22 0092 UV lamp Item No 09 1002 Immersion tube Item No 22 0040 Stopper Item No 14 0187 Stopper Item No 21 5008 These stoppers are located in the UV lamp casing UV lamp CAUTION Never look directly into a UV lamp when it is on It could damage your sight ...

Страница 100: ...ion Figure 1 Switch the Dionex IC Pure system off 2 Remove the cover for the ultrapure cartridge 3 a Take the ultrapure cartridge out of the unit see Changing the ultrapure cartridge on page 79 If an optional pretreatment cartridge is installed remove it too see Replacing the pretreament cartridge optional on page 80 b Use the Phillips screwdriver to unscrew the two screws from the bracket for the...

Страница 101: ...you do not touch it with your fingers This could impair proper functioning of the lamp We therefore recommend that you wear clean disposable gloves when performing this work CAUTION When installing a new UV lamp ensure that the flat seal ring and the O ring are on the correct position The flat seal ring must fit exactly in the groove provided for it on the top of the union nut figure 1 and 2 The O...

Страница 102: ...d UV button simultaneously The display shows UV Menu d Push the Menu button repeatedly until new UV lamp appears and press enter to confirm The Display shows then Please wait Step Action Figure Note For this action you must have a Level 3 code Refer to section Entering a Code number on page 71 to read where to find this code and how to enter it Note The system sets the operating hours counter of t...

Страница 103: ...ile filter in a steam autoclave at 121 C for 30 minutes You can repeat the sterilization process for the sterile filter up to 5 times When sterilization is completed screw the sterile filter back into the 1 4 thread on the sampling tap see Replacing the 0 2 µm final filter on page 92 1 4 thread 0 2 µm final filter Note If you wish to remove purified water and the flow rate is too low this is an in...

Страница 104: ...ws a level of 100 c Locate the setting screw of the sensor for additional tank indicator and rotate the setting screw until the indicator shows 90 d Stop the rotating of the setting screw as soon as it reaches 100 on the tank indicator display b Cover Snapper Note A small setting screw is also located on the sensor module You can use this screw for adjustment the additional tank indicator On the i...

Страница 105: ... connected to the system Note This process is required only when you operate your Dionex IC Pure system with a pretreatment cartridge and without any external 20 L tank with level control CAUTION Without the external 20 L tank with level control the concentrate of the pretreatment cartridge is redirected into the tank which degrades the feedwater purity and increases the conductivity Therefore at ...

Страница 106: ...hen using an external 20 L tank take the Take the drain piece for tank IC Pure o d 8 mm 0 31 in tube with female quick disconnect supplied with it and attach it to the bottom connection on the front of the 20 L tank and route the tube with a slight downward slope to the drain see Illustration of drain on page 33 When you hear an audible click the quick connectors have been inserted correctly 3 a O...

Страница 107: ...omic Area to contact our local service centre or our headquarters weee recycle thermofisher com WEEE Reg no DE 12471402 In countries outside of the European Economic Area please contact your local authorities or waste disposal company Note Before returning your Dionex IC Pure system for waste disposal contact your local service organization or waste disposal company for proper disposal of the syst...

Страница 108: ... Waste disposal 98 Dionex IC Pure system Thermo Scientific Chapter 14 ...

Страница 109: ...e sterile filter see Replacing the 0 2 µm final filter on page 92 Install new pretreatment cartridge Resistance 18 2 M cm Cartridge is exhausted Temperature compensation deactivated recalibration required Check feedwater quality Activating temperature compensation TC should appear in the display Contact the service organization for calibration Control panel non responsive Microprocessor locked up ...

Страница 110: ...nex IC Pure system for operation with an analyzer Settings in OEM menu are incorrect IC system not activated Cable to IC system not connected Cable break Correct the settings in the OEM menu see OEM menu on page 72 Activate IC system Connect the cable to the IC system Replace the cable Wrong time or date Time zone Summer winter time Reset time and date Wrong language Wrong language set Correct lan...

Страница 111: ...lace measuring cell Replace system control see Ultra pure water limiting value on page 68 Error message Measuring cell LF2 Measuring cell cable break System control defect Feedwater conductivity outside measuring range Replace measuring cell Replace system control see Feedwater limiting value on page 67 Error message Measuring cell LF3 Measuring cell cable break System control defect Replace measu...

Страница 112: ... Troubleshooting 102 Dionex IC Pure system Thermo Scientific Chapter 15 ...

Страница 113: ...ries or wear parts from other manufacturers will nullify the warranty for this unit Figure Part number Description 1 50132730 2 50132289 3 50134036 4 50142984 5 17 0147 6 50134032 7 26 0025 8 50133988 Keyboard foil Display front part Display holder Tank indicator Display back part Rotary knob Control display part Dispensing valve ...

Страница 114: ...4 50133996 15 50149264 16 50142981 17 50131190 18 50142246 19 16 0126 20 50133979 21 50150598 Connector Connector Concentrate adjust valve TOC measuring cell Ultrapure water measuring cell Connector Pressure pump Sensor for tank indicator Solenoid valve Pressure hold valve Feedwater measuring cell Fuseholder with fuse Check valve 1 0 9 1 5 1 6 1 7 1 9 1 8 2 1 2 0 1 4 1 3 1 2 1 1 ...

Страница 115: ...6 UV booster unit Control interface part Figure Part number Description 24 50143195 25 50131190 26 50142891 27 50148086 28 50148086 29 50145876 30 50143964 31 50149597 Level control unit Solenoid valve Sensor for tank indicator Float switch Float switch Wire jumper not shown Connecting wire 20 L tank not shown Taple top power supply not shown ...

Страница 116: ... Dionex IC Pure system spare parts 106 Dionex IC Pure system Thermo Scientific Chapter 16 ...

Страница 117: ...91 Designation Item No Hardness Stabilizer to pretreat potable water for hard water Recommended for water hardness exceeding 10 dH or 178 ppm 09 4001 Carbon filter to treat chlorinated tap water if using pretreatment cartridge only if experiencing short pre treatment life 50134022 Pretreatment cartridge 09 2012 Wall mounting bracket 09 2212 External 20 L tank 50146376 External 20 L tank with level...

Страница 118: ... Consumables 108 Dionex IC Pure system Thermo Scientific Chapter 17 ...

Страница 119: ...Thermo Scientific Dionex IC Pure system 109 Terminal assignment ...

Страница 120: ... Terminal assignment 110 Dionex IC Pure system Thermo Scientific Chapter 18 ...

Страница 121: ...quality of the system 1x Weekly enter measured values Customer address Location System type Serial no Year made Date Feedwater resistance MΩ cm Ultrapure water resistance MΩ cm Temperature C UV lamp operating time h Ultra pure water volume flow l h Last change of ultrapure cartridge Last cleaning disinfection Notes Signature ...

Страница 122: ... Maintenance record 112 Dionex IC Pure system Thermo Scientific Chapter 19 ...

Страница 123: ...from Latin America Sales 1 866 984 3766 Service 1 866 984 3766 Enquiries from Asia China Sales 86 10 8419 3588 Service toll free 1 8008105118 Support Mobile 4006505118 or 86 10 8419 3588 India Sales 91 22 6716 2200 Service toll free 1 800 22 8374 or 91 22 6716 2200 Japan Sales 81 45 453 9220 Service 81 45 453 9224 Inquiries from other countries Asia Australia New Zealand Sales 852 2885 4613 Servic...

Страница 124: ...ll free 0800 1 112110 or 49 6184 90 6940 E mail info labequipment de thermofisher com Italy Sales 39 02 95059 341 Service 39 02 95059 250 Netherlands Sales 31 76 579 5555 Service 31 76 579 5639 Russia CIS Sales 7 812 703 4215 Service 7 812 703 4215 Spain Portugal Sales 34 93 223 0918 Service 34 93 223 0918 Switzerland Sales 61 716 7755 Service 61 716 7755 UK Ireland Sales 44 870 609 9203 Service 4...

Страница 125: ...e number 71 Entering the serial number 76 Error history 71 Examination on receipt 2 Extent of delivery 9 F Feedwater requirements 13 Filter cartridge Change 80 Final Autoclave 93 Final filter Change 92 Flow chart 53 Functional Describtion 55 G General 65 I ICS 2100 46 Illustration of drain 33 Initial start up 57 Installation 21 Intended use of the device 11 Interval mode 65 L Language selection 75...

Страница 126: ...pure cartridge serial number 69 Unlocking code 72 UV lamp 67 UV reactor assembly 89 V Venting the sterile filter 59 W Wall Mounting 24 Waste disposal 97 Water connections DIONEX IC Pure system 15 Water connections for external 20L tank 16 ...

Страница 127: ...Thermo Scientific IC Pure 117 ...

Страница 128: ...entific Inc and its subsidiaries Specifications terms and pricing are subject to change Not all products are available in all countries Please consult your local sales representative for details thermoscientific com Thermo Fisher Scientific 1214 Oakmead Parkway Building 10 Sunnyvale CA 94085 BRXXXXX_E 01 14W ...

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